DIN EN 15664-1-2014 Influence of metallic materials on water intended for human consumption - Dynamic rig test for assessment of metal release - Part 1 Design and operation German .pdf

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1、March 2014 Translation by DIN-Sprachendienst.English price group 15No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS

2、67.250!%,Sj“2094871www.din.deDDIN EN 15664-1Influence of metallic materials on water intended for humanconsumption Dynamic rig test for assessment of metal release Part 1: Design and operation;English version EN 15664-1:2008+A1:2013,English translation of DIN EN 15664-1:2014-03Einfluss metallischer

3、Werkstoffe auf Wasser fr den menschlichen Gebrauch Dynamischer Prfstandversuch fr die Beurteilung der Abgabe von Metallen Teil 1: Auslegung und Betrieb;Englische Fassung EN 15664-1:2008+A1:2013,Englische bersetzung von DIN EN 15664-1:2014-03Influence des matriaux mtalliques sur leau destine la conso

4、mmation humaine Banc dessai dynamique pour lvaluation du relargage de mtaux Partie 1: Conception et fonctionnement;Version anglaise EN 15664-1:2008+A1:2013,Traduction anglaise de DIN EN 15664-1:2014-03SupersedesDIN EN 15664-1:2008-06 andDIN EN 15664-1 Corrigendum1:2009-07www.beuth.deDocument compris

5、es 32 pagesIn case of doubt, the German-language original shall be considered authoritative.02.14DIN EN 15664-1:2014-03 2 A comma is used as the decimal marker. National foreword This document (EN 15664-1:2008+A1:2013) has been prepared by Technical Committee CEN/TC 164 “Water supply” (Secretariat:

6、AFNOR, France). The responsible German body involved in its preparation was the Normenausschuss Wasserwesen (Water Practice Standards Committee), Working Committee NA 119-04-14 AA Werkstoffe und Bauteile in Kontakt mit Trinkwasser. Amendments This standard differs from DIN EN 15664-1:2008-06 and DIN

7、 EN 15664-1 Corrigendum 1:2009-07 as follows: a) normative references have been updated; b) Table C.1 “Test water monitoring and analysis Data on test water composition” has been revised and rendered more precise. Previous editions DIN 50931: 1960-12, 1999-11 DIN EN 15664-1: 2008-06 DIN EN 15664-1 C

8、orrigendum 1: 2009-07 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 15664-1:2008+A1 November 2013 ICS 67.250 Supersedes EN 15664-1:2008English Version Influence of metallic materials on water intended for human consumption - Dynamic rig test for assessment of metal release -Part 1: Design and

9、 operation Influence des matriaux mtalliques sur leau destine la consommation humaine - Banc dessai dynamique pour lvaluation du relargage de mtaux - Partie 1: Conceptionet fonctionnement Einfluss metallischer Werkstoffe auf Wasser fr den menschlichen Gebrauch - Dynamischer Prfstandversuch fr die Be

10、urteilung der Abgabe von Metallen - Teil 1: Auslegung und Betrieb This European Standard was approved by CEN on 28 October 2007 and includes Amendment 1 approved by CEN on 12 October 2013. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for gi

11、ving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three of

12、ficial versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies

13、of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain

14、, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2013 CEN All rights of exploitation in any form and by any means reserved worldwide

15、for CEN national Members. Ref. No. EN 15664-1:2008+A1:2013 EEN 15664-1:2008+A1:2013 (E) 2 Contents Page Foreword 4 Introduction .5 1 Scope 6 2 Normative references 6 3 Terms and definitions .7 4 Principle 9 5 Test rig 9 5.1 General 9 5.2 Test rig arrangement .9 5.3 Control line 10 5.4 Test lines . 1

16、0 5.4.1 General . 10 5.4.2 Materials in the form of pipes 10 5.4.3 Materials in the form of test pieces. 10 5.5 Reference lines for comparative testing 10 6 Operating conditions 10 6.1 General . 10 6.2 Conditioning 11 6.3 Fractional Sampling . 11 6.3.1 General . 11 6.3.2 Calculation and expression o

17、f results for fractional sampling 11 6.3.3 Requirements for the hydraulic function of the test rig . 13 6.3.4 Determination of sampling volumes . 13 6.4 Normal operation of the test rig 14 7 Test water 14 7.1 Composition 14 7.2 Check of test water . 14 8 Sampling 15 8.1 General . 15 8.2 Test water s

18、ampling . 15 8.3 Sampling to determine metal release . 15 8.4 Sampling volumes 16 8.4.1 General . 16 8.4.2 Test lines with test pieces . 16 8.4.3 Test pipes 16 9 Analysis . 16 10 Expression of results . 16 10.1 Metal concentrations after fixed stagnation time 16 10.2 Equivalent pipe concentration 16

19、 10.3 Mean concentration after a given operating time 17 10.4 Presentation of the test results . 17 11 Test report . 17 Annex A (normative) Test rig components and assembly. 19 A.1 Test rig . 19 A.2 Test piece 20 DIN EN 15664-1:2014-03 EN 15664-1:2008+A1:2013 (E) 3 A.3 Connecting piece . 21 Annex B

20、(normative) Test rig flow regime 23 B.1 Test rig flow regime and sampling plan (24 h cycle) . 23 B.2 Test rig flow regime and sampling plan for 16 h stagnation time 24 Annex C (normative) Test water monitoring and analysis Data on test water composition 25 Annex D (informative) Example of graphs for

21、 expression of results 27 Bibliography 30 DIN EN 15664-1:2014-03 ! “EN 15664-1:2008+A1:2013 (E) 4 Foreword This document (EN 15664-1:2008+A1:2013) has been prepared by Technical Committee CEN/TC 164 “Water supply”, the secretariat of which is held by AFNOR. This European Standard shall be given the

22、status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2014, and conflicting national standards shall be withdrawn at the latest by May 2014. Attention is drawn to the possibility that some of the elements of this document may be the subject

23、 of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document includes Amendment 1 approved by CEN on 12 October 2013. This document supersedes EN 15664-1:2008. The start and finish of text introduced or altered by amendment is indic

24、ated in the text by tags . This European Standard is one of a series of test methods that supports associated product standards. The standard has been prepared under the mandate given to CEN by the Commission of the European Communities and the European Free Trade Area deleted text. With respect to

25、potential adverse effects on the quality of water intended for human consumption caused by metallic materials, attention is drawn to the fact that the relevant national regulations remain in force until the adoption of verifiable European acceptance criteria. Water intended for human consumption is

26、hereafter referred to as “drinking water” and means the same as the definition given at Article 2(1) of the Council Directive 98/83/EC on the quality of water intended for human consumption. This European Standard has been drafted in accordance with the CEN Internal Regulations, Part 3. This Europea

27、n Standard is Part 1 of a series dealing with the test method to determine the release of metals from metallic products into drinking water comprising: Part 1: Design and operation; ! Part 2: Test waters.“ Part 1 describes a test method to produce contact waters for the assessment of metal release f

28、rom metallic materials. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic o

29、f Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. DIN EN 15664-1:2014-03 EN 15664-1:2008+A1:2013 (E) 5 Introducti

30、on The main application of metallic materials in water supply is within the domestic installation. The test method given in this standard is designed to provide information on metal release over time from metallic materials into drinking water. The test is based on a programme of alternating periods

31、 of once-through flow and stagnation in a rig, simulating the conditions in a domestic distribution system. The test conditions are more relevant than conditions of continuous through-flow or sit and soak tests and are applicable to all metallic materials in distribution systems. Internal corrosion

32、of metallic products in water conveying systems generally leads to the build-up of layers, which might or might not be protective. The factors influencing corrosion are described in EN 12502-1. Type and rate of the production of corrosion products and the rate of metal release can depend on: charact

33、eristics of the metallic material; characteristics of the water; design and construction; pressure testing and commissioning; operating conditions and duration of operation. Corrosion product layers begin to form as soon as a metallic material comes into contact with water. Their properties depend o

34、n the factors noted above and for a given water/material combination especially on the operating conditions. It is not possible to reproduce the conditions of an actual installation in tests by constant once-through flow or circulation of water. The flow regime (3.16) used in this test simulates the

35、 operating conditions in domestic drinking water installations where stagnation times of water considerably exceed the times of through-flow. An assessment by testing is possible only if the influence of the flow regime (3.16) and the operation period (3.19) is taken into consideration. A compilatio

36、n of data are needed, which has been determined under defined conditions over a prolonged period of time. In most cases, metal release decreases with operation time. For some alloying elements and impurities, however, an increase in their release can be observed. DIN EN 15664-1:2014-03 EN 15664-1:20

37、08+A1:2013 (E) 6 1 Scope This European Standard specifies a procedure to determine the release of metals from metallic materials used in construction products intended to come into contact with drinking water1). The test can be used for three purposes: a) assess a material as a reference material fo

38、r a category of materials using the results of several investigations in different waters covering a broad range of water compositions; b) assess a material for approval by way of comparative testing; c) obtain data on the interaction of local water with a material. 2 Normative references The follow

39、ing documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 1484, Water an

40、alysis Guidelines for the determination of total organic carbon (TOC) and dissolved organic carbon (DOC) EN 10088-1, Stainless steels Part 1: List of stainless steels EN 12502-1:2004, Protection of metallic materials against corrosion Guidance on the assessment of corrosion likelihood in water distr

41、ibution and storage systems Part 1: General EN 25813, Water quality - Determination of dissolved oxygen Iodometric method (ISO 5813:1983) EN 25814, Water quality Determination of dissolved oxygen Electrotechnical probe method (ISO 5814:1990) EN 27888, Water quality Determination of electrical conduc

42、tivity (ISO 7888:1985) EN ISO 6878, Water quality Determination of phosphorus Ammonium molybdate spectrometric method (ISO 6878:2004) EN ISO 8044:1999, Corrosion of metals and alloys Basic terms and definitions (ISO 8044:1999) EN ISO 9963 (all parts), Water quality Determination of alkalinity (ISO 9

43、963, all parts) EN ISO 10304-1, Water quality Determination of dissolved fluoride, chloride, nitrite, orthophosphate, bromide, nitrate and sulphate ions, using liquid chromatography of ions Part 1: Method for water with low contamination (ISO 10304-1:1992) EN ISO 11885, Water quality Determination o

44、f 33 elements by inductively coupled plasma atomic emission spectroscopy (ISO 11885:1996) 1) Water intended for human consumption is referred to as “drinking water“ and means the same as the definition given at Article 2(1) of the Council Directive 98/83/EC on the quality of water intended for human

45、 consumption. Luxembourg, Office for Official Publications of the European Communities. 3 November 1998. DIN EN 15664-1:2014-03 EN 15664-1:2008+A1:2013 (E) 7 EN ISO 14911, Water quality Determination of dissolved Li+, Na+, NH4+, K+, Mn2+, Ca2+, Mg2+, Sr2+ and Ba2+ using ion chromatography Method for

46、 water and waste water (ISO 14911:1998) EN ISO 15586, Water quality Determination of trace elements using atomic absorption spectrometry with graphite furnace (ISO 15586:2003) EN ISO 17294 (all parts), Water quality Application of inductively coupled plasma mass spectrometry (ICP-MS) (ISO 17294, all

47、 parts) ISO 6058, Water quality Determination of calcium content EDTA titrimetric method ISO 6059, Water quality Determination of the sum of calcium and magnesium EDTA titrimetric method ISO 9297, Water quality Determination of chloride Silver nitrate titration with chromate indicator (Mohrs method)

48、 ISO 9964-3, Water quality Determination of sodium and potassium Part 3: Determination of sodium and potassium by flame emission spectrometry ISO 10523, Water quality Determination of pH 3 Terms and definitions For the purposes of this document, the terms and definitions given in EN ISO 8044:1999, E

49、N 12502-1:2004 and the following apply. 3.1 test rig assembly of test lines, control lines and where necessary reference lines together with test water inlet and discharge arrangements, see Annex A, Figure A.1 3.2 line continuous part between a check valve and the corresponding flow regulator 3.3 control line line containing a single length of pipe made of an inert material for the purposes of the test 3.4 test line line containing test pieces or a test pipe 3.