DIN EN 12697-11-2012 Bituminous mixtures - Test methods for hot mix asphalt - Part 11 Determination of the affinity between aggregate and bitumen German version EN 12697-11 2012《沥青.pdf

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1、-XO7UDQVODWLRQE,16SUDFKHQGLHQVW(QJOLVKSULFHJURXS1RSDUWRIWKLVWUDQVODWLRQPDEHUHSURGXFHGZLWKRXWSULRUSHUPLVVLRQRI,1HXWVFKHV,QVWLWXWIU1RUPXQJH9%HUOLQ%HXWK9HUODJ*PE+%HUOLQ*HUPDQKDVWKHHFOXVLYHULJKWRIVDOHIRU*HUPDQ6WDQGDUGV ,11RUPHQ , b) 5.1.12: a requirement for the horizontal positioning of the rolling mac

2、hine has been added; c) 5.2.2.1: a reference to EN 58 has been added for sampling; d) 6.1.1: “Shallow tray(s)” has been changed to “Flat bottomed container”; e) 6.3.1 and 6.3.2: The original text for preparation of aggregate and bitumen has been changed to a reference to similar clauses in the rolli

3、ng bottle method; f) 6.4.1: Now the use of 8-11,2 mm fraction is allowed as an alternative, and the definition of mixing temperature has been changed from (130 5)C to 15C less than the mixing temperature defined in EN 12697-35; g) 6.6: In the report, a new list entry b) (sample identification number

4、 and date and time of testing) has been added; h) 7.2.1: the requirements for test sieves have been changed to a reference to 5.2.1 (previously specified sieves 7 and 14 mm have been deleted); i) 7.5.1.1., 7.5.1.2, 7.6.1.1, and 7.6.2.1: the symbol “r” previously used for the acid/base equivalent fac

5、tor has been changed to “feq” to avoid any misunderstandings, as “r” is also used for repeatability; j) 7.3.3.4: the use of (8-11,2) mm aggregates has been added; k) informative Annex A has been added. Previous editions DIN EN 12697-11: 2004-03, 2005-12 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE N

6、ORM EN 12697-11 April 2012 ICS 93.080.20 Supersedes EN 12697-11:2005English Version Bituminous mixtures - Test methods for hot mix asphalt - Part 11: Determination of the affinity between aggregate and bitumen Mlanges bitumineux - Mthodes dessai pour mlange hydrocarbon chaud - Partie 11: Dterminatio

7、n de laffinit granulat-bitume Asphalt - Prfverfahren fr Heiasphalt - Teil 11: Bestimmung der Affinitt von Gesteinskrnungen und Bitumen This European Standard was approved by CEN on 9 March 2012. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions

8、for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in th

9、ree official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards b

10、odies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

11、 United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 12697-1

12、1:2012: EEN 12697-11:2012 (E) 2 Contents Page Foreword 31 Scope 72 Normative references 73 Terms and definitions .74 Principle 85 Rolling bottle method 85.1 Equipment 85.2 Preparation of test specimens 115.2.1 Aggregate 115.2.2 Bitumen 125.2.3 Mixing aggregate and bitumen 125.3 Conditioning 135.4 Pr

13、ocedure 135.5 Calculation and expression of results 155.6 Report 155.7 Precision 166 Static method 166.1 Equipment . 166.2 Solvent and other materials . 176.3 Preparation of test specimens 176.3.1 Aggregate 176.3.2 Bitumen 176.4 Procedure 176.5 Calculation and expression of results 186.6 Report 186.

14、7 Precision 187 Boiling water stripping method . 187.1 General . 187.2 Equipment and materials . 197.3 Sample preparation 207.3.1 Aggregate 207.3.2 Bitumen 217.3.3 Mixing aggregate and bitumen 217.4 Conditioning 217.5 Test procedure 217.5.1 Establishing the acid/base equivalence factor 217.5.2 Estab

15、lishing the calibration curve 227.5.3 Stripping test . 237.6 Calculation and expression of results 247.6.1 Determination of the calibration curve . 247.6.2 Calculation of the degree of bitumen coverage 257.7 Test report . 267.8 Precision 26Annex A (informative) Guidance for estimation of the degree

16、of bitumen coverage 27Bibliography . 28DIN EN 12697-11:2012-07 EN 12697-11:2012 (E) 3 Foreword This document (EN 12697-11:2012) has been prepared by Technical Committee CEN/TC 227 “Road materials”, the secretariat of which is held by DIN. This European Standard shall be given the status of a nationa

17、l standard, either by publication of an identical text or by endorsement, at the latest by October 2012, and conflicting national standards shall be withdrawn at the latest by October 2012. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent

18、rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 12697-11:2005. List of main changes since this new edition: Most clauses, subclauses, etc. in the existing standard renumbered and headlines for methods A (rolling bott

19、le), B (static immersion) and C (Boiling water stripping method) deleted (which may be confusing to users of previous version of standard!); 5.1.12: Requirement to horizontally positioning of rolling machine added; 5.2.2.1: Reference to EN 58 added for sampling; 6.1.1: “Shallow trays” changed to “Fl

20、at bottomed container”; 6.3.1 and 6.3.2: Original text for preparation of aggregate and bitumen changed to reference to similar clauses in the rolling bottle method; 6.4.1: Now allowing use of 8-11,2 mm fraction alternatively, and definition of mixing temperature changed from 130 C 5 C to 15C less t

21、han the mixing temperature defined in EN 12697-35; 6.6: In report, new list entry b) (sample identification number and date and time of testing, is added; 7.2.1: Requirements for test sieves changed to reference to 5.2.1 (previously specified sieves 7 and 14 mm deleted); 7.5.1.1., 7.5.1.2, 7.6.1.1,

22、and 7.6.2.1: the symbol “r” previously used for acid/base equivalent factor is changed to “feq” to avoid misunderstanding as “r” is also used for repeatability (change introduced with the latest comments); 7.3.3.4: Use of (8-11,2) mm aggregates added; Informative Annex A added. This European Standar

23、d is one of a series of standards as listed below: EN 12697-1, Bituminous mixtures Test methods for hot mix asphalt Part 1: Soluble binder content EN 12697-2, Bituminous mixtures Test method for hot mix asphalt Part 2: Determination of particle size distribution EN 12697-3, Bituminous mixtures Test

24、methods for hot mix asphalt Part 3: Binder recovery: Rotary evaporator DIN EN 12697-11:2012-07 EN 12697-11:2012 (E) 4 EN 12697-4, Bituminous mixtures Test methods for hot mix asphalt Part 4: Bitumen recovery: Fractionating column EN 12697-5, Bituminous mixtures Test methods for hot mix asphalt Part

25、5: Determination of the maximum density EN 12697-6, Bituminous mixtures Test methods for hot mix asphalt Part 6: Determination of bulk density of bituminous specimen EN 12697-7, Bituminous mixtures Test methods for hot mix asphalt Part 7: Determination of bulk density of bituminous specimens by gamm

26、a rays EN 12697-8, Bituminous mixtures Test methods for hot mix asphalt Part 8: Determination of void characteristics of bituminous specimens EN 12697-10, Bituminous mixtures Test methods for hot mix asphalt Part 10: Compactability EN 12697-11, Bituminous mixtures Test methods for hot mix asphalt Pa

27、rt 11: Determination of the affinity between aggregates and bitumen EN 12697-12, Bituminous mixtures Test methods for hot mix asphalt Part 12: Determination of the water sensitivity of bituminous specimens EN 12697-13, Bituminous mixtures Test methods for hot mix asphalt Part 13: Temperature measure

28、ment EN 12697-14, Bituminous mixtures Test methods for hot mix asphalt Part 14: Water content EN 12697-15, Bituminous mixtures Test methods for hot mix asphalt Part 15: Determination of the segregation sensitivity EN 12697-16, Bituminous mixtures Test methods for hot mix asphalt Part 16: Abrasion by

29、 studded tyres EN 12697-17, Bituminous mixtures Test methods for hot mix asphalt Part 17: Particle loss of porous asphalt specimen EN 12697-18, Bituminous mixtures Test methods for hot mix asphalt Part 18: Binder drainage EN 12697-19, Bituminous mixtures Test methods for hot mix asphalt Part 19: Per

30、meability of specimen EN 12697-20, Bituminous mixtures Test methods for hot mix asphalt Part 20: Indentation using cube or cylindrical specimens (CY) EN 12697-21, Bituminous mixtures Test methods for hot mix asphalt Part 21: Indentation using plate specimens EN 12697-22, Bituminous mixtures Test met

31、hods for hot mix asphalt Part 22: Wheel tracking EN 12697-23, Bituminous mixtures Test methods for hot mix asphalt Part 23: Determination of the indirect tensile strength of bituminous specimens EN 12697-24, Bituminous mixtures Test methods for hot mix asphalt Part 24: Resistance to fatigue EN 12697

32、-25, Bituminous mixtures Test methods for hot mix asphalt Part 25: Cyclic compression test DIN EN 12697-11:2012-07 EN 12697-11:2012 (E) 5 EN 12697-26, Bituminous mixtures Test methods for hot mix asphalt Part 26: Stiffness EN 12697-27, Bituminous mixtures Test methods for hot mix asphalt Part 27: Sa

33、mpling EN 12697-28, Bituminous mixtures Test methods for hot mix asphalt Part 28: Preparation of samples for determining binder content, water content and grading EN 12697-29, Bituminous mixtures Test methods for hot mix asphalt Part 29: Determination of the dimensions of a bituminous specimen EN 12

34、697-30, Bituminous mixtures Test methods for hot mix asphalt Part 30: Specimen preparation by impact compactor EN 12697-31, Bituminous mixtures Test methods for hot mix asphalt Part 31: Specimen preparation by gyratory compactor EN 12697-32, Bituminous mixtures Test methods for hot mix asphalt Part

35、32: Laboratory compaction of bituminous mixtures by a vibratory compactor EN 12697-33, Bituminous mixtures Test methods for hot mix asphalt Part 33: Specimen prepared by roller compactor EN 12697-34, Bituminous mixtures Test methods for hot mix asphalt Part 34: Marshall test EN 12697-35, Bituminous

36、mixtures Test methods for hot mix asphalt Part 35: Laboratory mixing EN 12697-36, Bituminous mixtures Test methods for hot mix asphalt Part 36: Determination of the thickness of a bituminous pavement EN 12697-37, Bituminous mixtures Test methods for hot mix asphalt Part 37: Hot sand test for the adh

37、esivity of binder on precoated chippings for HRA EN 12697-38, Bituminous mixtures Test methods for hot mix asphalt Part 38: Common equipment and calibration EN 12697-39, Bituminous mixtures Test methods for hot mix asphalt Part 39: Binder content by ignition EN 12697-40, Bituminous mixtures Test met

38、hods for hot mix asphalt Part 40: In situ drainability EN 12697-41, Bituminous mixtures Test methods for hot mix asphalt Part 41: Resistance to de-icing fluids EN 12697-42, Bituminous mixtures Test methods for hot mix asphalt Part 42: Amount of coarse foreign matter in reclaimed asphalt EN 12697-43,

39、 Bituminous mixtures Test methods for hot mix asphalt Part 43: Resistance to fuel EN 12697-44, Bituminous mixtures Test methods for hot mix asphalt Part 44: Crack propagation by semi-circular bending test FprEN 12697-45, Bituminous mixtures Test methods for hot mix asphalt Part 45: Saturation Ageing

40、 Tensile Stiffness (SATS) conditioning test FprEN 12697-46, Bituminous mixtures Test methods for hot mix asphalt Part 46: Low temperature cracking and properties by uniaxial tension tests DIN EN 12697-11:2012-07 EN 12697-11:2012 (E) 6 EN 12697-47, Bituminous mixtures Test methods for hot mix asphalt

41、 Part 47: Determination of the ash content of natural asphalts prEN 12697-49, Bituminous mixtures Test methods for hot mix asphalt Part 49: Determination of friction after polishing According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are

42、 bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spa

43、in, Sweden, Switzerland, Turkey and the United Kingdom. DIN EN 12697-11:2012-07 EN 12697-11:2012 (E) 7 1 Scope This European Standard specifies procedures for the determination of the affinity between aggregate and bitumen and its influence on the susceptibility of the combination to stripping. This

44、 property is intended to be of assistance to the designer for mixture design rather than as a type test. Susceptibility to stripping, as determined by these procedures, is an indirect measure of the power of a binder to adhere to various aggregates, or of various binders to adhere to a given aggrega

45、te. The procedures can also be used to evaluate the effect of moisture on a given aggregate-binder combination with or without adhesion agents including liquids, such as amines, and fillers, such as hydrated lime or cement. In the rolling bottle method, the affinity is expressed by visual registrati

46、on of the degree of bitumen coverage on uncompacted bitumen-coated mineral aggregate particles after influence of mechanical stirring action in the presence of water. NOTE 1 The rolling bottle test is a simple but subjective test and suitable for routine testing. It is not appropriate for aggregates

47、 that are highly abrasive. In the static test method, the affinity is expressed by visual registration of the degree of bitumen coverage on uncompacted bitumen-coated mineral aggregate particles after storage in water. NOTE 2 The static test is a simple, though subjective test that is generally less precise, but that can cope with high PSV-aggregates. In the boiling water stripping test method,