BS EN 14415-2004 Geosynthetic barriers Test method for determining the resistance to leaching《土工合成物隔层 耐浸出性测定的试验方法》.pdf

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1、BRITISH STANDARD BS EN 14415:2004 Geosynthetic barriers Test method for determining the resistance to leaching The European Standard EN 14415:2004 has the status of a British Standard ICS 59.080.70 BS EN 14415:2004 This British Standard was published under the authority of the Standards Policy and S

2、trategy Committee on 26 May 2004 BSI 26 May 2004 ISBN 0 580 43817 1 National foreword This British Standard is the official English language version of EN 14415:2004. The UK participation in its preparation was entrusted to Technical Committee B/553, Geosynthetics, which has the responsibility to: A

3、 list of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BSI Catalogue under the section entitled “International Sta

4、ndards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standa

5、rd does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; monitor related international and European

6、 developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN title page, pages 2 to 10, an inside back cover and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendm

7、ents issued since publication Amd. No. Date CommentsEUROPEANSTANDARD NORMEEUROPENNE EUROPISCHENORM EN14415 May2004 ICS59.080.70 Englishversion GeosyntheticbarriersTestmethodfordeterminingthe resistancetoleaching BarriresgosynthtiquesMthodedessaipourla dterminationdelarsistancelalixiviation Geosynthe

8、tischeDichtungsbahnenPrfverfahrenzur BestimmungderBestndigkeitgegenAuslaugen ThisEuropeanStandardwasapprovedbyCENon2February2004. CENmembersareboundtocomplywiththeCEN/CENELECInternalRegulationswhichstipulatetheconditionsforgivingthisEurope an Standardthestatusofanationalstandardwithoutanyalteration.

9、Uptodatelistsandbibliographicalreferencesconcernings uchnational standardsmaybeobtainedonapplicationtotheCentralSecretariatortoanyCENmember. ThisEuropeanStandardexistsinthreeofficialversions(English,French,German).Aversioninanyotherlanguagemadebytra nslation undertheresponsibilityofaCENmemberintoits

10、ownlanguageandnotifiedtotheCentralSecretariathasthesamestatusast heofficial versions. CENmembersarethenationalstandardsbodiesofAustria,Belgium,Cyprus,CzechRepublic,Denmark,Estonia,Finland,France, Germany,Greece,Hungary,Iceland,Ireland,Italy,Latvia,Lithuania,Luxembourg,Malta,Netherlands,Norway,Poland

11、,Portugal, Slovakia, Slovenia,Spain,Sweden,SwitzerlandandUnitedKingdom. EUROPEANCOMMITTEEFORSTANDARDIZATION COMITEUROPENDENORMALISATION EUROPISCHESKOMITEEFRNORMUNG ManagementCentre:ruedeStassart,36B1050Brussels 2004CEN Allrightsofexploitationinanyformandbyanymeansreserved worldwideforCENnationalMemb

12、ers. Ref.No.EN14415:2004:EEN14415:2004(E) 2 Contents page Foreword3 Introduction .4 1 Scope 5 2 NormativeReferences .5 3 TermsandDefinitions. 5 4 Principle5 5 Reagents.5 6 Apparatus.6 6.1 Analyticalbalance .6 6.2 Conditionedroom 6 6.3 Liquidbath. 6 6.4 Dryingchamber .6 6.5 Desiccator .6 7 Sampling.6

13、 7.1 Geosyntheticclaybarriers .6 7.2 Polymericandbituminousgeosyntheticbarriers 6 8 Procedure.6 8.1 Methods.6 8.2 Testconditions . .7 8.3 Determinationofthedrymassbeforetesting .7 8.4 Procedureforcontrolspecimens . .7 8.4.1 Conditioning 7 8.4.2 Geosyntheticclaybarriers 7 8.4.3 Polymericandbituminous

14、geosyntheticbarriers 7 8.5 Procedurefortestspecimens .7 8.5.1 Immersioninliquid. .7 8.5.2 Inspectionandtesting .8 9 Evaluation.8 9.1 Massdifference. 8 9.2 Mechanicalproperties . 8 9.2.1 Geosyntheticclaybarriers 8 9.2.2 Polymericandbituminousgeosyntheticbarriers 8 10 Testreport 8 Bibliography 10EN144

15、15:2004(E) 3 Foreword Thisdocument(EN14415:2004)hasbeenpreparedbyTechnicalCommitteeCEN/TC189,“Geosynthetics“,the secretariatofwhichisheldbyIBN. ThisEuropeanStandardshallbegiventhestatusofanationalstandard,eitherbypublicationofanidenticaltextor byendorsement,atthelatestbyNovember2004,andconflictingna

16、tionalstandardsshallbewithdrawnatthelatest byNovember2004. ThisdocumentincludesaBibliography. AccordingtotheCEN/CENELECInternalRegulations,thenationalstandardsorganizationsofthefollowing countriesareboundtoimplementthisEuropeanStandard:Austria,Belgium,Cyprus,CzechRepublic,Denmark, Estonia,Finland,Fr

17、ance,Germany,Greece,Hungary,Iceland,Ireland,Italy,Latvia,Lithuania,Luxembourg,Malta, Netherlands,Norway,Poland,Portugal,Slovakia,Slovenia,Spain,Sweden,SwitzerlandandUnitedKingdom.EN14415:2004(E) 4 Introduction ThisEuropeanStandarddefinesamethodfortestingthebehaviourgeosyntheticbarriersinhotwater,aqu

18、eous alkalineliquidsandorganicalcohols,withrespecttoleaching,visiblechanges,andtensileproperties.Leachingof stabilizerscanacceleratetheoxidationofthegeosyntheticbarrier. Thestandarddoesnotpurporttoaddressallofthesafetyproblems,ifany,associatedwithitsuse.EN14415:2004(E) 5 1Scope ThisEuropeanStandardd

19、escribesamethodoftestingtheresistancetoleachingofpolymericorbituminous geosyntheticbarriers,andthepolymericcomponentofgeosyntheticclaybarriers,inhotwater(methodA),aqueous alkalineliquids(methodB)andorganicalcohols(methodC). 2 NormativeReferences ThisEuropeanStandardincorporates,bydatedorundatedrefer

20、ence,provisionsfromotherpublications.These normativereferencesarecitedattheappropriateplacesinthetextandthepublicationsarelistedhereafter.For datedreferences,subsequentamendmentstoorrevisionsofanyofthesepublicationsapplytothisEuropean Standardonlywhenincorporatedinitbyamendmentorrevision.Forundatedr

21、eferencesthelatesteditionofthe publicationreferredtoapplies(includingamendments). ENISO291 PlasticsStandardatmospheresforconditioningandtesting(ISO291:1997) ENISO5271 PlasticsDeterminationoftensilepropertiesPart1:Generalprinciples(ISO5271:1993 includingCorr1:1994) ENISO5273 PlasticsDeterminationofte

22、nsilepropertiesPart3:Testconditionsforfilmsandsheets (ISO5273:1995) prENISO10318:2000 GeosyntheticsGeotextiles,geotextilerelatedproducts,geomembranesand geosyntheticclaylinersTermsandtheirdefinitions(ISO/DIS10318:2000) EN12226:2000 GeotextilesandgeotextilerelatedproductsGeneraltestsforevaluationfoll

23、owing durabilitytesting EN14030 GeotextilesandgeotextilerelatedproductsScreeningtestmethodfordeterminingthe resistancetoacidandalkalineliquids(ISO/TR12960:1998,modified) 3 TermsandDefinitions ForthepurposesofthisEuropeanStandard,thetermsanddefinitionsgiveninprENISO10318:2000apply. 4Principle Asample

24、ofgeosyntheticbarrierisplacedinthetestliquidfor56days.Subsequentlythesampleisrecoveredfrom theliquidandchangesinproperties(masschange,mechanicalandvisible)aremeasuredinaccordancewithEN ISO527. 5Reagents Followingreagentsareused: Distilledordeionizedwater; SaturatedCa(OH) 2 inaccordancewithEN14030; A

25、mixtureof: 30volume%methanol; 30volume%2propanol(isopropanol); 40volume%1,2ethanediol(glycol).EN14415:2004(E) 6 6Apparatus 6.1 Analyticalbalance Abalancewithaminimummeasurementrangeof200gandaprecisionofatleast0,01g. 6.2Conditioned room Aroomwithanatmospherecontrolledtoatemperatureof(202)Candarelativ

26、ehumidityof(655)% accordingtoENISO291. 6.3Liquid bath Arecipientwithavolumeofatleastonelitrepersample,comprising: anexposuretankmadeofinert,noncorrosivematerial,impermeabletothesolutionbeingused; acovertopreventtheintrusionoflight; astirringdevicetomaintainthehomogeneityofsolvent,solutesandtemperatu

27、re; asystemformaintainingtheliquidat(502)C;andcapableofbeingsealedwithachemicallyresistant materialinordertopreventlossofvolatilecomponentsofinterest. Unlessotherwisespecified,agreedupon,orrequired,provisionsshallbemadeformaintainingambient atmosphericpressureinthetank. 6.4Drying chamber Achamberwit

28、hcirculatingairof(502)Cfordryingthesamples. 6.5Desiccator Adesiccatoranddesiccatingagents(silicagelorcalciumchloride). 7Sampling 7.1 Geosyntheticclaybarriers SamplingofgeosyntheticclaybarriersshallbedoneinaccordancewithEN12226.Thebentoniteshallberemoved fromthegeosyntheticclaybarrierwiththeaidofcomp

29、ressedair,bywashing,orbyanyotherappropriatemethod. Takeonegroupoftestspecimensandonegroupofcontrolspecimens. 7.2 Polymericandbituminousgeosyntheticbarriers Aminimumofthreesamplesofpolymericandbituminousgeosyntheticbarrier(200mm200mm)shallbetaken. Takeonegroupoftestsamplesandonegroupofcontrolsamples.

30、SpecimensfortensiletestingtoENISO5273 shallbecutafterexposure. 8Procedure 8.1Methods Thistestcanbeperformedusingthreedifferentleachingenvironments: MethodA:leachingbyhotwater;EN14415:2004(E) 7 MethodB:leachingbyaqueousalkalineliquids; MethodC:leachingbyorganicalcohols. 8.2Test conditions Thetestshal

31、lbeperformedinaroomwithacontrolledatmosphere,accordingtoENISO291:atemperatureof(20 2)Candarelativehumidityof(655)%. 8.3 Determinationofthedrymassbeforetesting Storethesamplesfor24hinthedryingchamberatatemperatureof(502)C.Subsequentlycoolthesamplesin thedesiccatorforatleast24horuntiltheyattainthetemp

32、eratureoftheconditioningroom. Immediatelyafterremovingthesamplesfromthedesiccator,determinethemass(M 1 )ofthesampleswitha precisionof0,01g. 8.4 Procedureforcontrolspecimens 8.4.1Conditioning Thecontrolspecimensshallbeconditionedinaccordancewith8.2andshallbetestedatthesametimeasthe immersedspecimenst

33、oavoidageingofthespecimens(inparticularforbituminousmaterials). 8.4.2 Geosyntheticclaybarriers MeasurethetensilestrengthandelongationatbreakofthecontrolspecimensinaccordancewithEN12226,but withelongationatbreakreplacingstrainatmaximumload(seeEN12226:2000,6.2). 8.4.3 Polymericandbituminousgeosyntheti

34、cbarriers PreparespecimensinaccordancewithENISO5273(specimentype5)andmeasuretheelongationatbreakin accordancewithENISO5271.Determinethemeanelongationatbreak. 8.5 Procedurefortestspecimens 8.5.1 Immersioninliquid Weighthesamplesandplacethemimmediatelyintheholdersuchthateachsampleshallbeseparatedbyatl

35、east 10mmfromallothersamplesandfromthetankwall.Addtheliquidandensurethatitcoversthesamples completely.Ballastthesamplesifnecessarytopreventthemfromfloating.Onlysamplesbasedonthesame materialshallbeplacedinthesameliquidbath. Keepthetesttemperatureoftheliquid(methodA,methodBandmethodC)constantat(502)C

36、.Renewthe volumeoftheliquidcompletelyatleastevery12to14days.Renewalshallbedonewithin30min.Duringthewhole test,thetestliquidshallbestirredcontinuously. After56daysimmersionremovethesamplesfromthebath,rinsethemwithdeionizedwater.Subsequently,place thesamplesinthedryingchamberwithcirculatingairatatempe

37、ratureof(502)C. After24hofdrying,coolthesamplesandweighthemforthefirsttime.Next,placethesamplesintheconditioning roomfor24h,coolthemandweighthemforthesecondtime.Ifthemassofthesampledeterminedthesecond time,deviatesbylessthan0,20%fromthemassdeterminedthefirsttime,proceedtovisualinspectionand measurem

38、entofstrength(see8.6).Ifnot,placethesampleinthedryingroomforafurther24h,coolandweighit againuntilthedifferencebetweenthelasttwodryingstepsislessthan0,20%.ThismassisdenotedM 2 . Thesamplesshallnotbeplacedinthedryingroomformorethan96h.Ifafter96h,themassofthesampleshas notreachedaconstantvalue,thelastm

39、assofthesamplesshallbeincludedinthetestreport.EN14415:2004(E) 8 8.5.2 Inspectionandtesting 8.5.2.1 Geosyntheticclaybarriers Inspectthespecimensvisuallyandreporteveryevidenceofdegradation. MeasuretheelongationatbreakofthegeotextilecomponentofgeosyntheticclaybarriersinaccordancewithEN 12226. 8.5.2.2 P

40、olymericandbituminousgeosyntheticbarriers Inspectthespecimensvisuallyandreporteveryevidenceofdegradation. PreparespecimensofgeosyntheticbarriersinaccordancewithENISO5273(specimentype5).Measurethe elongationatbreakinaccordancewithENISO5271.Determinethemeanelongationatbreak. 9Evaluation 9.1Mass differ

41、ence DeterminethedifferencebetweenM 2 andM 1 andexpressitasapercentageofM 1 ,forallofthesamplesandafter 56daysofimmersioninwater. 9.2 Mechanicalproperties 9.2.1 Geosyntheticclaybarriers ExpresstheresultsaccordingtoEN12226,butwithelongationatbreakreplacingstrainatmaximumload. 9.2.2 Polymericandbitumi

42、nousgeosyntheticbarriers Determinetheratioofthemeanelongationatbreakoftheexposedspecimens(see8.5.2.2)tothatofthecontrol specimens(see8.4.3).Expressthisratioasapercentage. NOTE Inordertoassesspossibleleachingofstabilizersthespecimenscanbesubjectedtoanoxidationtestaccordingto ENVISO13438,followedbythe

43、determinationofthetensilestrengthandelongationatbreakaccordingtoENISO5271. 10 Testreport Thetestreportshallincludethefollowinginformation: a) referencetothisstandardandtothemethodused; b) identificationofthetestlaboratory; c) identificationoftheproducttested; d) number,sizeanddirection(transverseormachine)ofspecimens; e) testtemperature; f) testduration; g)apparatusused; h) durationofdryingbeforeaconstantmasswasobtained;EN14415:2004(E) 9 i) observedresults,measurem