BS 3762-0-1991 Analysis of formulated detergents - General introduction《配制洗涤剂分析 第0部分 总则》.pdf

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1、BRITISH STANDARD BS3762-0: 1991 Analysis of formulated detergents Part0: General introductionBS3762-0:1991 This British Standard, having been prepared under the directionof the Chemicals Standards Policy Committee, waspublished under the authorityof the Standards Boardand comes into effect on 31May1

2、991 BSI 10-1999 First published December1983 First revision November1986 Second revision February1989 Third revision May1991 The following BSI references relate to the work on this standard: Committee reference CIC/34 Draft (reference90/57708) announced in BSI News February1991 ISBN 0 580 19555 4 Co

3、mmittees responsible for this British Standard The preparation of this British Standard was entrusted by the Chemicals Standards Policy Committee (CIC/-) to Technical Committee CIC/34, upon which the following bodies were represented: Chemical Industries Association Chemical Industries Association (

4、GOSIP) Department of Trade and Industry (Laboratory of the Government Chemist) Ministry of Defence Royal Society of Chemistry Soap and Detergent Industry Association Society of Dyers and Colourists Amendments issued since publication Amd. No. Date CommentsBS3762-0:1991 BSI 10-1999 i Contents Page Co

5、mmittees responsible Inside front cover Foreword ii 1 Scope 1 2 Reagents 1 3 Other methods 1 Table 1 Methods of analysis for formulated detergents: structure and relationship between BS3762 and International Standards 2 Publication(s) referred to Inside back coverBS3762-0:1991 ii BSI 10-1999 Forewor

6、d This Part of BS3762 has been prepared under the direction of the Chemicals Standards Policy Committee and supersedes BS3762-0:1989, which is withdrawn. BS3762 provides a series of analytical methods for formulated detergents, i.e.products ready for use (possibly after dilution) in solid, paste or

7、liquid form. The revised BS3762 is published in five Parts, the analytical methods in Parts3 and4 being published separately as Sections. The Parts together supersede BS3762:1964, which is withdrawn, and from which they differ in the following ways. a) Methods of analysis of detergent raw materials

8、are not included as they are published in BS6829 “Analysis of surface active agents (raw materials)”. b) Analytical methods applicable to all washing powders (including soap powders) are included. The test methods in BS1715 apply only to soap. c) The schematic examination of active matter has been w

9、ithdrawn. d) Certain physical and performance tests have been omitted. In preparing this revision of BS3762, the opportunity has been taken, if appropriate, to implement, preferably without alteration, International Standards describing test methods for surface active agents. These have been prepare

10、d, with the active participation of the UK, by Technical Committee91, Surface active agents, of the International Organization for Standardization (ISO). In this Part of BS3762, Table 1 gives the Parts and Sections of the standard and the analytical methods included therein and, where appropriate, t

11、heir relationships to the corresponding International Standards. The range of analytical methods, although wide, is not exhaustive and it is intended that work should continue with the object of improving existing test methods and preparing others for publication as further Sections of BS3762. BS376

12、2 does not include methods of sampling detergents from bulk. Guidance in this respect is given, however, in BS5309-1, BS5309-3 and BS5309-4. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct applica

13、tion. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, pagesi andii, pages1 and2, an inside back cover and a back cover. This standard has been updated (see copyright date) and

14、 may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover.BS3762-0:1991 BSI 10-1999 1 1 Scope This Part of BS3762 outlines, in Table 1, the structure of BS3762 and gives guidance on its use. NOTEThe titles of the publications referred to in this P

15、art are listed on the inside back cover. 2 Reagents During the analyses, unless otherwise stated, use only reagents of recognized analytical grade and water complying with grade3 of BS3978. 3 Other methods In addition to the methods given in Table 1, other British Standards appropriate for the analy

16、sis of formulated detergents include BS1647-1, BS1796 and BS3900-A11. BS3762-0:1991 2 BSI 10-1999 Table 1 Methods of analysis for formulated detergents: structure and relationship between BS3762 and International Standards BS3762 Subject Corresponding International Standard no. Relationship of Inter

17、national Standard to BS test method Part no. and title Section no. 0. General introduction Introduction 1. Methods of sample division Sample division 607 Identical 2. Qualitative test method Type of surface active agent Oxidizing agents Peroxy-compounds Urea Fluorescent whitening agents 3. Quantitat

18、ive test methods 3.1 3.2 3.3 3.4 3.5 3.6 3.7 3.8 3.9 3.10 3.11 3.12 3.13 3.14 3.15 3.16 3.17 3.18 3.19 3.20 3.21 3.22 3.23 3.24 3.25 3.26 Anionic-active matter content Hydrolyzable and non-hydrolyzable anionic-active matter content after alkaline hydrolysis Hydrolyzable and non-hydrolyzable anionic-

19、active matter content after acid hydrolysis Lower molecular mass cationic-active matter content Total organic matter content Matter soluble in light petroleum Total non-ionic matter content Alkanolamides content Soap content Short chain alkylbenzenesulphonates content Free formaldehyde content Ammon

20、ia content Total boron content Carbonate content Carboxymethylcellulose content Chloride content Active oxygen content Chlorine oxidizing agents content Total phosphorus(V) oxide content Phosphate types Total silica content Inorganic sulphate content Chelating agents content Low molecular mass alcoh

21、ols content Water and volatile matter content High molecular mass cationic-active matter content 2271 2869 2870 2871-2 6835 4321 4313 8215 8214 4325 4317, 4318 ISO2871-1 Identical Identical Identical Identical Identical Identical Identical Identical Identical Identical Related Identical 4. Physical

22、test methods 4.1 4.2 Clear point of liquid detergents Apparent bulk density 697 IdenticalBS3762-0:1991 BSI 10-1999 Publication(s) referred to BS1647, pH measurement. BS1647-1, Specification for pH scale. BS1715, Analysis of soaps 1) . BS1796, Test sieving. BS3900, Methods of test for paints. BS3900-

23、A11, Small scale test for combustibility. BS3978, Specification for water for laboratory use. BS5309, Methods for sampling chemical products. BS5309-1, Introduction and general principles 1) . BS5309-3, Sampling of liquids 1) . BS5309-4, Sampling of solids 1) . BS6829, Analysis of surface active age

24、nts (raw materials) 1) . ISO607, Surface active agents and detergents Methods of sample division. ISO697, Surface active agents Washing powders Determination of apparent density Method by measuring the mass of a given volume. ISO2271, Surface active agents Detergents determination of anionic-active

25、matter by manual or mechanical direct two-phase titration procedure. ISO2869, Surface active agents Detergents Anionic-active matter hydrolyzable under alkaline conditions Determination of hydrolyzable and non-hydrolyzable anionic-active matter. ISO2870, Surface active agents Detergents Determinatio

26、n of anionic-active matter hydrolyzable and non-hydrolyzable under acid conditions. ISO2871-1, Surface active agents Detergents Determination of cationic-active matter content. ISO2871-1, High-molecular-mass cationic-active matter. ISO2871-2, Surface active agents Detergents Determination of cationi

27、c-active matter content. ISO2871-2, Cationic-active matter of low-molecular-mass (between200 and500). ISO4313, Washing powders Determination of total phosphorus(V) oxide content Quinoline phosphomolybdate gravimetric method. ISO4317, Surface active agents Determination of water content Karl Fischer

28、method. ISO4318, Surface active agents and soaps Determination of water content Azeotropic distillation method. ISO4321, Washing powders Determination of active oxygen content Titrimetric method. ISO4325, Soaps and detergents Determination of chelating agent content Titrimetric method. ISO6835, Surf

29、ace active agents Washing powders Determination of total boron content Titrimetric method. ISO8214, Surface active agents Washing powders Determination of inorganic sulfates Gravimetric methods. ISO8215, Surface active agents Washing powders Determination of total silica content Gravimetric method.

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