BS PD IEC TS 62282-7-1-2017 Fuel cell technologies Test methods Single cell performance tests for polymer electrolyte fuel cells (PEFC)《燃料电池技术 试验方法 聚合物电解质燃料电池(PEFC)的单电池性能试.pdf

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1、Fuel cell technologies Part 7-1: Test methods Single cell performance tests for polymer electrolyte fuel cells (PEFC) PD IEC/TS 62282-7-1:2017 BSI Standards Publication WB11885_BSI_StandardCovs_2013_AW.indd 1 15/05/2013 15:06National foreword This Published Document is the UK implementation of IEC/T

2、S 62282-7- 1:2017. The UK participation in its preparation was entrusted to Technical Committee GEL/105, Fuel cell technologies. A list of organizations represented on this committee can be obtained on request to its secretary. This publication does not purport to include all the necessary provision

3、s of a contract. Users are responsible for its correct application. The British Standards Institution 2017. Published by BSI Standards Limited 2017 ISBN 978 0 580 91695 3 ICS 27.070 Compliance with a British Standard cannot confer immunity from legal obligations. This Published Document was publishe

4、d under the authority of the Standards Policy and Strategy Committee on 28 February 2017. Amendments/corrigenda issued since publication Date Text affected PUBLISHED DOCUMENT PD IEC/TS 62282-7-1:2017 IEC TS 62282-7-1 Edition 2.0 2017-01 TECHNICAL SPECIFICATION Fuel cell technologies Part 7-1: Test m

5、ethods Single cell performance tests for polymer electrolyte fuel cells (PEFC) INTERNATIONAL ELECTROTECHNICAL COMMISSION ICS 27.070 ISBN 978-2-8322-3768-7 Registered trademark of the International Electrotechnical Commission Warning! Make sure that you obtained this publication from an authorized di

6、stributor. colour inside PD IEC/TS 62282-7-1:2017 2 IEC TS 62282-7-1:2017 IEC 2017 CONTENTS FOREWORD . 7 INTRODUCTION . 9 1 Scope 10 2 Normative references 10 3 Terms and definitions 10 4 General safety considerations . 14 5 Cell components 14 5.1 General . 14 5.2 Membrane electrode assembly (MEA) .

7、 14 5.3 Gasket 14 5.4 Flow plate . 14 5.5 Current collector . 15 5.6 Clamping plate (or pressure plate) 15 5.7 Clamping hardware . 15 5.8 Temperature-control device 15 6 Cell assembly 16 6.1 Assembly procedure . 16 6.2 Cell orientation and gas connections . 16 6.3 Leak check . 16 7 Test station setu

8、p 16 7.1 Minimum equipment requirement 16 7.2 Schematic diagram . 17 7.3 Maximum variation in test station controls (inputs to test) . 18 8 Measuring instruments 18 8.1 Instrument uncertainty 18 8.2 Measuring instruments and measuring methods 18 8.2.1 General . 18 8.2.2 Voltage 18 8.2.3 Current 18 8

9、.2.4 Internal resistance (IR) 19 8.2.5 Fuel and oxidant flow rates 19 8.2.6 Fuel and oxidant temperature 19 8.2.7 Cell temperature 19 8.2.8 Fuel and oxidant pressures 19 8.2.9 Fuel and oxidant humidity 20 8.2.10 Ambient conditions 20 8.3 Measurement units . 20 9 Gas composition 21 9.1 Fuel compositi

10、on . 21 9.1.1 Hydrogen . 21 9.1.2 Reformed gases 21 9.2 Oxidant composition . 21 10 Test preparation 21 10.1 Standard test conditions . 21 10.2 Ambient conditions 22 10.3 Data sampling rate 22 PD IEC/TS 62282-7-1:2017IEC TS 62282-7-1:2017 IEC 2017 3 10.4 Repeatability and reproducibility . 22 10.5 N

11、umber of test samples 22 10.6 Leak check of gas circuit with inert or test gas 23 10.7 Initial conditioning and stable state check . 23 10.8 Shutdown 23 10.9 Reconditioning 23 11 Basic performance test methods 23 11.1 General . 23 11.2 Polarization curve tests . 24 11.2.1 General . 24 11.2.2 Polariz

12、ation curves at constant gas stoichiometries . 24 11.2.3 Polarization curves at constant flow rate 25 11.3 Steady-state test . 25 11.3.1 General . 25 11.3.2 Test methods . 25 11.4 Long-term operation test . 26 11.4.1 General . 26 11.4.2 Test method 26 11.5 Voltammetry 26 11.5.1 General . 26 11.5.2 H

13、ydrogen crossover test 27 11.5.3 Electrochemical surface area (ECA) measurement 28 11.6 Internal resistance (IR) measurement . 30 11.6.1 General . 30 11.6.2 Test methods . 31 11.7 Electrochemical impedance spectroscopy (EIS) 32 11.7.1 General . 32 11.7.2 Test conditions 32 11.7.3 Test method 32 11.7

14、.4 Analysis of EIS data 33 11.7.5 IR measurement by EIS . 33 12 Applied performance test methods . 33 13 Test report . 35 13.1 General . 35 13.2 Report items . 35 13.3 Test data description 35 13.4 Description of measurement conditions . 36 13.5 Test cell parameter description . 36 Annex A (informat

15、ive) Flow plate . 37 Annex B (informative) Cell component alignment . 39 Annex C (informative) Leak test . 40 C.1 Purpose 40 C.2 Test procedures 40 Annex D (informative) Initial conditioning . 42 Annex E (informative) Shutdown 43 Annex F (informative) Reconditioning protocols . 44 Annex G (informati

16、ve) Polarization curve test supplement 45 Annex H (normative) Applied performance tests. 47 PD IEC/TS 62282-7-1:2017 4 IEC TS 62282-7-1:2017 IEC 2017 H.1 Gain tests . 47 H.1.1 Hydrogen gain test 47 H.1.2 Oxygen gain test 47 H.2 Gas stoichiometry tests . 48 H.2.1 Fuel stoichiometry test . 48 H.2.2 Ox

17、idant stoichiometry test . 48 H.3 Temperature effect test . 49 H.3.1 General . 49 H.3.2 Test method 49 H.4 Pressure effect test . 49 H.4.1 General . 49 H.4.2 Test method 49 H.5 Humidity effect tests . 49 H.5.1 Fuel humidity effect test . 49 H.5.2 Oxidant humidity effect test 50 H.6 Limiting current

18、test 50 H.6.1 General . 50 H.6.2 Test method 50 H.7 Overload test 51 H.7.1 General . 51 H.7.2 Test method 51 H.8 Subzero storage test . 51 H.8.1 General . 51 H.8.2 Test method 51 H.9 Subzero start test . 52 H.9.1 General . 52 H.9.2 Test method 52 H.10 Membrane swelling test (humidity cycle test) 52

19、H.10.1 General . 52 H.10.2 Test conditions 53 H.10.3 Test method 53 H.11 Open circuit voltage (OCV) test . 53 H.11.1 General . 53 H.11.2 Test conditions 53 H.11.3 Test method 54 H.12 Oxygen reduction reaction (ORR) activity test . 54 H.12.1 General . 54 H.12.2 Test conditions 54 H.12.3 Test method 5

20、4 H.13 Fuel composition test 56 H.13.1 General . 56 H.13.2 Test method 56 H.14 Cycling tests . 56 H.14.1 Start/stop cycling test 56 H.14.2 Load cycling test 57 H.14.3 Potential cycle test (start/stop durability) . 57 H.14.4 Potential cycle test (load cycle durability) 58 H.15 Impurity influence test

21、s . 59 H.15.1 Influence at rated current density . 59 PD IEC/TS 62282-7-1:2017IEC TS 62282-7-1:2017 IEC 2017 5 H.15.2 Influence on polarization curves 60 H.15.3 Long-term impurity influence test . 61 Annex I (informative) Test report for polarization curve tests 62 I.1 General . 62 I.2 General infor

22、mation 62 I.2.1 General information on the test report . 62 I.2.2 General information concerning the test. 62 I.3 Introductory remarks . 62 I.4 Objective and scope of the test . 62 I.5 Description of cell components . 63 I.6 Background. 63 I.7 Description of the test setup . 64 I.8 Description of op

23、erating conditions, inputs and outputs . 64 I.9 Test procedure and results . 66 I.9.1 Description of startup and conditioning 66 I.9.2 Description of shutdown (when relevant) . 66 I.9.3 Description of measurement and results 66 I.9.4 Deviation from test procedures 67 I.10 Data post-processing 67 I.1

24、1 Conclusion and acceptance criteria . 67 Annex J (informative) Polarization curves in helox . 68 Annex K (informative) Test report for subzero start test . 69 Annex L (informative) Start/stop cycling test supplement 70 Annex M (informative) Load cycling test supplement 71 Bibliography 73 Figure 1 T

25、est station schematic diagram for single cell testing . 17 Figure 2 Typical testing flowchart . 22 Figure 3 Hydrogen crossover test 28 Figure 4 Determination of adsorption/desorption charge (q h ) . 29 Figure 5 Determination of CO desorption charge (q co ) . 30 Figure 6 Measurement of V CI31 Figure

26、7 Typical diagram of a complex impedance plot 33 Figure A.1 Design for flow plate (single-serpentine flow channel) . 38 Figure A.2 Design for flow plate (triple-serpentine flow channel) 38 Figure B.1 Single cell assembly using typical components . 39 Figure H.1 ORR activity test procedure 55 Figure

27、H.2 Example of Tafel plot 56 Figure H.3 Potential cycle test (start/stop durability) procedure 58 Figure H.4 Potential cycle test (load cycle durability) procedure . 59 Figure J.1 Illustration of losses identified by comparison of polarization curves in oxygen, helox and air 68 Figure M.1 Dynamic lo

28、ad cycling profile. 71 Figure M.2 Second dynamic load cycling profile . 71 Figure M.3 Dynamic load cycling based on road vehicle driving . 72 PD IEC/TS 62282-7-1:2017 6 IEC TS 62282-7-1:2017 IEC 2017 Table 1 Parameters and units 21 Table 2 Applied performance tests . 34 Table G.1 Current density inc

29、rements if maximum current density is known . 45 Table G.2 Current density increments if maximum current density is unknown . 46 Table I.1 Test input parameters . 65 Table I.2 Test output parameters . 66 Table I.3 Cell performance during startup and conditioning 66 Table I.4 Cell performance during

30、test . 67 Table K.1 Energy consumption, gas consumption and heat balance data during subzero startup . 69 Table K.2 Cell characteristics comparison before and after subzero testing . 69 PD IEC/TS 62282-7-1:2017IEC TS 62282-7-1:2017 IEC 2017 7 INTERNATIONAL ELECTROTECHNICAL COMMISSION _ FUEL CELL TEC

31、HNOLOGIES Part 7-1: Test methods Single cell performance tests for polymer electrolyte fuel cells (PEFC) FOREWORD 1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising all national electrotechnical committees (IEC National Committees). The

32、object of IEC is to promote international co-operation on all questions concerning standardization in the electrical and electronic fields. To this end and in addition to other activities, IEC publishes International Standards, Technical Specifications, Technical Reports, Publicly Available Specific

33、ations (PAS) and Guides (hereafter referred to as “IEC Publication(s)”). Their preparation is entrusted to technical committees; any IEC National Committee interested in the subject dealt with may participate in this preparatory work. International, governmental and non- governmental organizations l

34、iaising with the IEC also participate in this preparation. IEC collaborates closely with the International Organization for Standardization (ISO) in accordance with conditions determined by agreement between the two organizations. 2) The formal decisions or agreements of IEC on technical matters exp

35、ress, as nearly as possible, an international consensus of opinion on the relevant subjects since each technical committee has representation from all interested IEC National Committees. 3) IEC Publications have the form of recommendations for international use and are accepted by IEC National Commi

36、ttees in that sense. While all reasonable efforts are made to ensure that the technical content of IEC Publications is accurate, IEC cannot be held responsible for the way in which they are used or for any misinterpretation by any end user. 4) In order to promote international uniformity, IEC Nation

37、al Committees undertake to apply IEC Publications transparently to the maximum extent possible in their national and regional publications. Any divergence between any IEC Publication and the corresponding national or regional publication shall be clearly indicated in the latter. 5) IEC itself does n

38、ot provide any attestation of conformity. Independent certification bodies provide conformity assessment services and, in some areas, access to IEC marks of conformity. IEC is not responsible for any services carried out by independent certification bodies. 6) All users should ensure that they have

39、the latest edition of this publication. 7) No liability shall attach to IEC or its directors, employees, servants or agents including individual experts and members of its technical committees and IEC National Committees for any personal injury, property damage or other damage of any nature whatsoev

40、er, whether direct or indirect, or for costs (including legal fees) and expenses arising out of the publication, use of, or reliance upon, this IEC Publication or any other IEC Publications. 8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publicatio

41、ns is indispensable for the correct application of this publication. 9) Attention is drawn to the possibility that some of the elements of this IEC Publication may be the subject of patent rights. IEC shall not be held responsible for identifying any or all such patent rights. The main task of IEC t

42、echnical committees is to prepare International Standards. In exceptional circumstances, a technical committee may propose the publication of a Technical Specification when the required support cannot be obtained for the publication of an International Standard, despite repeated efforts, or the subj

43、ect is still under technical development or where, for any other reason, there is the future but no immediate possibility of an agreement on an International Standard. Technical Specifications are subject to review within three years of publication to decide whether they can be transformed into Inte

44、rnational Standards. IEC TS 62282-7-1, which is a Technical Specification, has been prepared by IEC technical committee 105: Fuel cell technologies. PD IEC/TS 62282-7-1:2017 8 IEC TS 62282-7-1:2017 IEC 2017 This second edition cancels and replaces the first edition published in 2010. This edition co

45、nstitutes a technical revision. This edition includes the following significant technical changes with respect to the previous edition: a) addition of new tests, mainly regarding transportation applications; and, b) restructuring of the format: basic and applied performance test methods. The text of

46、 this Technical Specification is based on the following documents: Enquiry draft Report on voting 105/568/DTS 105/621/RVC Full information on the voting for the approval of this technical specification can be found in the report on voting indicated in the above table. This document has been drafted

47、in accordance with the ISO/IEC Directives, Part 2. A list of all parts of the IEC 62282 series, published under the general title: Fuel cell technologies, can be found on the IEC website. The committee has decided that the contents of this publication will remain unchanged until the stability date i

48、ndicated on the IEC website under “http:/webstore.iec.ch“ in the data related to the specific publication. At this date, the publication will be transformed into an International standard, reconfirmed, withdrawn, replaced by a revised edition, or amended. A bilingual version of this publication may

49、be issued at a later date. IMPORTANT The colour inside logo on the cover page of this publication indicates that it contains colours which are considered to be useful for the correct understanding of its contents. Users should therefore print this document using a colour printer. PD IEC/TS 62282-7-1:2017IEC TS 62282-7-1:2017 IEC 2017 9 INTRODUCTION This part of IEC 62282 describes standard single-cell test methods for polymer electrolyte fu