DB45 T 2256-2021 重松节油中石竹烯含量的测定 气相色谱法.pdf

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1、g3 g3 g3 ICSg3g3g26g20g17 CCS g3g37g3g25 g5301 g39g72g87 g21g19g21g20 g16 g19g23g19g17g28g28g3 g19g3 g16309 g3876 g18435 g72g85g80g76g81g68g87g76 g19g21 g16 g19g24g2567 g3876g7173 g7604g14520 g82g81g3g82g73g3g70g68 g5177 g5301g16309g3876 g7173 g14368 g8943g1123 g8778 g85g92g82g83g75g92g79 g42g68g86g

2、3g70g75g85 g7173g14368g8945g2416 g8945 g3 g11817g12591 g11566g14504 g79g72g81g72g3g70g82g81 g82g80g68g87g82g74g85g68 g5176g3440g11527g11673 g2416 g10021g2657 g16999g8971 g87g72g81g87g3g76g81g3 g83g75g76g70g3g80g72g87 g12759g10812g4726 g3430 g39g37 g18437g11450g9089 g3 g75g72g68g89g92g3g87 g75g82g71g

3、3 g2567 g5177 4 g7151 g7741 g23g24g18g55g3g21g21g24 g9089g4560g3 g87g88g85g83g72g81g87g76g81 g21g19g21g20 g16 g19 g3 5g3 g7741g2044 g25g258g21g19g21g20 g3g3g3g3g3 g72g3g82g76g79g258g3 g22 g16 g19g24g4564 g2044g3 g3 g3 g7155 g39g37g23g24g18g55g3g21g21g24g25g252g21g19g21g20g3 g44g3 g11556g8535g3 g2173

4、g16432g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g44g44g44g3 g20g3g3g14643g3364g3g17g17g17g17g17g17

5、g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g20g3 g21g3g3g16372g14643g5719g5445g11096g7095g1318g3g17g17g17g17g17g17g17g17g1

6、7g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g20g3 g22g3g3g7519g16925g2748g4554g1145g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g

7、17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g20g3 g23g3g3g2511g10806g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17

8、g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g20g3 g24g3g3g16901g2162g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g1

9、7g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g20g3 g25g3g3g1306g3224g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g1

10、7g17g17g17g17g17g17g17g17g17g17g17g17g3g20g3 g26g3g3g16901g7783g20148g3892g10806g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g1

11、7g3g21g3 g27g3g3g14498g16993g2102g7616g7569g1318g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g22g3 g28g3g3g11811g12585g10015g265

12、1g18431g11444g9083g4554g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g22g3 g20g19g3g3g16849g12743g2554g13571g7628g16024g12138g3g17g17g17g17g1

13、7g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g22g3 g20g20g3g3g13038g4598g5334g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g1

14、7g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g22g3 g19572g5509g36g708g17268g7113g5719g709g3g3g8772g11560g14498g16993g3374g3g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17

15、g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g17g3g23g3 g39g37g23g24g18g55g3g21g21g24g25g252g21g19g21g20g3 g44g44g44g3 g2179g16438g3 g7516g7095g1318g6457g10135g42g37g18g55g3g20g17g20g252g21g19g21g19g457g7735g2038g2374g5141g1420g4652g2121

16、g3g3g12636g20g18200g2102g726g7735g2038g2374g7095g1318g11444g13571g7604g2748g17319g14713g16372g2121g458g11444g16372g4554 g17319g14713g452g3 g16935g8984g5951g7516g7095g1318g11444g7680g1227g1973g4585g2591g14125g9145g2554g1091g2137g452g7516g7095g1318g11444g2561g5171g7530g7604g1085g6319g6389g16886g2139g1

17、091g2137g11444g17235g1323g452g3 g7516g7095g1318g11105g2439g4529g5170g5170g3434g11521g11667g12753g10806g4720g6656g2090g5286g4563g17247g452g3 g7516g7095g1318g11105g5295g16303g3870g7167g14362g8939g2410g7598g14130g7735g2038g2374g6320g7519g4100g2696g1354g5506g2579g452g3 g7516g7095g1318g17319g14713g2437g1

18、405g726g5295g16303g3927g4502g451g7895g5134g5170g1239g2801g17240g18431g7920g20668g6256g451g5295g16303g12289g5424g6208g7623g12289g6320g7481g19584g1948g2600g451g5295g16303g7735g2038g2374g2431 g1354g451g3373g4582g7598g14130g7623g2374g1239g2801g17240g18431g11521g11667g7920g20668g1117g5619g708g5295g16303g

19、709g451g10681g7623g5170g7920g20668g7920g9083g11844g12454g19602g452g3 g7516g7095g1318g1131g16305g17319g14713g1258g726g16978g4543g7261g451g10683g10851g10851g451g7857g7584g10749g451g19576g4671g21631g451g2629g12539g11512g451g21748g7623g2430g451g15117g2012g1133g451g19990g4671g7584g451g19576g13758 g10722g

20、451g7550g7253g10245g451g5456g1117g1968g451g9608g8995g16432g451g19576g4582g17050g451g11811g7039g451g19576g4671g13522g451g16989g10337g451g14811g13872g7623g451g4495g7334g7334g451g11811g7237g3625g451g5382g5418g7584g451g19990 g12539g1912g451g19574g4019g4019g451g2120g12145g1217g452 g39g37g23g24g18g55g3g21

21、g21g24g25g252g21g19g21g20g3 g20g3 g3 g18435g7604g14520g8943g1123g11817g12591g10021g2657g18437g11450g9089g4560g3 g8778g11566g14504g16999g8971g3 g20g3 g14649g3370g3 g7516g7095g1318g16372g4554g1206g18429g17240g7598g14514g8937g1117g11811g12585g10015g2651g18431g11444g8772g11560g14498g16993g9083g4554g7145

22、g8965g452g3 g7516g7095g1318g17970g11096g1214g18429g17240g7598g14514g8937g1117g11811g12585g10015g2651g18431g11444g9083g4554g452g3 g21g3 g16378g14649g5725g5451g11102g7101g1324g3 g1083g2119g7095g1318g1117g11444g1973g4585g17994g17911g7095g1117g11444g16372g14643g5719g5445g11096g13884g7604g6208g7516g7095g

23、1318g5621g1085g2591g4673g11444g7569g8558g452g1958g1117g712g8984g7189g7503g11444g5445g11096g7095g1318g712 g1269g16917g7189g7503g4649g5316g11444g10360g7516g17970g11096g1214g7516g7095g1318g727g1085g8984g7189g7503g11444g5445g11096g7095g1318g712g1958g7472g7136g10360g7516g708g2357g6428g6256g7481g11444g156

24、6g7017g2437g709g17970g11096g1214g7516 g7095g1318g452g3 g42g37g18g55g3g22g22g19g21g28g3g3g7598g14514g8937g2554g11560g1955g14924g10015g1239g2801g13556g6208g3g3g8715g13558g12753g8772g11560g14498g16993g2102g7616g7145g8965g3 g22g3 g7525g16931g2754g4560g1151g3 g7516g7095g1318g8913g7481g19760g16305g11132g4

25、554g11444g7519g16925g2748g4554g1145g452g3 g23g3 g2517g10812g3 g18429g7598g14514g8937g1117g11444g2612g13556g2102g3344g1958g18221g14125g5575g2144g1909g2102g8772g2374g5286g17931g15996g8772g11560g14498g16993g2102g12267g15g1958g13556g2102g11444g11560g4649g17240g18431g2102g7072g2591g2137g11096g13556 g2102

26、g11444g4896g19858g12319g11438g2102g7072g11g5506g1072g2374g8965g12g17931g15996g16849g12743g452g3 g24g3 g16907g2168g3 g24g17g20g3 g11811g12585g10015g708g14498g16993g13535g709g452g3 g24g17g21g3 g17837g8772g726g8798g8772g6214g8793g8772g712g13535g5334g1085g1406g1214g28g28g17g28g28g705g452g3 g24g17g22g3 g

27、17845g2265g8772g1411g726g8786g8772g712g13535g5334g1085g1406g1214g28g28g17g28g28g705g712g5282g10261g12458g8772g712g13535g5334g1085g1406g1214g28g28g17g28g705g452g3 g25g3 g1312g3230g3 g25g17g20g3 g15086g20421g16123g13732g3 g16369g3374g20g452g3 g39g37g23g24g18g55g3g21g21g24 g21g3 g7735g5445g5311g2599 g2

28、0g252g252g2256g10013 g21g252g252g15080g20415 g22g252g252g2023g2061 g23g252g252g11599g12458 g24g252g252g6613g7014 g25g252g252g11599g12458 g26g252g252g11599g12458 g27g252g252g56g3515 g25g17g21g3 g8778g11566g14504 g1959g7481g8786 g25g17g22g3 g14504g16999g7719 g2591g17977g11096 g2506g19g17g21g24 g3 g173

29、g80 g25g17g23g3 g7078g6564g16870 g1959g7481g7072 g26g3 g16907g7789g20154g3898 g12320g18431g18429 g4013g15080g20415g16117g13726 g6381g11599g12458g712g6615 g2423g9305g452g5507g15080 g12458g8997g712g1676g2023 g3 g25g252g21g19g21g20g3 g16932g7230g726g3 g3975g727g3 g11046g727g3 g12753g727g3 g6613g2567g12

30、753g727g3 g11046g727g3 g13635g2018g13696g727g3 g8997g727g3 g2491g2251g16849g452g3 g16999g1312g3 g9883g10080g12267g4480g2374 g3 g1973g9138g19854g7601g5719 g11444g14498g16993g7713g712g6214 g5515g2560g3898g10812g13105 g6558g16864g5509g2748g3892 g10812g3 g17240g7598g14514g8937g21g19 g452g6613g17994g2023

31、g2061 g2150g11599g12458g5334g3416 g20415g10007g11046g11444g20415 g2061g8804g452g6390g2472 g2374g7920g9083g3224g708g41g44g39 g6214g5473g7601g5719g3370g4554 g2620g12665g7569g1318g1083 g13589 g3892g10806g2255g14125g11444g16849g12743 g3 g74g1602g1941g15080g20415g11046 g8804g712g11096g11811g7929 g26g21 g

32、3 g70g80g43g74g794g26g23 g2090g10393g7113g9186g9508g17999 g16117g13726g7206g1912g12331g5424 g3380g20g3 g709g2748g12347g5311g2423 g9186g11444g11811g14625g8715 g2591g17902g2144g2102g12267 g7530g14498g16993g5141g1420 g712g4662g15080g20415g11046 g708g6214g8715g5166g709g2357 g3 g70g80g43g74g19492g452g150

33、80 g5334g4673g1214g24g9508 g2023g2061g12753g712g1981 g15086g20421g16123g13732g3380 g9305g6615g2150g13099g13583 g13558g12753g14498g16993g7713 g7032g7628g11444g14498g16993 g12553g452 g7022g1941g2256g10013g3975 g16169g15080g20415g11046g712 g20415g11046g1973g9186g11560 g8703g2102g19151g7206g2472 g6390g1

34、5080g20415g11046g1082 g3 g11444g8772g11560g14498g16993 g712g4556g1455g11096g7713 g7713g452g3 g3370g4554g4013g712g6658 g6275g5424g2256g10013g3975 g9305g5334g17902g2144g20g26 g11599g12458g712g2472g11599 g11444g9305g5334g16849g712 g1306g452g3 g19375g22g19 g3 g80g451g1973g5556 g1941g8877g451g9186g11560

35、g11109g9408g5424g4091g2256 g19 g3 g263g7206g1955g19485g2256 g12458g7206g1085g5316g17911g5659 g4662g16117g13726g6390g19604 g3 g5556g19g17g21g24 g3 g80g80g2748 g11560g9305g5334g16849g712g6457 g2256g10013g452g6275g5424g11599g12458 g2256g10013g11109g2491g712g16857 g5659g452g2472g4540g11599g12458 g19604g

36、452g3 g3 g3370g4554g9186g14284 g3374g20g17934g6613 g8997g17931g15996 g1958g13635g6034 g1955g19485g11599 g39g37g23g24g18g55g3g21g21g24g25g252g21g19g21g20g3 g22g3 g27g3 g14504g16999g2108g7622g7575g1324g3 g14498g16993g2102g7616g7569g1318g1485g6558g14498g16993g1306g2591g14125g1354g7481g6256g1085g2620g71

37、2g4556g17977g6425g11444g14498g16993g2102g7616g7569g1318g4018g1083g726 g252g252g3g7713g12769g17319g4091g9305g5334g726g20g19g19 g3 g263g727g3 g252g252g3g2423g9305g12347g5311g726g1278g2125g4091g9305g5334g20g19g19 g3 g263g712g1301g24 g3 g263g18g80g76g81g17999g10679g2423g9305g2144g20g21g23 g3 g263g712g19

38、81g1301g19g17g24 g3 g263g18g80g76g81g17999g10679g2423g9305g2144 g20g21g27 g3 g263g712g7472g2622g1301g21g19 g3 g263g18g80g76g81g17999g10679g2423g9305g2144g21g24g19 g3 g263g712g5286g3416g21g24g19 g3 g263g1549g6449g22 g3 g80g76g81g727g3 g252g252g3g7920g9083g3224g9305g5334g726g21g26g19 g3 g263g727g3g3 g

39、252g252g3g17931g7783g2579g9305g5334g726g21g26g19 g3 g263g727g3 g252g252g3g2102g9073g8708g726g24g19g29g20g727g3 g252g252g3g17837g8772g9073g17999g726g20g19g19 g3 g80g47g18g80g76g81g727g3 g252g252g3g8786g8772g9073g17999g726g23g19 g3 g80g47g18g80g76g81g727g3 g252g252g3g12458g8772g9073g17999g726g22g19g19

40、 g3 g80g47g18g80g76g81g727g3 g252g252g3g4718g2665g8772g9073g17999g726g21g24 g3 g80g47g18g80g76g81g727g3 g252g252g3g17931g7783g18431g726g19g17g20 g3 g173g47g452g3 g28g3 g11817g12591g10021g2657g18437g11450g9089g4560g3 g18423g7783g11556g6613g17931g7783g712g6457g10135g42g37g18g55g3g22g22g19g21g28g1117g1

41、9858g12319g5506g1072g2374g8965g11444g16305g8818g9083g4554g452g18429g17240g7598g14514g8937g1960g3515g8772g11560g14498g16993g3374g708g4896g19858g12319 g5506g1072g2374g8965g709g2546g16369g3374g36g17g20g452g3 g20g19g3g16855g12749g2560g13577g7634g16030g12144g3 g18429g17240g7598g14514g8937g1117g11811g1258

42、5g10015g11444g2651g18431g59g51g708g705g709g16849g12743g18423g11096g14498g16993g19858g12319g5506g1072g2374g8965g712g1301g11811g12585g10015g11444g8772g11560g14498g16993g4896g19858g12319g2448g8772 g11560g14498g16993g3374g1117g6256g7481g14498g16993g4896g19858g12319g11444g11438g2102g7072g708g705g709g1602

43、4g12138g712g6457g5439g708g20g709g17931g15996g16849g12743g452g3 g3 g1850 g3017 g3404 g3040 g3117 g3002 g3265 g3040uni2211 g3002 g3284 g3284 g3117 g3400g883g882g882 uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni0

44、0B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni

45、00B7uni00B7uni00B7uni00B7uni00B7uni00B7uni00B7 g11g20g12g3 g5439g1117g726g3 m g252g252g15080g20415g2173g18429g17240g7598g14514g8937g11444g17240g18431g727 m 1 g252g252g15080g20415g6256g5575g20415g2102g11444g17240g18431g727 A P g252g252g11811g12585g10015g11444g14498g16993g4896g19858g12319g727g3 i 1 i

46、Ag258g258g6256g7481g14498g16993g4896g19858g12319g1147g2748g452g3 g2566g1108g8529g5283g15996g9083g4554g13571g7628g11444g12743g7519g5283g3447g1644g1130g6357g2682g13571g7628g712g1549g11145g14371g4671g7072g9961g2622g20g1405g452g3 g20g20g3g13044g4604g5340g3 g3416g18429g3901g5719g7569g1318g1083g14823g5575

47、g11444g1108g8529g5283g15996g9083g4554g13571g7628g11444g11560g4649g5150g1644g1085g3927g1214g20g19g8g452g3 g3g3g3 g3 g3 g3 g3 g39g37g23g24g18g55g3g21g21g24 g23g3 g36g17g20g3 g8778g11566g14504 g18429g17240g7598 g7735g5445g5311g2599 g20g252g252g162g16 g21g252g252g14816g10015 g22g252g252g163g16 g23g252g2

48、52g162g16 g24g252g252g14615g10015 g25g252g252g19375g2598 g26g252g252g11811g12585 g27g252g252g14974g14713 g25g252g21g19g21g20g3 g16999g3380g3 g14514g8937g1960g3515g8772 g16932g7230g726g3 g15038g10015g727g3 g727g3 g15038g10015g727g3 g20425g2598g10015g727g3 g727g3 g10015g727g3 g10015g727g3 g10015g452g3

49、 g11560g14498g16993g3374g16369 g3380 g19578 g8778 g3374g36g17g20g452g3 g36g17g20g3g3g18435g17246 g3 g36 g3g36 g3 g5515g36g3 g948g17274g7119g5725g949g3 g11566g14504g16999g3380g3 g7604g14520g8943g1966g3521g8778g11566g14504g16999g3380g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g726g1255g800g3486g1056g1430g1677g2296g5940g1696g2996g3221g1101g1 g6615g3162g5355g3571g726g4482g4715g3927g1380g6617g4361g3645g2047g3488g4400g5347g6119g3585g1 g37g35g1g21g22g16g53g1g19g19g22g23g803g19g17g19g18g1 g2296g5940g1828g3007g5292g3572g1244g2249g1699g4386g4437g4781g4144g2124g4945g694g1278g1156g1 g10366g7