DB37 T 1206-2009 饲料中孔雀石绿的测定 高效液相色谱法.pdf

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1、a0a1a2 a3a4a5a6a7a8 a9 a7a8 DB37 山 东 省 地 方 标 准 DB37/T 12062009 饲料中孔雀石绿的测定 高效液相色谱法 Determination of malachite green and leucomalachite green in feeds High-Performance Liquid Chromatography 2009-03-03发布 2009-04-01实施 山东省质量技术监督局 发 布 DB37/T 12062009 I 前 言 a10a11a12a13a14a15a16a17a18a19a13a14a20 a10a11a12

2、a21a22a23a24a25a26a27a11a12a28a29a30a31a32a33a34a35a36a37a38a20 a10a11a12a39a40a41a42a43a22a23a24a44a18a45a46a47a48a49a20 a10a11a12a50a51a39a40a52a43a53a33a54a55a53a56a57a55a58a59a55a60a57a57a55a61a62a63a20 DB37/T 12062009 1 a64 a65a66 a67a68a69a70a71a72a73a74a75a76a77a78a79a80a81a71a82a83a84a85a86a

3、87a88a89a90a78a85a86a87a88a91a92a93a94 a67a68a69a95a73a96a97a98a99a100a101a82a83a99a102a103a82a83a89a104a101a105a106a101a82a83a84a85a86a87a88a89a90a78a85a86a87a88a91a81a71a94 a67a92a93a107a108a71a109a110a111a112 a113 a114 a115a116 a114 a94 a117 a118a65 a119a120a121a122a123 a124a125a126a127a84a91a128

4、a129a130a131a67a68a69a91a132a73a133a134a111a67a68a69a91a128a129a94a135a136a137a138a139a91a132a73a126a127a140a141a142a143a144a145a91 a146a147a148a149a150a151a152a153a154a91a155a156a157a158a146a159a160a161a150a95a73a96a67a68a69a140a162a133a140a163a164a165a166a67a68a69a167a134a168a169a91a170a92a171a172

5、 a136a173a174a175a73a176a177a126a127a91a107a178a160a67a94a135a136a150a137a138a139a91a132a73a126a127a140a141a107a178a160a67a95a73a96a67a68a69a94 a179a180 a115 a181 a182a182a183a184 a185 a186a187a188a189a73a190a70a191a89a192a188a92a93 a179a180 a115 a181 a184a113 a112 a193a194 a195 a196a82a83a192a197a9

6、1a198a199 a200 a201a202 a192a197a84a91a85a86a87a88a73a85a86a87a88a203a204a205a81a206a207a208a192a209a210a211a212a91a192a209a211a213a99a102a103a143a214a74a75a76a77a78a79a80 a149 a215a216a217a218 a157a219a220a221a222 a185a223 a140a73a224a225a226a227a125a205a81a228a229a230a71a231a140a232a233a174a234a23

7、5a205a81a228 a182 a112 a183 a236a237 a207a81a71a94 a238 a239a240 a241a242a243a145a244a245a140a214 a185 a186a84a246a175a73a247a248a111 a185 a186a249a91a192a209a94a190a140a250a101 a179a180a115a181 a182a182a183a184a251a252 a190a91a70a71a94 a238a253a64 a254 a255a0a78a79a249a94 a238a253a117 a90a190a1a2a3

8、a94 a238a253a200 a4 a5a0a78a79a249a94 a238a253a238 a6a254 a7a0a78a79a249a94 a238a253a8 a9a10 a11a94 a238a253a12 a13a14a15 a16a17a2a94 a238a253a18 a90a190a1a2a19a94 a238a253a20 a254 a7a21a22a23a24a25a0a26a213a27a28 a193a194 a114 a90a190a1a2a3a89 a113 a28 a193a194 a114 a13a14a15 a16a17a2a29a30a96a31 a

9、183a113a113 a237 a217 a190a84a140a73a32a1a2 a33a34a35 a215a36 a27a28 a194 a140a73a190a71a156 a36 a112 a113a113a113 a237 a217 a94a131 a113 a28a27 a194 a37 a237a38 a39a140a199a73a94 a238a253a40 a41a42 a43a0a1a44a45a1a2a3a46a47a76 a149a27a28 a183 a157 a48 a182a113 a45a27 a113 a140a106a49a140a50a51a52a5

10、3 a194 a237a54a236a55 a112 a113 a237a54a236 a94 a238a253a64a56 a85a86a87a88a203a204a205a81a206a207a208a192a209a210a57a58 a94 a192a209a210a84a151a152a59a27a28a112 a113 a28a112a211a213a209a112a149a76a60a111 a184a113 a28 a113 a237 a217 a157 a61 a27a28a112 a113 a28 a184 a211a213a209 a184 a149a62a60a31a1

11、12 a113 a114 a157 a61 a27a28a112 a113 a28 a63 a85a86a87a88a64a73a62a77a65a213a66a221a94 a238a253a64a64 a67 a68a25a69a0a1a44a45a32a1a2 a48 a193a183 a45 a184 a94 a238a253a64a117 a67 a68a25a70a0a1a44a45a32a1a2 a48 a193a194 a45 a194 a94 a238a253a64a200 a67 a71 a240 a69a0a32a1a2a72 a15 a11 a73 a184a113 a

12、72 a183a113 a94 a238a253a64a238 a67 a71 a240 a70a0a1a44a72a190 a73 a184a113 a72 a183a113 a94 a74a75a76a77a78a79a80a81a82a83a84a85a86a87a88a89a90a91 a92a93a82a94a82a95a96a97a98a99a100a98a101a102a103a104a105a106a82a107a108a109a110a111a112a113a114a114a115a116a106a115 a117a118a119a120a121a122a123a124a12

13、5a90a126a127a120a128a129a130a116a131a132a133a134a135a136a137a138a139a140a90a129a130a141a142a143a144a145a122a123a114a115a116a146a147a119 饲料中孔雀石绿的测定 高效液相色谱法 DB37/T 12062009 2 a148a149a150a151 a152 a153a154a155a156a157a158a159a160a161a162 a163a164 a165a166a167 a152 a153a154a168a169a170a171a172 a163a173

14、 a174a175a167a176 a168a177a178 a152 a153a179a180a181 a182a183a164 a162 a173 a168a184a185a186 a187 a183a188a173a173a173 a174a175a189 a190 a173 a162 a191a164a192 a174a193 a194a168a195a177 a189 a148a149a150a196 a197a198 a199a200a201 a166a202 a197a198 a199a200a203a204a205a158a206a207a208a171a172 a164a20

15、9 a189 a148a149a150a210 a197a198 a199a200a203a204a211a195a169a157a158a204a212a159a160 a197a198 a199a200a173a162 a188a173a173a173 a165 a171 a188a173a173 a174a175a213a202 a187a214a215 a176 a168a216a161 a173 a174a175 a152 a217a169a170 a185a168a177 a152 a217a186a187 a189 a218a169a157a219a207a220 a188 a1

16、74a165 a221 a174a175a189 a222a223a224a225 a189a226 a188a163a227 a224a228a229a230a231a232 a189 a148a149a150a233 a166a202 a197a198 a199a200a203a204a211a195a169a157a158a204a212a159a160 a166a202 a197a198 a199a200a173a162 a188a173a173a173 a165 a171 a188a173a173 a174a175a213a202 a187a214a215 a176 a168a216

17、a161 a173 a174a175 a152 a217a169a170a185a168a177 a152 a217a186a187 a189 a218a169a157a219a207a220 a188 a174a165 a221 a174a175a189 a222a223a224a225 a189a226 a188a163a227 a224a228a229a230a231a232 a189 a148a149a150a234 a197a198 a199a200a201 a166a202 a197a198 a199a200a235a236 a176 a237a157a158a204a212a23

18、8a160 a197a198 a199a200a203a204a211a195a169a157a239 a191 a162 a188a240a241 a201 a166a202 a197a198 a199a200 a203a204a211a195a169a157a239 a191 a162 a188a163a241 a242 a188 a174a175 a168a243a171 a188a173a173 a174a175a213a202 a187a214a215 a176 a168a177 a152 a217a186a187 a189 a218a169a157 a197a198 a199a20

19、0a201 a166a202 a197a198 a199 a200a219a207a244a220 a188a173a192 a165 a221 a174a175a189 a230 a227 a245 a163a227 a224a228a229 a188 a231a232 a189 a148a149a246a247 a197a198 a199a200a201 a166a202 a197a198 a199a200a235a236a203a204a248a249a157a158a204a212a238a160a197a198a199a200a201 a166a202 a197a198 a199a2

20、00a235a236 a176 a237a157a239 a191 a162 a188 a172 a241 a188 a174a175 a168a243a171 a188a173a173 a174a175 a213a202 a187a214a215 a176 a168a177a250a251a252 a239 a191 a162a172 a241 a186a187 a189 a218a169a157 a197a198 a199a200a201 a166a202 a197a198 a199a200a219a207a244a220 a188a173a173 a253a165 a221 a174a1

21、75a189 a254a177a254a255 a189 a151 a0a1 a2a3a4 a151a149a150 a5 a6a7a8a9a10a214 a173 a162 a188 a174a165a189 a151a149a246 a11 a206 a167 a12 a189 a151a149a13 a14a15 a235a236a12 a189 a151a149a148 a16a17 a18a9a19a20 a164a173a173a173 a21 a221 a174a22a253a189 a151a149a151 a23 a24a157a252 a202 a25a26a158a255

22、a27a28a29a30a12a201a31a32a33a34a35a29a30a12 a189 a151a149a196 a36 a252a37a160a38a243 a189 a196 a39 a40a41a42a4 a43a160a44a45a46a47a48a49a50a205 a183a51a164a173a173 a165 a168a52a53 a54 a221 a55 a230 a173a188 a172 a164a56 a195a50a205a168a57a58a168a59a60a61a190 a197 a62a220 a173 a162 a191a164 a174a174a

23、63 a64 a65a66a168a235a67 a189 a38a68a69a70a187a12 a176 a222a223a224a225 a189 a210 a5 a6a71a72 a210a149a150 a73a74 a204a212a159a160a64a50 a164 a165 a239a75a212 a183a173 a162 a173a173a173 a230 a165 a241 a168a243a171 a164a173 a174a175a76 a77a78a79a33 a176 a168a204a212a216 a167 a164 a174a175 a168a235a67

24、a168a80a81 a82a243 a164 a174a22a253a189 a216a68a83a160a84 a188 a239 a191 a162 a188a173 a162 a188a241 a168a85a86a33a85a168a171 a14a15 a235a236a12a87 a15a14 a230 a174a22a253a189 a88a216a68a83a160a84a230a239 a191 a162 a188a173 a162a230 a241 a168 a15a14 a230 a174a22a253a189 a171a78a79a89 a164a173a173a17

25、3 a21 a221 a174a22a253 a78a79 a188a173 a174a22a253a189 a87a90a157a195a177 a189 a210a149a246 a91a92 a210a149a246a149a150 a93 a94a95a96a97a98a99a95a100a101a98a99a41 a91a92 a197a198a199 a200a102a177 a36 a252a37a160a103a104a105a106a177a230 a174a107a108 a109a157a110a239 a191 a162 a188a188a241 a111 a164 a

26、174a107a108 a112a84a110a239 a191 a162 a188 a161 a241 a201 a164 a174a175a167a113 a114a168 a115a116 a183 a117a118 a189 a204a212a238a160a78a79a87a90a157 a239 a240 a162 a188a241a164 a174a175 a171a230 a173 a174a175a63a76 a77a64a33 a176 a168a216a68 a188a173 a174a175a167 a168a235a67a168a105a119a120a68 a197

27、a198a199 a200a102a177 a36 a252a37a160a103a104a239 a191 a162 a188a173 a162a161 a241 a176 a168a88a177a230 a174a175a167 a121a105 a108 a112a64a33a185 a122 a115a190a104 a189 a123a177 a164 a174a175a108 a112a84a124a239 a191 a162 a188 a161 a241 a108 a112a168a125a118a104 a176 a157a126a168a216a68 a188 a162 a1

28、27 a174a175a63a108 a109a157a124a239 a191 a162 a188 a230 a241 a108 a109 a189 a128a129 a108 a109a157a168a177 a152 a153a154a155a156a157a239 a191 a162 a188a164a241 a186 a187 a183 a230a162 a173a173 a174a175a189 a190 a173 a162a230 a174a63 a130 a197 a193 a194a168a131a87a89a30a186 a189 a210a149a246a149a246

29、a132a133 a101a98a99a41 a91a92 a160a78a79a87a90a169a157 a239 a240 a162 a188a241 a168a190 a173 a162a230 a174a63 a130 a197 a193 a194a168a131a87a89a30a186 a189 a210a149a13 a134 a135a136a137a138a139a140a141a142a143 a202 a25a104a158a144a145a104a168a230 a164a173 a174a174a146 a191 a162 a127 a174a174a147 a10

30、4a185a148a114a149a104a158a161 a164 a174a174a146 a191 a162 a127 a174a174a147 a250a251a252a158 a152 a217a150 a152 a153a151a155a156a169a157 a152 a127a173 a150 a191a173 a147 DB37/T 12062009 3 a153a154a155 a156 a157 a158 a159a160a161a159a162a163a164 a165a166a155a167a166 a164 a168a169a170a155 a171a158a172

31、 a160a164 a173a174a175a176a155 a177a156a178 a163a159a179 a180a181a182 a183 a184 a185a186a187a188a189a190a191a192a193a194a195a196a197a198a197a199a200a201a202a203a204a190a205a206a201a202a203a204a200a207a208a209a210a211a199a212a213a201a202a203a204a190a205 a206a201a202a203a204a214a215a216a217 a218a219 a

32、220a221 a222a223a224a225a226a227a213a228a229a230a231a232a233a234a230a231a200a209a210a211a235a205a236a237a238a239a240a186a187a188a189 a241 a242a240 a243a223a224a225a226a244a245a246a247a213 a180a181a248 a183a249 a250 a183 a251a252a253a231a246a206a210a254a255a236a0a1a2a254a198a3a4a5a6a213a7a231a246a206

33、a210a8a9a10a11a201a202a203a204a190a205a206a201a202a203a204a233a234a12 a4a231a13a228a229a230a231a240a14a15a206a210a227a16a17a18a235a19a240a185a20a233a21a199a22a213 a180a181a23 a24a25 a26a27 a228a229a9a201a202a203a204a28a205a206a201a202a203a204a200a29a22a30a6 a31a32a240a6a19a33a34a35a36a37a35 a38 a39

34、a40a41 a39 a42a43a44a240a251a45 a46a217a47a48a49a50 1000 1000 = mP cVPX st ii i (1) a51a52a53 a54a55 a56a56a57a58a59a60a61 a62a63a64a65 a66 a56a56a58a67a68 a69a70a71a72a63a73a74a75a76a77a78 a79 a80a81a82 a65 a83 a55 a56a56a84a85a59a60 a86a87a73a74a75a76a88a89a90a77a78 a79 a91a92 a93 a80a81a82 a65 a5

35、4a94a95 a56a56a84a85a59a60a61 a62a63a96a97a64a65 a98a56a56a57a58a99a100 a73a74a75a76a89 a79 a92a101 a102 a103a104a105a106a107a108a109a110a111a103a112a113a114a115a116a117a118a119a120a121a122a123a124a125 a126 a127a128 a129 a130a131a132a133a134a135a136a137a138a139a140a141a142a143a105a144a107a108a139a14

36、5a146a147a148a149a150a151 a152 a153a154 a125 DB37/T 12062009 4 a155 a156 a157 a158a159a160a161a155a156a162 a163a164a165a166a167a168a169a170a171a172a173a166a167 a167 a157a174a175 a176a177a178a179a180 a181 a182a183a184a185a163a164a165a166a167 a167 a157a174 a186 a187 a173a176a177a178a179a180 a181 a182a

37、183a184a185a163a164a165a166a167 a167 a157a174 a188 a176a177a178a179a168 a187 a173a176a177a178a179a180a173a166a167 a189 a190a191a192a193a194a195a196a197a198 a189 a199a191a194a195a196a197a200 DB37/T 12062009 5 DB37/T 12062009 6 DB 37 /T DB 37 /T DB 37 /T DB 37 /T 1 20 6 12 06 12 06 12 06 20 09 20 09 20 09 20 09