EN 15860-2018 Plastics - Thermoplastic semi-finished products for machining - Requirements and test methods.pdf

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1、BSI Standards PublicationWB11885_BSI_StandardCovs_2013_AW.indd 1 15/05/2013 15:06Plastics - Thermoplastic semi-finished products for machining - Requirements and test methodsBS EN 15860:2018National forewordThis British Standard is the UK implementation of EN 15860:2018. It supersedes BS EN 15860:20

2、10, which is withdrawn.The UK participation in its preparation was entrusted to Technical Committee PRI/21, Testing of plastics.A list of organizations represented on this committee can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions

3、of a contract. Users are responsible for its correct application. The British Standards Institution 2018 Published by BSI Standards Limited 2018ISBN 978 0 580 89035 2ICS 83.080.20Compliance with a British Standard cannot confer immunity from legal obligations.This British Standard was published unde

4、r the authority of the Standards Policy and Strategy Committee on 31 August 2018.Amendments/corrigenda issued since publicationDate Text affectedBRITISH STANDARDBS EN 15860:2018EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN 15860July 2018ICS 83.080.20 Supersedes EN 15860:2010EUROPEAN COMMITTEE FO

5、R STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGCEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2018 CEN Ref. No. EN 15860:2018: EAll rights of exploitation in any form and by any means reserved worldwide for CEN national MembersPlastics - Thermoplastic

6、semi-finished products for machining - Requirements and test methodsMatires plastiques - Produits semi-finis thermoplastiques pour usinage - Exigences et mthodes dessaiKunststoffe - Thermoplastische Halbzeuge fr die spanende Verarbeitung - Anforderungen und PrfmethodenThis European Standard was appr

7、oved by CEN on 27 March 2018.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national s

8、tandards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and

9、 notified to the CEN-CENELEC Management Centre has the same status as the official versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary

10、, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.English VersionEN 15860:2018 (E)European foreword .iv1 Scope . 52 Normative references 53 Terms and defin

11、itions . 54 Materials . 65 Requirements 75.1 As-delivered condition . 75.2 Surface appearance . 85.3 Dimensions and tolerances for rods . 85.3.1 Diameter . 85.3.2 Length. 105.3.3 Roundness 105.3.4 Straightness . 105.4 Dimensions and tolerances for hollow bars . 125.4.1 Diameters 125.4.2 Length. 135.

12、4.3 Roundness 135.4.4 Straightness . 135.4.5 Concentricity 145.5 Dimensions and tolerances for sheets . 155.5.1 Thickness . 155.5.2 Length and width .165.5.3 Straightness . 175.6 Properties . 195.6.1 Material properties .195.6.2 Dimensional stability after heat treatment 195.6.3 Physiological behavi

13、our 216 Test methods 216.1 Test conditions . 216.2 Sampling size . 216.3 Test specimen preparation 216.3.1 Mechanical properties .216.3.2 Density . 236.3.3 Melt volume-flow rate, viscosity number, melting temperature/glass transition temperature 236.3.4 Dimensional stability after heat treatment 236

14、.4 As-delivered condition 246.5 Surface appearance 246.6 Accuracy of the dimension measuring instruments 246.7 Density 256.8 Tensile stress at yield and elongation at break 256.9 Tensile modulus of elasticity 256.10 Vicat softening temperature . 256.11 Melt volume-flow rate (MVR) 256.12 Melting temp

15、erature/glass transition temperature 266.13 Viscosity number . 266.14 Dimensional stability after heat treatment . 266.15 Expression of test results 297 Designation .307.1 Rods . 307.2 Hollow bars . 307.3 Sheets . 30iiContents PageBS EN 15860:2018EN 15860:2018 (E)8 Marking .31Annex A (normative) Det

16、ermination of microporosity Dye penetration method 32Annex B (normative) Tables for the conversion of deflection values (straightness) 34Annex C (informative) Examples of calculation of dimensional stability after heat treatment .37Annex D (informative) Some guideline values for material properties

17、of thermoplastic semi-finished products .39Bibliography .43 ISO ISO pub-date year All rights reserved iiiBS EN 15860:2018EN 15860:2018 (E)European forewordThis document (EN 15860:2018) has been prepared by Technical Committee CEN/TC 249 “Plastics”, the secretariat of which is held by NBN.This Europe

18、an Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by January 2019, and conflicting national standards shall be withdrawn at the latest by January 2019.Attention is drawn to the possibility that some of the elemen

19、ts of this document may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent rights.This document supersedes EN 15860:2010.This edition cancels and replaces former editions which were technically revised. The main changes are as follows: ECTFE was

20、 deleted in Table 1 due to the fact that there was no need anymore; in subclause 5.1 POM-H was changed into POM; in subclause 5.3.4, Table 3 “Straighness requirements for rods”, the material PE-UHMW was changed from column 3 to column 2; the notes in Table 3, subclause 5.3.4 are updated; in Figure 4

21、c) (subclause 5.5.3) the reference “3” was deleted; Annex A “Determination of miocroporosity Dye penetration method” has been rewritten; Annex D has been rearranged.According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following countries are bound to impleme

22、nt this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, S

23、erbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.ivBS EN 15860:2018EN 15860:2018 (E)1 ScopeThis document specifies the requirements and associated test methods that apply to semi-finished products such as rods, hollow bars and plates made from thermoplastic materi

24、als. These semi-finished products are used predominantly for the manufacture of finished parts by means of machining.2 Normative referencesThe following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated referenc

25、es, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.EN ISO 291, Plastics Standard atmospheres for conditioning and testing (ISO 291)EN ISO 306, Plastics Thermoplastic materials Determination of Vicat softening t

26、emperature (VST) (ISO 306)EN ISO 307, Plastics Polyamides Determination of viscosity number (ISO 307)EN ISO 527-1, Plastics Determination of tensile properties Part 1: General principles (ISO 527-1)EN ISO 527-2, Plastics Determination of tensile properties Part 2: Test conditions for moulding and ex

27、trusion plastics (ISO 527-2)EN ISO 1133-1, Plastics Determination of the melt mass-flow rate (MFR) and melt volume-flow rate (MVR) of thermoplastics Part 1: Standard method (ISO 1133-1)EN ISO 1183-1, Plastics Methods for determining the density of non-cellular plastics Part 1: Immersion method, liqu

28、id pyknometer method and titration method (ISO 1183-1)EN ISO 1183-2, Plastics Methods for determining the density of non-cellular plastics Part 2: Density gradient column method (ISO 1183-2)EN ISO 1628-5, Plastics Determination of the viscosity of polymers in dilute solution using capillary viscomet

29、ers Part 5: Thermoplastic polyester (TP) homopolymers and copolymers (ISO 1628-5)EN ISO 2818, Plastics Preparation of test specimens by machining (ISO 2818)EN ISO 10350-1, Plastics Acquisition and presentation of comparable single-point data Part 1: Moulding materials (ISO 10350-1)EN ISO 11357-1, Pl

30、astics Differential scanning calorimetry (DSC) Part 1: General principles (ISO 11357-1)EN ISO 11357-3, Plastics Differential scanning calorimetry (DSC) Part 3: Determination of temperature and enthalpy of melting and crystallization (ISO 11357-3)EN ISO 15527, Plastics Compression-moulded sheets of p

31、olyethylene (PE-UHMW, PE-HD) Requirements and test methods (ISO 15527)3 Terms and definitionsFor the purposes of this document, the following terms and definitions apply.ISO and IEC maintain terminological databases for use in standardization at the following addresses: IEC Electropedia: available a

32、t http:/www.electropedia.org/ ISO Online browsing platform: available at http:/www.iso.org/obp 5BS EN 15860:2018EN 15860:2018 (E)3.1semi-finished productrod, hollow bar and sheet from which finished parts are manufactured by means of machining3.2rodlong, straight and solid product manufactured by me

33、ans of extrusion, casting or compression moulding and having a uniform circular cross-section over their entire length3.3hollow barlong, straight and hollow product manufactured by means of extrusion, casting or compression moulding and having a uniform circular cross-section, with concentric inside

34、 and outside diameter, over their entire length3.4sheetflat, rectangular, solid product manufactured by means of extrusion, extrusion, calendering, casting or compression moulding and having a thickness of at least 0,2 mm which is uniform over their full cross- section4 MaterialsThe semi-finished pr

35、oducts shall be made of thermoplastic materials (see Table 1). The compounds may contain additives such as processing aids, reinforcing agents, fillers, stabilizers or colorants, in which case, they are further referred to in this standard as “modified materials”.The nature and the quantity of these

36、 additives can influence the mechanical, thermal and electrical properties of the semi-finished products. The choice and the quantities of additives used are left to the discretion of the manufacturer.Table 1 List of the thermoplastic materials most commonly used for the manufacture of semi-finished

37、 productsAbbreviated terms MaterialsABS Acrylonitrile-butadiene-styrene plasticPA6 Polyamide 6PA6 C aPolyamide 6, castPA66 Polyamide 66PA12 Polyamide 12PA12 C aPolyamide 12, castPA46 Polyamide 46PA6/12 C abPolyamide 6/12, castPBT Polybutylene terephthalatePC PolycarbonatePEEK PolyetheretherketonePE-

38、HD Polyethylene, high density (Group 2.1 or 3.1 of EN ISO 15527)PE-LD Polyethylene, low densityPE-UHMW Polyethylene, ultra high molecular weight (Group 1.1 or 1.2 of EN ISO 15527)PEI PolyetherimidePESU PolyethersulfonePET Polyethylene terephthalatePOM-C Polyoxymethylene, copolymer6 BS EN 15860:2018E

39、N 15860:2018 (E)Abbreviated terms MaterialsPOM-H Polyoxymethylene, homopolymerPP-B Polypropylene, block copolymerPP-H Polypropylene, homopolymerPP-R Polypropylene, random copolymerPPE + PS Polystyrene modified polyphenylene etherPPS Polyphenylene sulfidePPSU Polyphenylene sulfonePSU PolysulfonePVC-C

40、 Polyvinyl chloride, chlorinatedPVC-HI Polyvinyl chloride, high-impact modifiedPVC-U Polyvinyl chloride, unplasticizedPVDF Polyvinylidene fluoridea“C” means “cast” bPA6/12 with max. 15 % laurinlactam 5 Requirements5.1 As-delivered conditionSemi-finished products shall be free of blisters, voids, cra

41、cks, foreign matter and other defects which make the product unfit for the intended use. Specific requirements in this respect shall be agreed upon between manufacturer and customer.The semi-finished products shall be manufactured in such a way that their internal stress level is minimal (see 5.6.2)

42、.Natural coloured materials: slight variations in hue originating from raw materials and/or manufacturing process are allowed.Natural colour means that no additives (colorants) are added to the raw material during their manufacture and processing into semi-finished products for the purpose of obtain

43、ing another colour.Colorations: These shall be agreed upon between manufacturer and customer. The coloration shall be uniform. Slight variations in hue originating from raw materials and/or manufacturing process are allowed.The testing of the as-delivered condition shall be performed according to 6.

44、4.NOTE Semi-finished products made from PA are dry after manufacture, but absorb moisture during storage. The moisture content in the as-delivered condition depends on the type of moulding material, the cross-section (plate thickness, rod diameter or hollow bar wall thickness) of the semi-finished p

45、roducts, as well as the type and period of storage.Semi-finished products made from POM, PEEK and PP are permitted to have light patches in the centre of the cross-section.Microporosity in the centre of the cross-section may occur in semi-finished products made from POM and PP. The largest diameter

46、or the widest part of the microporosity line(s) shall not exceed 4 %. The procedure for the determination and measurement of microporosity is described in Annex A.When semi-finished products made from POM and PP are subject to specific requirements, e.g. pressure tightness (microporosity) and/or die

47、lectric strength, they shall be agreed upon between manufacturer and customer.7BS EN 15860:2018EN 15860:2018 (E)5.2 Surface appearanceSemi-finished products shall essentially have smooth surfaces. Shallow marks, grooves and irregularities resulting from the manufacturing process are allowed provided

48、 that the product meets the dimensional requirements according to 5.3, 5.4 and 5.5.Testing of the surface appearance shall be performed according to 6.5.Specific requirements with respect to the surface appearance are to be agreed upon between manufacturer and customer.5.3 Dimensions and tolerances

49、for rods5.3.1 DiameterThe diameters commonly available are given in the delivery programmes of the manufacturers.The tolerances on the diameters are given in Table 2 for different diameter ranges.Table 2 Tolerances on diameters for rodsDimensions in millimetresDiameter rangesColumn 1 Column 2 Column 3 Column 4 Column 5PA6PA46PA66PA12PBTPEEKPETPOMPPSPVDFPA6 CPA6/12 CPA12 CABSPCPEIPESUPPE + PSPPSUPSUPE-LDPE-HDPE-UHMWPP-BPP-HPP-RPVC-CPVC-HIPVC-Uup to 4+0,6+0,1+0,7+0,1+0,3+0,1over 4 up to 6+0,4+0,1over 6 up