IEC 60454-2-2007 Pressure-sensitive adhesive tapes for electrical purposes - Part 2 Methods of test《电工用压敏粘带.第2部分 试验方法》.pdf

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1、 INTERNATIONAL STANDARD IEC 60454-2Third edition 2007-06Pressure-sensitive adhesive tapes for electrical purposes Part 2: Methods of test Reference number IEC 60454-2:2007(E) THIS PUBLICATION IS COPYRIGHT PROTECTED Copyright 2007 IEC, Geneva, Switzerland All rights reserved. Unless otherwise specifi

2、ed, no part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from either IEC or IECs member National Committee in the country of the requester. If you have any questions about

3、IEC copyright or have an enquiry about obtaining additional rights to this publication, please contact the address below or your local IEC member National Committee for further information. IEC Central Office 3, rue de Varemb CH-1211 Geneva 20 Switzerland Email: inmailiec.ch Web: www.iec.ch About th

4、e IEC The International Electrotechnical Commission (IEC) is the leading global organization that prepares and publishes International Standards for all electrical, electronic and related technologies. About IEC publications The technical content of IEC publications is kept under constant review by

5、the IEC. Please make sure that you have the latest edition, a corrigenda or an amendment might have been published. Catalogue of IEC publications: www.iec.ch/searchpub The IEC on-line Catalogue enables you to search by a variety of criteria (reference number, text, technical committee,). It also giv

6、es information on projects, withdrawn and replaced publications. IEC Just Published: www.iec.ch/online_news/justpub Stay up to date on all new IEC publications. Just Published details twice a month all new publications released. Available on-line and also by email. Customer Service Centre: www.iec.c

7、h/webstore/custserv If you wish to give us your feedback on this publication or need further assistance, please visit the Customer Service Centre FAQ or contact us: Email: csciec.ch Tel.: +41 22 919 02 11 Fax: +41 22 919 03 00 INTERNATIONAL STANDARD IEC 60454-2Third edition 2007-06Pressure-sensitive

8、 adhesive tapes for electrical purposes Part 2: Methods of test X For price, see current catalogue PRICE CODE Commission Electrotechnique Internationale International Electrotechnical Commission 2 60454-2 IEC:2007(E) CONTENTS FOREWORD.5 1 Scope.7 2 Normative references .7 3 Conditioning and specimen

9、 preparation8 4 Determination of thickness .8 4.1 Test apparatus 8 4.2 Test specimens .8 4.3 Procedure .8 4.4 Results8 5 Determination of width8 5.1 Method A.8 5.2 Method B.9 5.3 Method C 9 6 Determination of roll length.10 6.1 Principle10 6.2 Method A Measurement of turns method 10 6.3 Method B Len

10、gth sensor method 11 7 Corrosion-related properties.11 7.1 General .11 7.2 Preparation of water extract for pH and conductivity determinations11 7.3 Determination of pH value of water extract 12 7.4 Determination of conductivity of water extract .12 7.5 Detection of corrosive sulfur13 7.6 Insulation

11、 resistance method.14 7.7 Visual method .14 7.8 Wire tensile strength method.14 8 Tensile strength and elongation at break 15 8.1 Apparatus15 8.2 Test specimens .15 8.3 Procedure .15 8.4 Results15 9 Low-temperature properties15 9.1 Principle15 9.2 Test specimen.16 9.3 Procedure .16 9.4 Flexibility.1

12、6 9.5 Electric strength 16 9.6 Results16 10 Resistance to penetration at elevated temperatures .17 10.1 Apparatus17 10.2 Test specimens .17 10.3 Procedure .17 10.4 Results17 11 Adhesion 17 60454-2 IEC:2007(E) 3 11.1 Principle17 11.2 Materials .18 11.3 Apparatus18 11.4 Test samples and test pieces 19

13、 11.5 Procedure .20 11.6 Expression of results.20 12 Adhesion to backing at low temperatures21 12.1 Test specimens .21 12.2 Procedure .21 12.3 Results21 13 Shear adhesion to backing after liquid immersion.21 13.1 Apparatus21 13.2 Test specimens .21 13.3 Procedure .22 13.4 Results22 14 Curing propert

14、ies of thermosetting adhesive tapes .22 14.1 Bond separation during thermal treatment (adhesive to backing).22 14.2 Bond separation after thermal treatment (adhesion to backing) .22 15 Flagging tests.23 15.1 Principle23 15.2 Apparatus23 15.3 Test specimens .23 15.4 Preparation of specimens for test

15、24 15.5 Test conditions24 15.6 Results24 16 Water vapor permeability24 16.1 Apparatus24 16.2 Test specimens .24 16.3 Procedure .25 16.4 Results25 17 Electric strength .25 17.1 General .25 17.2 Test specimens .25 17.3 Procedure .25 17.4 Results25 18 Electric strength after humid conditioning .26 19 R

16、esistance to flame propagation 26 19.1 Principle26 19.2 Apparatus26 19.3 Test specimen.26 19.4 Procedure .27 19.5 Results27 20 Flame test 27 20.1 Principle27 20.2 Apparatus28 20.3 Preparation of test specimen.28 20.4 Procedure .29 20.5 Results29 4 60454-2 IEC:2007(E) 21 Thermal endurance 29 21.1 Det

17、ermination of thermal endurance (based on IEC 60216-1 and IEC 60216-2).29 21.2 Voltage breakdown30 21.3 Loss of mass.31 Annex A (normative) Rollers to be used in various tests.40 Bibliography41 Figure 1 Measuring device for determination of roll length of tape (measurement of turns method) .32 Figur

18、e 2 Measuring device for determination of roll length of tape (length sensor method) 32 Figure 3 Sequence of bends 33 Figure 4 Dielectric strength test in water33 Figure 5 Sketch of penetration tester .34 Figure 6 Steel test plate.35 Figure 7 Arrangement for stripping the tape from the plate.35 Figu

19、re 8 Flagging test Preparation of test specimen36 Figure 9a Draught protection device 37 Figure 9b Use of Bunsen burner and sliding plate with draught protection device.37 Figure 9 Flame test enclosures 37 Figure 10 Essential dimensions for flame test (proportions exaggerated for clarity of details)

20、 .38 Figure 11 Dimensions of wedge .39 Table 1 Conditioning for low temperature properties 16 60454-2 IEC:2007(E) 5 INTERNATIONAL ELECTROTECHNICAL COMMISSION _ PRESSURE-SENSITIVE ADHESIVE TAPES FOR ELECTRICAL PURPOSES Part 2: Methods of test FOREWORD 1) The International Electrotechnical Commission

21、(IEC) is a worldwide organization for standardization comprising all national electrotechnical committees (IEC National Committees). The object of IEC is to promote international co-operation on all questions concerning standardization in the electrical and electronic fields. To this end and in addi

22、tion to other activities, IEC publishes International Standards, Technical Specifications, Technical Reports, Publicly Available Specifications (PAS) and Guides (hereafter referred to as “IEC Publication(s)”). Their preparation is entrusted to technical committees; any IEC National Committee interes

23、ted in the subject dealt with may participate in this preparatory work. International, governmental and non- governmental organizations liaising with the IEC also participate in this preparation. IEC collaborates closely with the International Organization for Standardization (ISO) in accordance wit

24、h conditions determined by agreement between the two organizations. 2) The formal decisions or agreements of IEC on technical matters express, as nearly as possible, an international consensus of opinion on the relevant subjects since each technical committee has representation from all interested I

25、EC National Committees. 3) IEC Publications have the form of recommendations for international use and are accepted by IEC National Committees in that sense. While all reasonable efforts are made to ensure that the technical content of IEC Publications is accurate, IEC cannot be held responsible for

26、 the way in which they are used or for any misinterpretation by any end user. 4) In order to promote international uniformity, IEC National Committees undertake to apply IEC Publications transparently to the maximum extent possible in their national and regional publications. Any divergence between

27、any IEC Publication and the corresponding national or regional publication shall be clearly indicated in the latter. 5) IEC itself does not provide any attestation of conformity. Independent certification bodies provide conformity assessment services and, in some areas, access to IEC marks of confor

28、mity. IEC is not responsible for any services carried out by independent certification bodies. 6) All users should ensure that they have the latest edition of this publication. 7) No liability shall attach to IEC or its directors, employees, servants or agents including individual experts and member

29、s of its technical committees and IEC National Committees for any personal injury, property damage or other damage of any nature whatsoever, whether direct or indirect, or for costs (including legal fees) and expenses arising out of the publication, use of, or reliance upon, this IEC Publication or

30、any other IEC Publications. 8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publications is indispensable for the correct application of this publication. 9) Attention is drawn to the possibility that some of the elements of this IEC Publication may

31、 be the subject of patent rights. IEC shall not be held responsible for identifying any or all such patent rights. International Standard IEC 60454-2 has been prepared by IEC technical committee 15: Solid electrical insulating materials. This third edition cancels and replaces the second edition pub

32、lished in 1994, and constitutes a technical revision. This revision includes improved text regarding the flame test (Clause 20), the improved text on adhesion (Clause 11) and a new Figures 9a and 9b. The text of this standard is based on the following documents: FDIS Report on voting 15/377/FDIS 15/

33、387/RVD Full information on the voting for the approval of this standard can be found in the report on voting indicated in the above table. 6 60454-2 IEC:2007(E) This publication has been drafted in accordance with the ISO/IEC Directives, Part 2. A list of all the parts in the IEC 60454 series, unde

34、r the general title Pressure-sensitive adhesive tapes for electrical purposes, can be found on the IEC website. The committee has decided that the contents of this publication will remain unchanged until the maintenance result date indicated on the IEC web site under “http:/webstore.iec.ch“ in the d

35、ata related to the specific publication. At this date, the publication will be reconfirmed; withdrawn; replaced by a revised edition, or amended. A bilingual version of this publication may be issued at a later date. The contents of the corrigendum of December 2009 have been included in this copy. 6

36、 60454-2 IEC:2007(E) This publication has been drafted in accordance with the ISO/IEC Directives, Part 2. A list of all the parts in the IEC 60454 series, under the general title Pressure-sensitive adhesive tapes for electrical purposes, can be found on the IEC website. The committee has decided tha

37、t the contents of this publication will remain unchanged until the maintenance result date indicated on the IEC web site under “http:/webstore.iec.ch“ in the data related to the specific publication. At this date, the publication will be reconfirmed; withdrawn; replaced by a revised edition, or amen

38、ded. A bilingual version of this publication may be issued at a later date. The contents of the corrigendum of December 2009 have been included in this copy. 60454-2 IEC:2007(E) 7 PRESSURE-SENSITIVE ADHESIVE TAPES FOR ELECTRICAL PURPOSES Part 2: Methods of test 1 Scope This part of IEC 60454 specifi

39、es methods of test for pressure-sensitive adhesive tapes for electrical purposes. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the

40、referenced document (including any amendments) applies. IEC 60216-1:2001, Electrical insulating materials Properties of thermal endurance Part 1: Ageing procedures and evaluation of test results IEC 60216-2:2005, Electrical insulating materials Thermal endurance properties Part 2: Determination of t

41、hermal endurance properties of electrical insulating materials Choice of test criteria IEC 60216-3:2006, Electrical insulating materials Thermal endurance properties Part 3: Instructions for calculating thermal endurance characteristics IEC 60243-1:1998, Electrical strength of insulating materials T

42、est methods Part 1: Tests at power frequencies IEC 60426:1973, Test methods for determining electrolytic corrosion with insulating materials IEC 60454-3 (all parts), Pressure-sensitive adhesive tapes for electrical purposes Part 3: Specifications for individual materials IEC 60589:1977, Methods of t

43、est for the determination of ionic impurities in electrical insulating materials by extraction with liquids ISO 383: 1976, Laboratory glassware Interchangeable conical ground joints ISO 527-3:1995, Plastics Determination of tensile properties Part 3: Test conditions for films and sheets ISO 2194:199

44、1, Industrial screens Woven wire cloth, perforated place and electroformed sheet Designation and nominal sizes of openings ISO 3071:2005, Textiles Determination of pH of the aqueous extract ISO 3599:1976, Vernier callipers reading to 0,1 and 0,05 mm ISO 10093:1998, Plastics Fire tests Standard ignit

45、ion sources EN 1939:2003, Self-adhesive tapes Determination of peel adhesion properties (The peel adhesion test method of Clause 11 is based on test method A of EN 1939:2003. This standard is the result of the harmonisation of AFERA 5001 and PSTC-1,2,3 and 4, ASTM 3330/D, ASTM 3330/M and agreed by J

46、ATMA.) NOTE EN: European Norm (Europe) AFERA: Association des fabricants europens de rubans auto-adhsifs PSTC: Pressure sensitive tape council (USA) ASTM: American society for testing and materials (USA) JATMA: Japanese adhesive tapes manufacturers association. 8 60454-2 IEC:2007(E) 3 Conditioning a

47、nd specimen preparation Unless otherwise specified, rolls are to be conditioned for at least 24 h at (23 2) C and (50 5) % relative humidity and all test procedures are to be carried out in this atmosphere. Remove and discard the three outer turns before taking any test specimens from the conditione

48、d roll. Specimen preparation shall be done with care in a clean environment. Specific specimen preparation details will be included with the appropriate test method. Further conditioning of test specimens may be required. 4 Determination of thickness 4.1 Test apparatus A dead-weight thickness gauge

49、having two ground and concentric circular surfaces, flat within 0,001 mm and parallel to within 0,003 mm. The upper surface shall be 6 mm to 8 mm in diameter and the lower surface larger than the upper one. The upper surface shall move on the axis perpendicular to the two faces. The gauge shall be graduated to read directly to 0,002 mm. The frame of the thic