NAVY MIL-P-82522 C-1990 PROPELLANT JET ENGINE T-H DIMER GRADE RJ-4《RJ-4级喷气式发动机T-H二聚物的推进剂》.pdf

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1、MIL-P-82522C 26 October 1990 Superseding 5 March 1984 MIGP-82522B MILITARY SPECIFICATION PROPELLANT, JET ENGINE, T-H DIMER, GRADE RJ-4 This specification is approved for use by all Departments and Agencies of the Department of Defense. 1.1 Scope. This specification covers one grade of jet engine pro

2、pellant, which is a well defined chemical compound, principally composed of exo- and endo-isomers of tetrahydro- di(methylcyc1opentadiene) (See 6.1). 2. APPLICABLE DOCUMENTS 2.1 Government documents. 2.1.1 Specifications and standards. The following specification and standards form a part of this do

3、cument to the extent specified herein. Unless otherwise specified, the issues of these documents are those listed in the issue of the Department of Defense Index of Specifications and Standards (DODISS) and supplement thereto, cited in the solicitation (see 6.2). SPECIFICATIONS Military MIL-C-4556 M

4、IL-1-2768 6 Coating Kit, Epoxy, For Interior of Steel Fuel Tanks Inhibitor, Icing, Fuel System Feder al PPP-D-729 Drums, Metal, 55-Gallon (For Shipment of Non-corrosive Materials) STANDARDS Military MIL-STD-290 Packaging, Packing, and Marking of Petroleum and Related Products Beneficial comments (re

5、commendations, additions, deletions) and any pertinent data which may be of use in improving this document should be addressed to: Naval Air Systems Command, AIR-5363, Washington, DC 20361-5360, by using the Standardization Document Improvement Proposal (DD Form 1426) appearing at the end of this do

6、cument or by letter. AMSC NIA DISTRIBUTION STATEMENT A, FSC 9135 Approved for public release; distribution is unlimited. Licensed by Information Handling ServicesMIL-P-82522C 71 MIL-P-82522C MIL-STD-1189 Standard Symbology for Marking Unit Packs Federal FED-STD-3 13 FED-STD-791 Material Safety Data

7、Sheets Preparation and Submission of Lubricant, Liquid Fuel and Related Products, Method of Testing (Unless otherwise indicated, copies of federal and military specifications, standards, and handbooks are available from the Standardization Documents Order Desk, Bldg 4D, 700 Robins Avenue, Philadelph

8、ia, PA 191 11-5094.) 2.1.2 Other Government documents and publications. The following other Government documents and publications form a part of this document to the extent specified herein, Unless otherwise specified, the issues are those cited in the solicitation. 49 CFR 100-199 Department of Tran

9、sportation Rules and Regulations of the Transportation of Explosives and Dangerous Explosives and Dangerous Articles Preparing Hazardous Materials for Military Air Shipments AFR 71-4 (Application for copies should be addressed to the Superintendent of Documents, Government Printing Office, Washingto

10、n, DC 20402.) 2.2 Non-Government publications. The following documents form a part of this specification to the extent specified herein. Unless otherwise specified, the issues of the documents which are DOD adopted shall be those listed in the issue of the DODISS cited in the solicitation. Unless ot

11、herwise specified, the issues of documents not listed in the DODISS shall be the issue of the non-government documents which is current on the date of the solicitation (see 6.2). AMERICAN SOCIETY FOR TESTING ND MATERIALS ASTM D 86 ASTM D 93 ASTM D 130 ASTM D 156 ASTM D 240 ASTM D 381 ASTM D 445 ASTM

12、 D 1266 ASTM D 1298 ASTM D 1655 Distillation of Petroleum Products Flash Point by Pensky-Martens Closed Tester Detection of Copper Corrosion from Petroleum Products by the Copper Strip Tarnish Test Saybolt Color of Petroleum Products (Saybolt Chromometer Method) Heat of Combustion of Liquid Hydrocar

13、bon Fuels by Bomb Calorime ter Test Test for Existent Gum in Fuels by Jet Evaporation Viscosity of Transparent and Opaque Liquids (Kinematic and Dynamic Viscosities) Sulfur in Petroleum Products (Lamp Method) Test for Density, Specific Gravity, or API Gravity of Crude Petroleum and Liquid Petroleum

14、Products by Hydrometer Aviation Turbine Fuels, Specification for 2 Licensed by Information Handling ServicesI ASTM D 2276 ASTM D 2382 ASTM D 2386 ASTM D 2622 ASTM D 3120 ASTM D 3241 ASTM D 3828 ASTM D 4057 ASTM D 4176 ASTM D 5006 ASTM E 29 Tests for Particulate Contaminant in Aviation Turbine Fuels

15、Test for Heat of Combustion of Hydrocarbon Fuels by Bomb Calorimeter (High-Precision Method) Test for Freezing Point of Aviation Fuels Sulfur In Petroleum Products (X-Ray Spectrographic Method) Test for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry Te

16、st for Thermal Oxidation Stability of Aviation Turbine Fuels (JFIOT Procedure) Test Method for Flash Point by Setafash Closed Tester Standard practice for Manual Sampling of Petroleum and Petroleum Products Free Water and Particulate Contamination in Distillate Fuels (Clear and Bright Pass/Fail Proc

17、edures) Standard Method for Determination of Fuel System Icing Inhibitor Content of Hydrocarbon Fuels by Hand Refractometer Recommended Practices for Indicating Which Places of Figures Are To Be Considered Significant in Specified Limiting Values (Application for copies should be addressed to the Am

18、erican Society for Testing and Materials, 1916 Race Street, Philadelphia, PA 19103-1137.) AMERICAN NATIONAL STANDARDS INSTITUTE (ANSI) ANSI 2129.1 American National Standard for the Precautionary Labeling of Hazardous Industrial Chemicals. (Application for copies should be addressed to the American

19、National Standards Institute, 1430 Broadway, New York, NY 10018.) INTEXNATIONAL TRANSPORTATION AGENCIES IATA International Air Transport Association ICA0 International Civil Aviation Organization IMO International Maritime Dangerous Goods Code (Non-Government standards and other publications are nor

20、mally available from the organizations that prepare or distribute the documents. These documents also may be available in or through libraries or other informational services.) 2.3 Order of Precedence. In the event of a conflict between the text of this specification and the references cited herein,

21、 the text of this specification takes precedence. Nothing in this specification, however, supersedes applicable laws and regulations unless a specific exemption has been obtained. 3 Licensed by Information Handling ServicesMIL-P-82522C 93 = 9777906 0457353 b M .I J* MIGP-82522C 3. REQUIREMENTS 3.1 M

22、aterials. Except where otherwise specified herein, RJ-4 fuel shall consist solely of a exo- and endo-isomers of tetrahydrodi(methylcyc1opentadiene) devived via hydrogenation of methylcyclopentadiene dimer. 3.2 x, The chemical and physical requirements of the fuel shall conform to those listed in Tab

23、le I when tested in accordance with the applicable test methods. Requirements contained herein are absolute and are not subject to correction for tolerance of test methods. However, if multiple determinations are made, average results shall be used. For rounding off of significant figures, ASTM E 29

24、 shall apply to all tests required by this specification. 3.3 m. The additives listed shall be used in combination in amounts not to exceed those specified. The type and amount of each additive used shall be reported. 3.3.1 Antioxidant. The fuel shall contain at least 0.5 gram per liter, and not mor

25、e than 1.0 gram per liter of 2,6-ditertiary-butyl-4-methylphenol of which at least two-thirds of the amount present shall have been added to the finished fuel. 3.3.2 Fuel system icing inhibitor. The fuel system icing inhibitor shall conform to MIL-1-27686. 3.4 Material safety data sheets. Material s

26、afety data sheets shall be prepared and submitted in accordance with FED-STD-313. Material safety data sheets shall also be forwarded as specified in 4.7. The propellant shall have no adverse effect on the health of personnel when used for its intended purpose. Questions pertinent to this effect sha

27、ll be referred by the contracting activity to the appropriate departmental medical service who will act as an advisor to the contracting agency (see 4.7 and 6.2e). . 3.5 Workmanship. The finished fuel shall be visually free from undissolved water, sediment or suspended matter and shall be clear and

28、bright when examined according to ASTM 4176. 4. QUALITY ASSURANCE PROVISIONS 4.1 Responsibility for inspection. Unless otherwise specified in the contract or purchase order, the supplier of the fuel is responsible for the performance of all inspection requirements (examinations and tests) as specifi

29、ed herein. Except as otherwise specified in the contractor purchase order, the supplier of the fuel may use his own or any other facilities suitable for the performance of the inspection requirements specified herein, unless disapproved by the Government. The Government reserves the right to perform

30、 any of the inspections set forth in the specification where such inspections are deemed necessary to assure supplies and services conform to prescribed requirements. 4.1.1 Responsibility for compliance. All items must meet all requirements of sections 3 and 5. The inspection set forth in this speci

31、fication shall become a part of the fuel suppliers overall inspection system or quality program. The absence of any inspection 4 Licensed by Information Handling ServicesMILP-82522C 139,500 20.0 No. lb TABLE I CHEMICAL, AND PHYSICAL REQUIREMENTS AND TEST METHODS D 2382 or D 240 D 445 D 130 _ Propert

32、y Color, Saybolt min Distillation: Initial Boiling Point, min O C Fuel Evaporated, 5% “C Fuel Evaporated, 50% OC Fuel Evaporated, 90% “C End Point, max OC Residue, vol percent, max Distillation loss. vol Dercent. max Specific gravity, 60/60 o F, min-max Existent gum, mg/lOO mL, max Thermal stability

33、: Change in pressure drop, mm Hg, max Heater tube deposit visual rating, rnax Sulfur, total, percent wt., rnax Freezing Point. max OC Heat of combustion (net), BTU/gal min at 15C Viscosity, centistokes at -18 O C (O o F) rnax Copper Strip Corrosion classification, rnax Flash point min “C(“F) rnax C(

34、“F) Visual Appearance, clear and bright Particulates, mg/L, max a Antioxidant, concentration, g/L, min-max Fuel system icing inhibitor, % vol, min-max Notes: I/ To be reported, not limited. 3 See paragraph 4.8. Use 0.80-micron membrane filter. ASTM Limit I Method +25 I D 156 I D86 I/ I/ I/ I/ 232 1.

35、5 1.0 0.915-0.930 I D 1298 5.0 I D 381 0.005 I D 2622 or D 3120 -47 I D 2386 I D93 60 (140) 79 (175) I Pass I D 4176 1.0 I D 2276 0.5-1.0 I 0.10-0.15 I D 500 Usethe GME scale. Method 5327 of FED-STD-791 is also acceptable, 5 Licensed by Information Handling ServicesMIL-P-82522C 71 m 777770b 0457353

36、T m z .a MIGP-82522C requirements in the specification shall not relieve the contractor of the responsibility of assuring that all products or supplies submitted to the Government for acceptance comply with all requirements of the contract. Sampling inspection, as part of manufacturing operations, i

37、s an acceptable practice to ascertain conformance to requirements, however, this does aot authorize submission of known defective material, either indicated or actual, nor does it commit the Government to accept defective material. 4.2 Qualitv conformance inspection. The quality conformance inspecti

38、on of the propellant shall consist of tests of samples from 4.4.1 in accordance with Table I and an examination of samples from 4.4.2 for conformance with 4.5.3. Samples shall be labeled completely with the information identifjhg the purpose of the sample, name of product, specification number, lot

39、and batch number, date of sampling and contract number. 4.3 Inspection lot. 4.3.1 Bulk lot. A bulk lot shall consist of an indefinite quantity of a homogeneous mixture of material offered for acceptance in a single isolated container. 4.3.2 Packaged lot. A packaged lot shall consist of an indefinite

40、 number of 55-gallon drums or smaller unit packages of identical size and shape offered for acceptance and filled n from one isolated tank containing a homogenous mixture of material. 4.4 Sampling. 4.4.1 SamDling for verification of product auality. Each bulk or packaged lot of material shall be sam

41、pled for verification of product quality in accordance with ASTM method D 4057. 4.4.2 Samding for examination of filled containers. A random sample of filled containers shall be selected from each lot. The samples shall be examined in accordance with 4.5.3. 4.5 Methods of examinations. 4.5.1 Examina

42、tion of tiroduct. Samples selected in accordance with 4.4.1 shall be visually examined for compliance with 3.5. 4.5.2 Examination of empty containers. Prior to filling, each empty unit container shall be visually inspected for cleanliness and suitability. 4.5.3 Examination of filled containers. Samp

43、les taken as specified in 4.4,2 shall be examined for conformance to IvIL-STD-290 with regard to fill, closure, sealing, leakage, packaging, packing, and markings, Any container having one or more defects under the required fill shall be rejected. 6 Licensed by Information Handling ServicesMIL-P-825

44、22C 4.6 Test methods. 4.6.1 Chemical and physical properties. Tests to determine conformance to chemical and physical requirements shall be conducted in accordance with FED-STD-791, ASTM standards, or in the case of unique requirements, the test procedures as outlined in Table I and described in the

45、 attached Appendices, with the following exceptions: 4.6.1.1 Corrosion. The corrosion test shall be performed in accordance with ASTM method D 130 for Test at 100C for Volatile Materials.“ 4.6.1.2 Thermal stability. 4.6.1.2.1 ASTM D 3241. The thermal stability test shall be conducted using ASTM D 32

46、41 (JFTOT). The heater tube shall be rated visually. 4.6.1.2.2 ASTM D 3241 test conditions. a. Heater tube temperature at maximum point: 300C (572F). b. Fuel system pressure: 3.43 MPa (500 psig). c. Fuel flow rate: 3.0 ml/minute. d. Test duration: 150 minutes. 4.6.1.2.3 Results. The fuel sample is a

47、cceptable if all the following criteria are met: a. The maximum differential pressure across the test filter does not exceed 10 millimeters of mercury. b. The maximum visual rating of the heater tube deposits is a Code 2, and the visual rating of the heater tube shows neither peacock type deposits (

48、code P) nor abnormal type deposits (code A). 4.6.1.2.4 ASTM D 3241 reported data. The following data shall be reported: a. Differential pressure in millimeters of mercury at 150 minutes, or time to differential pressure of 10 millimeters of mercury, whichever comes first. b. Heater tube deposit Visu

49、al Rating Code at the end of the test. 4.6.1.3 Distillation. The distillation test shall be performed in accordance with ASTM D 86 except for the following: a. There shall be no adjustment in heat after the 95% recovery point. b. The time interval from the 5 ml residue to end point shall be less than five minutes. O 7 Licensed by Information Handling ServicesNIL-P-82522C 71 779770b 0457355 3 W MIL-P-82522C 1 Y 0 c. When observed, the decomposition point shall be considered the endpoint. 4.6.1.4 Freeze Point. The freeze point test will be performed in accordance with AST