NAVISTAR MPAPS G-32-2017 Decorative Physical Vapor Deposition (PVD) - Plastics.pdf

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1、 This document is restricted and may not be sent outside Navistar, Inc. or reproduced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability. 2017 by Navistar, Inc. JUNE 2017 Page 1 of 7 NAVISTAR, INC. Material, Parts, and Process Specifications

2、(MPAPS) NUMBER: MPAPS G-32 Former Designation: CEMS D-32 TITLE: Decorative Physical Vapor Deposition (PVD) - Plastics CURRENT REV No.: 1706 DATE: June 2017 WRITTEN/EDITED BY: J. Goldschmidt APPROVED BY: R. Goluch SUPERSEDES: Rev. New June 2013 PRINTED COPIES OF THIS DOCUMENT MUST BE VERIFIED FOR CUR

3、RENT REVISION This specification may involve hazardous materials, equipment, and procedures. This specification does not purport to address all of the safety issues associated with its use. The user is responsible to consult appropriate safety and health practices and to determine the applicability

4、of regulatory limits prior to use. 1.0 APPLICATION This specification applies to decorative physical vapor deposition coatings used on interior or exterior plastics. These parts may be exterior grilles, bumpers, light bezels, nameplates, interior ornaments, knobs, or similar applications. 2.0 SCOPE

5、This specification covers the material requirements of the base plastic, coating requirements, performance requirements, and quality of the finished part, qualification, source approval and quality control. 2.1 Restricted Chemical Substances Effective January 1, 2007, all product supplied to the req

6、uirements of this specification must comply with the requirements of the MPAPS B-50 specification. 3.0 REFERENCE DOCUMENTS Unless otherwise specified, the latest issue of all referenced standards shall apply. The following Specifications, Standards, and Regulations are referenced in this specificati

7、on. Quality System Standard ISO 9001 or TS-16949 ASTM B368 ASTM D1308 CFR Title 29, Part 1910 ASTM B456 ASTM D2247 NAVISTAR Supplier Packing and Shipping Std. D-13 ASTM B604 ASTM D3359 NAVISTAR Engineering Design Std. A-16 ASTM B727 ASTM D4060 NAVISTAR MPAPS B-50 ASTM D523 SAE J400 ASTM B244 ASTM D5

8、70 SAE J2527 4.0 REQUIREMENTS The general plastic family from which the unplated plastic part is molded shall be compatible with the particular PVD process used by the supplier. The plastic part shall be free from visible molding defects, sink marks, weld or flow lines. Unless otherwise specified on

9、 the part drawing, the significant surface finish shall be equal to or better than the No. 2 diamond finish as found in the SPISPE Mold Finish Comparison Kit.* * Available from D-M-E Corporation, 1975 N. 17th Street, Melrose Park, IL - Licensed by Society of Plastic Industry and Society for Plastic

10、Engineers. NUMBER: MPAPS G-32 TITLE: Decorative Physical Vapor Deposition (PVD) - Plastics REVISION: 1706 This document is restricted and may not be sent outside Navistar, Inc. or reproduced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability.

11、 2017 by Navistar, Inc. JUNE 2017 Page 2 of 7 4.1 Coating Requirements PVD Coating systems on plastic parts typically consist of three layers. The first layer applied to the plastic base is an ultraviolet light (UV) curable base coat. The second layer is a thin layer of vapor deposited metal. The th

12、ird layer is a UV resistant, clear, organic, topcoat. The performance requirements given below are expected of the composite coating not individual layers. Systems other than those specified which demonstrate satisfactory performance may be approved by Navistar Materials Engineering Laboratory. 4.2

13、Performance Requirements 4.2.1 Physical Measurements Ref Test Description Test Method(s) Performance Requirement 4.2.1.1 Overall Coating Thickness Use a DeFelsko B/Adv Non-destructive Sonic Gauge Analyzer per ASTM D6132 30 microns 5.0 microns 4.2.1.2 60Gloss ASTM D523 90 min or 8520 4.2.1.3 Crosshat

14、ch Adhesion - Dry ASTM D3359 Method B 5B 4.2.1.4 Crosshatch Adhesion ASTM D3359 Method B 1 hr wet sponge, 1B 4.2.1.5 Humidity Adhesion ASTM D2247 10-minute recovery 24 C 2 C and 50% 5% Relative Humidity. 1000 hours Panel shall be blister free and shall pass Adhesion per ASTM D3359 Test Method A afte

15、r each 250-hour interval. 4.2.1.6 Oven Aging Minimum 5 test panels. Cycle of Thermal Exposure Oven (Air Circulating) Exposure at 180F: 168 Hours Recovery: 1 Hour at Room Temperature Humidity Exposure: 750 Hours (-101, -102) 2 Panels: Pass Humidity Adhesion in 4.2.1.5 2 Panels: Crosshatch Adhesion in

16、 4.2.1.3 and Gravelometer in 4.2.3.2 1 Panel: Control Standard 4.2.1.7 Moisture Cold Cycle Testing: Minimum 3 Panels. Moisture Cycle Exposure 15 Cycles: Humidity Exposure: 24 Hours Cool Box Exposure (-18 C): 20 Hours Room Temperature: 4 Hours 1 Panel: Pass Crosshatch Adhesion in 4.2.1.3 2 Panels: Pa

17、ss 750 Hours of Humidity Exposure 4.2.1.9 Orange Peel BYK - Wave Scan Plus or ACT Orange Peel Standards 8.0 min. 4.2.1.10 Weatherometer/ (Xenon simulation/analysis) MPAPS GT-31 SAE J2527 Gloss retention (48 SPF Suntan Lotion Coffee Cola Armor-All Chewing Tobacco Transmission Fluid DEET (Insect Repel

18、lent)95% Testing of the following reagents per ASTM D1308, Method 3.3.1 utilizing a 75 mm watch glass for 4 hours and at the following temperatures: Armor-All 200F 48 SPF Suntan Lotion 180F DEET (95%) 130F No discoloration, wrinkling, bubbling or delamination. NUMBER: MPAPS G-32 TITLE: Decorative Ph

19、ysical Vapor Deposition (PVD) - Plastics REVISION: 1706 This document is restricted and may not be sent outside Navistar, Inc. or reproduced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability. 2017 by Navistar, Inc. JUNE 2017 Page 5 of 7 4.2.

20、3 Mechanical Durability Ref Test Description Test Method(s) Performance Requirement 4.2.3.1 Taber Abrasion ASTM D4060 500 cycles/mil. Class A Finish 4.2.3.2 Gravelometer Navistar MPAPS GT-Paint, 28 SAE J400 5A/6B, no C or D chips allowed Navistar 4B 4.2.3.3 Thermal Shock A separate sample shall be s

21、ubjected to three complete cycles consisting of the following sequence: 1) 85C (185F) for 30 minutes. 2) -34C (-30F) ethylene glycol/H2O bath for 30 minutes. Parts shall be transferred immediately from one environment to the other with no time allowed between cycles. There shall be no evidence of pl

22、ating and/or plastic failure due to cracks, crazing, blistering, corrosion, and loss of plating adhesion. After completion of the satisfactory number of prescribed thermal cycles and corrosion test, as well as the thermal shock test, parts passing these tests shall be scribed with an “X“ through the

23、 plating to the plastic surface. A strip of adhesive tape (suitable for ASTM D3359 testing) 1.9 cm (3/4 in) wide, shall be applied to the scribed “X“. The tape shall be pulled at 90 to the surface and the part examined for lifting of the plating. Evidence of loss of adhesion shall be cause for rejec

24、tion. NOTE: Test samples are PC/ABS plaques either 4” X 4”, 4” X 6”, or 12” X 12. Some analysis may occur from molded parts. Samples should be cloth wiped to remove airborne particulate material. Coated samples may be aged at Room Temperature at 50% 5% relative humidity prior to onset of analysis. 5

25、.0 QUALITY The plated part shall have a bright or satin finish as specified and a uniform reflective finish. Each plated deposit shall be adherent and free from cracks and foreign material (except for the post nickel strike and the resulting microporous chromium). The surface shall be dense, smooth,

26、 uniform, and free from stains, pinholes, nodules, or any other defects which affect the overall appearance of the plating or its ability to meet the requirements of this specification. 6.0 QUALIFICATION Engineering qualification of sources is required in advance of production shipments. Samples sha

27、ll be accompanied by test data certifying that all requirements of the specification have been met. Suppliers shall submit samples for approval of finish, luster, color and appearance to the Navistar Industrial Design Group. Upon approval, styling master samples denoting the minimum level of accepta

28、ble appearance quality shall be developed and retained by the supplier and the quality department of each using NAVISTAR facility. NUMBER: MPAPS G-32 TITLE: Decorative Physical Vapor Deposition (PVD) - Plastics REVISION: 1706 This document is restricted and may not be sent outside Navistar, Inc. or

29、reproduced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability. 2017 by Navistar, Inc. JUNE 2017 Page 6 of 7 6.1 Quality Control Plan A Quality Control Plan for products supplied to the requirements of this specification will be established by

30、 mutual agreement between NAVISTAR and the supplier. Unless specific exception is noted, the following characteristics, where applicable*, shall be included in the plan as features for management by statistical process control.* * Other characteristics for inclusion in the control plan may be specif

31、ied on the engineering drawing and/or purchase order. * See NAVISTAR Engineering Design Standard A-16 7.0 SOURCE APPROVAL AND QUALITY CONTROL 7.1 Supplier Requirements All suppliers to NAVISTAR are required to be registered to ISO 9001 Quality System Requirements. NAVISTAR will also accept TS-16949

32、registration as long as the supplier can also fulfill all AIAG PPAP (Production Part Approval Process) documentation and approval requirements. Suppliers must maintain their certification with an accredited registrar and must furnish copies of registration certificates to their Corporate Buyer upon

33、request. 7.2 Approval Parts supplied against contracts or purchase orders citing this specification shall be equivalent in all respects to those samples which were approved by the purchaser. No changes in formulation or processing practices are permitted without approval. In the event that changes i

34、n material, properties, processing practices, construction, color, or labeling of the product are required, the supplier shall notify NAVISTAR Materials Engineering and Purchasing and Supplier Development of the proposed change(s). Test data indicating conformance to all requirements of this specifi

35、cation, test samples, and new or amended or updated Material Safety Data Sheet(s) (MSDS), in accordance with CFR Title 29, Part 1910 shall be submitted with the request for change. 7.3 Process Control The supplier shall either, perform and report results of tests on specific lots of parts produced u

36、sing ISO 9001 or TS-16949 guidelines, or provide statistical evidence of the lot having been produced in a state of statistical control and with a process capable of providing all required properties. The part supplier and the quality control manager of the using NAVISTAR plant may determine testing

37、 and reporting requirements on specific products. 8.0 SHIPPING AND HANDLING Shipping and identification shall be in accordance with NAVISTAR Supplier Packing and Shipping Standard D-13. Parts shall be packaged so as to avoid any damage in shipment detrimental to the appearance of the part. NUMBER: M

38、PAPS G-32 TITLE: Decorative Physical Vapor Deposition (PVD) - Plastics REVISION: 1706 This document is restricted and may not be sent outside Navistar, Inc. or reproduced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability. 2017 by Navistar, I

39、nc. JUNE 2017 Page 7 of 7 9.0 DESIGNATION ON DRAWINGS Example of note to use on drawings: PVD per MPAPS G-32 10.0 TECHNICAL INFORMATION For further information related to the technical content of this specification, contact: Suppliers may purchase controlled copies of this specification by contactin

40、g: Materials Engineering and Technology Dept. 10400 W. North Avenue Melrose Park, IL 60160 E-mail: MaterialsEngineeringN IHS Markit Inc. 15 Inverness Way East Englewood CO 80112-5776 Phone: 1-800-854-7179 E-mail: AutomotiveIHS.com Website: http:/ A.0 GENERAL INFORMATION REVISION HISTORY Revision Level Change Approved by Date Approved 1706 Updated to MPAPS format. Changed from D-32 to G-32. Corrected name in title to read Physical not Pressure; editorial changes. Updated reference standards and misc. test criteria. R. Goluch 6/21/2017