KS D 1674-2009 Methods for inductively coupled plasma spectrometric analysis of trace elements in pure gold《高纯金的诱导结合等离子体放射分光法》.pdf

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1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS D 1674 KS D 1674:2009 2009 7 31 http:/www.kats.go.krKS D 1674:2009 : ( ) ( ) () ( ) : (http:/www.standard.go.kr) ： ：2004 3 22 ：2009 7 31 2009-0375 ： ： ( 02-509-7274) (http:/www.kats.go.kr). 10 5 , . KS D 1674:2009 Methods for inductively coupled plasma sp

2、ectrometric analysis of trace elements in pure gold 1 99 % , 0.05 % . 2 . . ( ) . KS D 0404, KS D 2589, KS I 3002, KS L ISO 3851, 1： KS L ISO 1042, KS M 0001, KS M 0032, KS M 8001, KS M 8003, 3 , . 4 . a) KS I 3002 b) 1.19 g/mL c) (1 1) d) (1 2) e) 1.42 g/mL KS D 1674:2009 2 f) (1 2) g) 1.84 g/mL h)

3、 (1 1) i) (1 2) j) 99.999 % . k) (1 000 mg Ag/L) 1.000 g (99.99 % ) (200 mL) , (11) 30 mL . . 1 000 mL , . l) (1 000 mg Pt/L) 1.000 g (99.99 % ) (200 mL) , 30 mL . . (111) 1 000 mL , (111) . m) (1 000 mg Pd/L) (99.95 % ) 1.000 g 10 mL , . 1 000 mL , (111) . n) (1 000 mg Rh/L) (III)(3) 2.56 g (14) 50

4、 mL , (111) 1 000 mL , (111) . o) (1 000 mg Ir/L) (IV)(3) 1.74 g (11) 50 mL . (111) 1 000 mL , (111) . p) (1 000 mg Ru/L) (III)(3) 2.56 g (14) 50 mL . (111) 1 000 mL , (111) . q) (1 000 mg Cu/L) 1.000 g (99.9 % ) (200 mL) , (11) 30 mL . . 1 000 mL , . r) (1 000 mg Cr/L) 1.000 g (99.9 % ) (200 mL) ,

5、(11) 30 mL . . 1 000 mL , . s) (1 000 mg Fe/L) 1.000 g (99.9 % ) (200 mL) , (11) 30 mL . . 1 000 mL , . t) (1 000 mg Mn/L) 1.000 g (99.9 % ) (200 mL) , (11) 20 mL . . 1 000 mL , . u) (1 000 mg Mo/L) 1.84 g ( 4) (200 mL) . 1 000 mL , . . v) (1 000 mg Ni/L) 1.000 g (99.9 % ) (200 mL) KS D 1674:2009 3

6、, (11) 30 mL . . 1 000 mL , . w) (1 000 mg Al/L) 1.000 g (99.99 % ) (200 mL) , (11) 50 mL . . 1 000 mL , . . x) (1 000 mg As/L) 1.000 g (99.9 % ) (200 mL) , (11) 10 mL . . 1 000 mL , . y) (1 000 mg Bi/L) 1.000 g (99.9 % ) (200 mL) , (11) 30 mL . . 1 000 mL , . z) (1 000 mg Ca/L) 2.50 g (200 mL) . 50

7、 mL, (21) 15 mL , . . 1 000 mL , . aa) (1 000 mg Cd/L) 1.000 g (99.9 % ) (200 mL) , (11) 40 mL 10 mL . . 1 000 mL , . ab) (1 000 mg Mg/L) 1.000 g (99.9 % ) (200 mL) , 50 mL (11) 50 mL . . 1 000 mL , . ac) (1 000 mg Pb/L) 1.000 g (99.9 % ) (200 mL) , (11) 30 mL . . 1 000 mL , . ad) (1 000 mg Sb/L) (S

8、bCl3) 1.87 g (200 mL) (21) 53 mL . 1 000 mL , . ae) (1 000 mg Sn/L) (99.9 % ) 1.00 g (100) , 50 mL 50 80 . (11) . 1 000 mL (11) , (11) . af) (1 000 mg Tl/L) 1.12 g (III)(Tl2O3) (200 mL) 10 mL . 1 000 mL , . KS D 1674:2009 4 ag) (1 000 mg Zn/L) 1.000 g (99.9 % ) (200 mL) , (11) 20 mL . . 1 000 mL , .

9、 5 a) KS M 0032 . . b) 1) KS L ISO 385 1 A 0.1 mL 50 mL 2) KS L ISO 1042 A 100 mL, 500 mL, 1 000 mL 3) KS L ISO 1042 A 500 mL 4. f) . 6 a) . b) , , . c) . 7 . 7.1 ( ) 99 % , 0.05 % . Ag, Pt, Pd, Rh, Ir, Ru, Cu, Cr, Fe, Mn, Mo, Ni, Al, As, Bi, Ca, Cd, Mg, Pb, Sb, Sn, Tl, Zn , . 7.2 A( ) 99 % 99.99 %

10、Cr, Mo, Bi, Sb, Sn, Tl . 7.3 B( ) 99 % 99.99 % Ag, Pt, Pd, Cu, Fe, Mn, Ni, Al, As, Ca, Cd, Mg, Pb, Zn . 8 8.1 KS D 1674:2009 5 a) A (50 mg Ag, Pt, Pd, Rh, Ir, Ru, Cu, Cr, Fe, Mn, Mo, Ni/L) Ag, Pt, Pd, Rh, Ir, Ru, Cu, Cr, Fe, Mn, Mo, Ni 1 000 mg/L 25 mL 150 mL 500 mL . b) B (50 mg Al, As, Bi, Ca, Cd,

11、 Mg, Pb, Sb, Sn, Tl, Zn/L) Al, As, Bi, Ca, Cd, Mg, Pb, Sb, Sn, Tl, Zn 1 000 mg/L 25 mL 150 mL1) 500 mL . 8.2 8.2.1 a) 2.000 g 0.001 g (200 mL) . b) 24 mL 6 mL , 100 mL . c) (1 2) . 500 mg 2.000 g . 8.2.2 . , . 8.3 8.3.1 a) A 1) 4. j) 2.000 g 0.001 g 4 (200 mL) . 2) (12) 40 mL 10 , 2 . 3) (12) 40 mL

12、10 , 2 . 4) A8.1 a) 3 2 mL(SA1, 1 mg/L), 6 mL(SA2, 3 mg/ L), 10 mL(SA3, 5 mg/ L) . 5) 24 mL 6 mL , , 3 100 mL (12) . A . b) B 1) 2.000 g 0.001 g 4 (200 mL) . 2) (12) 40 mL 10 , 2 . 3) (12) 40 mL 10 , 2 . 1) , . KS D 1674:2009 6 4) B8.1 b) 3 2 mL(SB1, 1 mg/ L), 6 mL(SB2, 3 mg/ L), 10 mL(SB3, 5 mg/L)

13、. 5) 24 mL 6 mL , , 3 100 mL (12) . B . 8.3.2 , (8.3.1) 1 2 . 8.3.3 (8.1) A B 1 2 , . 1 A 1 nm 2 nm 1 nm 2 nm Ag 338.289 328.068 Cu 324.752 327.393 Pt 265.945 214.423 Cr 284.325 205.560 Pd 340.458 Fe 238.204 259.939 Rh 343.489 Mn 257.610 259.372 Ir 205.220 Mo 202.031 203.845 Ru 349.849 Ni 232.003 23

14、1.604 2 B 1 nm 2 nm 1 nm 2 nm Al 308.215 Pb 217.000 220.353 As 197.197 188.979 Sb 231.146 206.836 Bi 223.061 222.821 Sn 189.927 242.170 Ca 317.933 Tl 276.787 351.954 Cd 226.502 Zn 213.857 202.548 Mg 279.077 285.213 8.4 . (mg/kg)mVA A ： (mg/L) KS D 1674:2009 7 V ： (mL) m ： (g) 9 A( ) 9.1 a) (50 mg Cr

15、, Mo, Bi, Sb, Sn, Tl/L) Cr, Mo, Bi, Sb, Sn, Tl 1 000 mg/L 25 mL 150 mL 500 mL . b) 1) 4 100 mL 9.1 a) 0 mL(SC0, 0 mg/L), 2 mL(SC1, 1 mg/L), 6 mL(SC2, 3 mg/L), 10 mL (SC3, 5 mg/L) . 2) (1 2) . 9.2 a) (2.0000.001) g (250 mL) . b) 24 mL 6 mL . c) (1 1) 10 mL . d) . e) (1 1) 40 mL 100 mL . f) (1 2) . 9.

16、3 , Cr, Mo, Bi, Sb, Sn, Tl 9.1 b) 1 2 , (9.1) . 9.4 . (mg/kg)(g)(mg/L)mVA A ： (mg/L) V ： (mL) m ： (g) 10 B( ) 10.1 a) D(50 mg Ag, Pt, Pd, Cu, Fe, Mn, Ni/L) Ag, Pt, Pd, Cu, Fe, Mn, Ni 1 000 mg/L 25 mL 150 mL 500 mL . KS D 1674:2009 8 b) E(50 mg Al, As, Ca, Cd, Mg, Pb, Zn/L) Al, As, Ca, Cd, Mg, Pb, Zn

17、 1 000 mg/L 25 mL 150 mL 500 mL . 10.2 a) D 1 1) 4 100 mL D 0 mL (SD0, 0 mg/L), 2 mL(SD1, 1 mg/L), 6 mL(SD2, 3 mg/L), 10 mL(SD3, 5 mg/L) . 2) (1 2) . b) E 1 1) 4 100 mL E 0 mL (SE0, 0 mg/L), 2 mL(SE1, 1 mg/L), 6 mL(SE2, 3 mg/L), 10 mL(SE3, 5 mg/L) . 2) (1 2) . 10.3 a) (2.0000.001) g (500 mL) . b) 24

18、 mL 6 mL . . c) . d) 185200 . e) (1 1) 40 mL 100 mL . f) (1 2) . 10.4 10.4.1 D 1 a) 10.2 a) D 1 D . b) D . 10.4.2 E 1 a) 10.2 b) E 1 E . b) E . 11 . (g)(mg/L)(mg/kg)mVA A ： (mg/L) V ： (mL) m ： (g) 135513 7017 (02)60094114 (02)600948878 http:/ KS D 1674:2009 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Methods for inductively coupled plasma spectrometric analysis of trace elements in pure gold ICS 71.040.40 Korean Agency for Technology and Standards http:/www.kats.go.kr