EN ISO 19069-2-2016 en Plastics - Polypropylene (PP) moulding and extrusion materials - Part 2 Preparation of test specimens and determination of properties《塑料-聚丙烯(PP)模塑和挤出材料第2部分 试.pdf

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1、BSI Standards PublicationBS EN ISO 19069-2:2016Plastics Polypropylene (PP) moulding and extrusion materials Part 2: Preparation of test specimens and determination of propertiesBS EN ISO 19069-2:2016 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN ISO 19069-2:20

2、16. It supersedes BS EN ISO 1873-2:2007 which is withdrawn.The UK participation in its preparation was entrusted to Technical Committee PRI/82, Thermoplastic materials.A list of organizations represented on this committee can be obtained on request to its secretary.This publication does not purport

3、to include all the necessary provisions of a contract. Users are responsible for its correct application. The British Standards Institution 2016. Published by BSI Standards Limited 2016ISBN 978 0 580 87191 7 ICS 83.080.20 Compliance with a British Standard cannot confer immunity from legal obligatio

4、ns.This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 March 2016.Amendments issued since publicationDate Text affectedEUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORMEN ISO 19069-2 March 2016 ICS 83.080.20 Supersedes EN ISO 1873-2:2007Englis

5、h Version Plastics - Polypropylene (PP) moulding and extrusion materials - Part 2: Preparation of test specimens and determination of properties (ISO 19069-2:2016) Plastiques - Polypropylne (PP) pour moulage et extrusion - Partie 2: Prparation des prouvettes et dtermination des proprits (ISO 19069-2

6、:2016) Kunststoffe - Polypropylen (PP)-Werkstoffe - Teil 2: Herstellung von Probekrpern und Bestimmung von Eigenschaften (ISO 19069-2:2016) This European Standard was approved by CEN on 23 January 2016. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the con

7、ditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exis

8、ts in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national sta

9、ndards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, S

10、lovenia, Spain, Sweden, Switzerland, Turkey andUnited Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2016 CEN All rights of exploitation in any form and by any means reserv

11、ed worldwide for CEN national Members. Ref. No. EN ISO 19069-2:2016 EBS EN ISO 19069-2:2016EN ISO 19069-2:2016 (E) 3 European foreword This document (EN ISO 19069-2:2016) has been prepared by Technical Committee ISO/TC 61 “Plastics“in collaboration with Technical Committee CEN/TC 249 “Plastics” the

12、secretariat of which is held byNBN. This European Standard shall be given the status of a national standard, either by publication of anidentical text or by endorsement, at the latest by September 2016, and conflicting national standardsshall be withdrawn at the latest by September 2016. Attention i

13、s drawn to the possibility that some of the elements of this document may be the subject ofpatent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patentrights. This document supersedes EN ISO 1873-2:2007. According to the CEN-CENELEC Internal Regulations, the

14、 national standards organizations of thefollowing countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia,Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, L

15、ithuania, Luxembourg, Malta, Netherlands,Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and theUnited Kingdom. Endorsement noticeThe text of ISO 19069-2:2016 has been approved by CEN as EN ISO 19069-2:2016 without anymodification. BS EN ISO 19069-2:2016ISO

16、19069-2:2016(E)Foreword iv1 Scope . 12 Normative references 13 Preparation of test specimens 33.1 General . 33.2 Treatment of the material before moulding 33.3 Injection moulding . 33.4 Compression moulding 34 Conditioning of test specimens . 45 Determination of properties 4Bibliography 8 ISO 2016 A

17、ll rights reserved iiiContents PageBS EN ISO 19069-2:2016ISO 19069-2:2016(E)ForewordISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO t

18、echnical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates clos

19、ely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.The procedures used to develop this document and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In particular the different approval criteria n

20、eeded for the different types of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).Attention is drawn to the possibility that some of the elements of this document may be the subject of paten

21、t rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent rights identified during the development of the document will be in the Introduction and/or on the ISO list of patent declarations received (see www.iso.org/patents).Any trade name used i

22、n this document is information given for the convenience of users and does not constitute an endorsement.For an explanation on the meaning of ISO specific terms and expressions related to conformity assessment, as well as information about ISOs adherence to the WTO principles in the Technical Barrie

23、rs to Trade (TBT), see the following URL: Foreword Supplementary information.The committee responsible for this document is ISO/TC 61, Plastics, Subcommittee SC 9, Thermoplastic materials.This first edition of ISO 19069-2 cancels and replaces the third edition of ISO 1873-2:2007, which has been tech

24、nically revised.ISO 19069 consists of the following parts, under the general title Plastics Polypropylene (PP) moulding and extrusion materials: Part 1: Designation system and basis for specifications Part 2: Preparation of test specimens and determination of propertiesiv ISO 2016 All rights reserve

25、dBS EN ISO 19069-2:2016INTERNATIONAL STANDARD ISO 19069-2:2016(E)Plastics Polypropylene (PP) moulding and extrusion materials Part 2: Preparation of test specimens and determination of properties1 ScopeThis part of ISO 19069 specifies the methods of preparation of test specimens and the test methods

26、 to be used in determining the properties of polypropylene (PP) moulding and extrusion materials. Requirements for handling test material and for conditioning both the test material before moulding and the specimens before testing are given.Procedures and conditions for the preparation of test speci

27、mens and procedures for measuring properties of the materials from which these specimens are made are also given. Properties and test methods which are suitable and necessary to characterize PP moulding and extrusion materials are listed.The properties have been selected from the general test method

28、s in ISO 10350-1. Other test methods in wide use for, or of particular significance to, these moulding and extrusion materials are also included in this part of ISO 19069, as are the designatory properties specified in ISO 19069-1.In order to obtain reproducible and comparable test results, it is ne

29、cessary to use the methods of preparation and conditioning, the specimen dimensions and the test procedures specified herein. Values determined will not necessarily be identical to those obtained using specimens of different dimensions or prepared using different procedures.2 Normative referencesThe

30、 following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 62, Pla

31、stics Determination of water absorptionISO 75-2, Plastics Determination of temperature of deflection under load Part 2: Plastics and eboniteISO 178, Plastics Determination of flexural propertiesISO 179-1, Plastics Determination of Charpy impact properties Part 1: Non-instrumented impact testISO 179-

32、2, Plastics Determination of Charpy impact properties Part 2: Instrumented impact tesISO 293, Plastics Compression moulding of test specimens of thermoplastic materialsISO 294-1, Plastics Injection moulding of test specimens of thermoplastic materials Part 1: General principles, and moulding of mult

33、ipurpose and bar test specimensISO 294-3, Plastics Injection moulding of test specimens of thermoplastic materials Part 3: Small platesISO 294-4, Plastics Injection moulding of test specimens of thermoplastic materials Part 4: Determination of moulding shrinkage ISO 2016 All rights reserved 1BS EN I

34、SO 19069-2:2016ISO 19069-2:2016(E)ISO 527-2, Plastics Determination of tensile properties Part 2: Test conditions for moulding and extrusion plasticsISO 899-1, Plastics Determination of creep behaviour Part 1: Tensile creepISO 1133-1, Plastics Determination of the melt mass-flow rate (MFR) and melt

35、volume-flow rate (MVR) of thermoplastics Part 1: Standard methodISO 1183-1, Plastics Methods for determining the density of non-cellular plastics Part 1: Immersion method, liquid pyknometer method and titration methodISO 1183-2, Plastics Methods for determining the density of non-cellular plastics P

36、art 2: Density gradient column methodISO 1183-3, Plastics Methods for determining the density of non-cellular plastics Part 3: Gas pyknometer methodISO 1628-3, Plastics Determination of the viscosity of polymers in dilute solution using capillary viscometers Part 3: Polyethylenes and polypropylenesI

37、SO 2818, Plastics Preparation of test specimens by machiningISO 4589-2, Plastics Determination of burning behaviour by oxygen index Part 2: Ambient-temperature testISO 6603-2, Plastics Determination of puncture impact behaviour of rigid plastics Part 2: Instrumented impact testingISO 8256, Plastics

38、Determination of tensile-impact strengthISO 10350-1, Plastics Acquisition and presentation of comparable single-point data Part 1: Moulding materialsISO 11357-2, Plastics Differential scanning calorimetry (DSC) Part 2: Determination of glass transition temperature and glass transition step heightISO

39、 11357-3, Plastics Differential scanning calorimetry (DSC) Part 3: Determination of temperature and enthalpy of melting and crystallizationISO 11359-2, Plastics Thermomechanical analysis (TMA) Part 2: Determination of coefficient of linear thermal expansion and glass transition temperatureISO 16152,

40、 Plastics Determination of xylene-soluble matter in polypropyleneISO 20753, Plastics Test specimensIEC 60093, Methods of test for volume resistivity and surface resistivity of solid electrical insulating materialsIEC 60112, Method for the determination of the proof and the comparative tracking indic

41、es of solid insulating materialsIEC 60243-1, Electrical strength of insulating materials Test methods Part 1: Tests at power frequenciesIEC 60250, Recommended methods for the determination of the permittivity and dielectric dissipation factor of electrical insulating materials at power, audio and ra

42、dio frequencies including metre wavelengthsIEC 60296, Fluids for electrotechnical applications Unused mineral insulating oils for transformers and switchgearIEC 60695-11-10, Fire hazard testing Part 11-10: Test flames 50 W horizontal and vertical flame test methods2 ISO 2016 All rights reservedBS EN

43、 ISO 19069-2:2016ISO 19069-2:2016(E)ASTM D 5420, Standard Test Method for Impact Resistance of Flat, Rigid Plastic Specimen by Means of a Striker Impacted by a falling Weight (Gardner Impact)3 Preparation of test specimens3.1 GeneralIt is essential that specimens are always prepared using the same p

44、rocedure (either injection moulding or compression moulding), and under the same processing conditions.The procedure to be used for each test method is indicated in Tables 3 and 4 (M = injection moulding, Q = compression moulding).3.2 Treatment of the material before mouldingPre-treatment of the mat

45、erial sample is normally not necessary before moulding.3.3 Injection mouldingInjection-moulded specimens shall be prepared in accordance with ISO 294-1 or ISO 294-3, under the conditions specified in Table 1. It has been found that bar test specimens prepared in accordance with ISO 20753 give better

46、 precision than those injection-moulded directly to their final dimensions, and so the use of this geometry is preferable.An appropriate hold pressure, consistent with the production of blemish-free mouldings, shall be used.Table 1 Conditions for injection moulding of test specimensMaterial Melt tem

47、perature CMould temperature CAverage injection velocitymm/sHold pressure time sTotal cycle time sMFR 1,5 times the original value shall be avoided with such materials. If the MFR increased by more than 1,5 times the original value, the melt temperature shall be lowered, 10C at a time, until the incr

48、ease in MFR is 10 %: test speed 50 mm/min.2.6Stress at breakB2.7Strain at breakB%2.8Tensile creep modulusEtc1ISO 899-1 MPaAt 1 hStrain 0,5 %2.9 Etc103At 1 000 h2.10Flexural modulusEfISO 178 80 10 4 MPa Test speed 2 mm/min.2.11Charpy impact strengthcUISO 179-1orISO 179-280 10 4kJ/m2Edgewise impact, m

49、ethod 1eU.Also record type of failure.2.12Charpy notched impact strengthcA80 10 4Machined V-notch,r = 0,25Edgewise impact, method 1eA.Also record type of failure.2.13Tensile notched impact strengthtlISO 825680 10 4Machined doubleV-notch,r = 1kJ/m2Only to be quoted if frac-ture cannot be obtained with notched Charpy test. ISO 2016 All rights reserved 5BS EN ISO 19069-2:2016ISO 19069-2:2016(E)Property Symbol Standard Spec