DLA O-B-41 H-2010 BATTERY WATER.pdf

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1、Beneficial comments, recommendations, additions, deletions, clarifications, etc. and any data that may improve this document should be sent to: STDZNMGTdla.mil or Defense Logistics Agency Aviation VEB, 8000 Jefferson Davis Highway, Richmond, VA 23297-5616. Since contact information can change, you m

2、ay want to verify the currency of this address information using the ASSIST database at https:/assist.daps.dla.mil/. AMSC N/A FSC 6810 METRIC O-B-41H 16 November 2010 SUPERSEDING O-B-41G 31 May 2005 FEDERAL SPECIFICATION BATTERY WATER The General Services Administration has authorized the use of thi

3、s federal specification by all federal agencies. 1. SCOPE AND CLASSIFICATION 1.1 Scope. This specification covers one type of battery water that is used in lead-acid storage batteries. 2. APPLICABLE DOCUMENTS 2.1 Other publications. The following documents form a part of this specification to the ex

4、tent specified herein. Unless a specific issue is identified, the issue in effect on the date of invitation for bids or request for proposal shall apply. ASTM International ASTM D511 - Standard Test Methods for Calcium and Magnesium In Water ASTM D512 - Standard Test Methods for Chloride Ion In Wate

5、r ASTM D1068 - Standard Test Methods for Iron in Water ASTM D1193 - Standard Specification for Reagent Water ASTM D1426 - Standard Test Methods for Ammonia Nitrogen In Water ASTM D1688 - Standard Test Methods for Copper in Water ASTM D1886 - Standard Test Methods for Nickel in Water Provided by IHSN

6、ot for ResaleNo reproduction or networking permitted without license from IHS-,-,-O-B-41H 2 ASTM International - Continued ASTM D6317 - Standard Test Method for Low Level Determination of Total Carbon, Inorganic Carbon and Organic Carbon in Water by Ultraviolet, Persulfate Oxidation, and Membrane Co

7、nductivity Detection (Private sector and civil agencies may purchase copies of these voluntary standards from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959. Electronic copies may be obtained from http:/www.astm.org/.) Waters Corporation Method B-1011 - Th

8、e Determination of Nitrite and Nitrate in Water Using Single Column Ion Chromatography 980896 - Anion Analysis Using Hydroxide Eluent and Indirect Conductivity Detection and EPA Method B-1011 for Nitrite and Nitrate Using UV Detection (Private sector and civil agencies may purchase copies of these v

9、oluntary standards from Waters Corporation, 34 Maple Street, Milford, MA 01757. Electronic copies may be obtained from http:/ 3. REQUIREMENTS 3.1 Physical characteristics. The battery water shall be clear, colorless, odorless, and free from suspended matter and sediment when tested as specified in 4

10、.3.1.1. 3.2 Impurities. The battery water shall conform to the maximum allowable impurity requirements shown in table I when tested in accordance with the applicable test paragraphs and test standards listed in table I. TABLE I. Maximum allowable impurities. Impurity Maximum (mg/L)1Test paragraph Te

11、st standard Total solids 100 4.3.1.2 ASTM D63172Organic and volatile matter 50 4.3.1.2 ASTM D63172Calcium and magnesium (total) 40 4.3.1.3 ASTM D511 Iron 0.5 4.3.1.4 ASTM D1068 Copper 2.5 4.3.1.5 ASTM D1688 Chloride 5 4.3.1.6 ASTM D512 Nickel 0.2 4.3.1.7 ASTM D1886 Ammonia (as NH4) 8 4.3.1.8 ASTM D1

12、426 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-O-B-41H 3 TABLE I. Maximum allowable impurities - Continued. Impurity Maximum (mg/L)1Test paragraph Test standard Nitrites (as NO2) 5 4.3.1.9 Waters Corp. document 9808962Nitrates (as NO3) 10 4.3.1.

13、10 Waters Corp. document 98089621When specific gravity is unity, the concentration of aqueous solute in milligrams per liter (mg/L) of solution will equal the parts per million (ppm). The concentration in micrograms per liter (g/L) will equal the parts per billion (ppb). When specific gravity is not

14、 equal to unity, mg/L or g/L divided by the specific gravity of the solution will equal ppm or ppb, respectively. 2Test measurements conducted in accordance with the indicated test standards are expressed in g/L and should be converted to the mg/L equivalent using 1 mg/L = 1000 g/L. 4. QUALITY ASSUR

15、ANCE PROVISIONS 4.1 Responsibility for inspection. Unless otherwise specified in the acquisition order (see 6.2), the contractor is responsible for the performance of all inspection requirements (examinations and tests) specified herein. Except as otherwise specified in the acquisition order (see 6.

16、2), the contractor may use his own or any other facilities suitable for the performance of the inspection requirements specified herein, unless disapproved by the Government. The Government reserves the right to perform any of the inspections set forth in this specification where such inspections ar

17、e deemed necessary to ensure supplies and services conform to prescribed requirements. 4.1.1 Responsibility for compliance. All items supplied to the Government shall meet all requirements of sections 3 and 5. The inspection set forth in this specification shall become a part of the contractors over

18、all inspection system or quality program. The absence of any inspection requirements in the specification shall not relieve the contractor of the responsibility of ensuring that all products or supplies submitted to the government for acceptance comply with all requirements of the contract. Sampling

19、 inspection, as part of the manufacturing operations, is an acceptable practice to ascertain conformance to requirements, however, this does not authorize submission of known defective material, either indicated or actual, nor does it commit the Government to accept defective material. 4.1.2 Contrac

20、tor assurance of compliance. The contractors quality program or detailed inspection system shall provide assurance of compliance of all characteristics with the applicable drawing and specification requirements using, as a minimum, the conformance criteria specified herein. 4.1.3 Alternative inspect

21、ion provisions. When specified in the acquisition order (see 6.2), alternative inspection provisions, methods, or equipment such as statistical process control, tool control, and other types of sampling procedures may be used by the contractor when they provide, as a minimum, the level of quality as

22、surance required by the inspection provisions specified herein. Prior to applying such alternative procedures, methods, or equipment, the contractor shall describe them in a written proposal submitted to the Government for evaluation and approval. The contractor shall demonstrate that the effectiven

23、ess of each proposed alternative is equal to or better than the quality assurance provisions specified herein. In cases of dispute as to whether the contractors proposed alternative provides equal quality assurance, the provisions of this Provided by IHSNot for ResaleNo reproduction or networking pe

24、rmitted without license from IHS-,-,-O-B-41H 4 specification shall apply. All approved alternative inspection provisions shall be specifically incorporated into the contractors quality program or detailed inspection system, as applicable. 4.2 Quality conformance inspection. 4.2.1 Lot. A lot shall co

25、nsist of the battery water produced by one manufacturer at one plant from the same materials and under essentially the same manufacturing conditions, provided the operation is continuous. In the event the process is a batch operation, each batch shall constitute a lot (see 6.3.1). 4.2.2 Sampling for

26、 battery water tests. Sampling shall be conducted in accordance with table II. A representative specimen of approximately 0.9 liter (L) shall be removed from each sample container and placed in a suitable clean, dry container labeled to identify the lot and container from which it was taken. TABLE I

27、I. Sampling for battery water tests. Number of containers in a batch or lot Number of samples 1 to 2 Sample 100% 3 to 25 2 26 to 150 3 151 to 1,200 5 1,201 to 7,000 8 7,001 to 20,000 10 over 20,000 20 4.2.3 Inspection procedures for battery water tests. Each sample specimen taken in accordance with

28、4.2.2 shall be tested as specified in 4.3.1. Failure of any test by any inspection shall be cause for rejection of the lot represented. 4.3 Test methods. 4.3.1 Battery water tests. Reagent-grade water meeting the requirements of ASTM D1193 and reagent-grade chemicals shall be used throughout the tes

29、ts. Where applicable, blank determinations shall be run and corrections applied where significant. Unless otherwise specified (see 6.2), acid and base reagents shall be concentrated acids and bases. Tests shall be conducted as specified in 4.3.1.1 through 4.3.1.10. 4.3.1.1 Physical characteristics t

30、est. Pour approximately 50 milliliters (mL) of the well-mixed specimen into a clean, dry, 25 x 150 mm test tube. Immediately examine for odor and then allow to stand for not less than 10 minutes. Examine by transmittance light for clarity, color, suspended matter, and sediment. 4.3.1.2 Total solids

31、and organic and volatile matter. Determine the total solids and organic and volatile matter content of the specimen in accordance with ASTM D6317. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-O-B-41H 5 4.3.1.3 Calcium and magnesium (total). Determ

32、ine the calcium and magnesium content of the specimen in accordance with method A (complexometric titration) of ASTM D511. 4.3.1.4 Iron. Determine the iron content of the specimen in accordance with method A (direct atomic absorption) of ASTM D1068. 4.3.1.5 Copper. Determine the copper content of th

33、e specimen in accordance with method A (direct atomic absorption) of ASTM D1688. 4.3.1.6 Chloride. Determine the chloride content of the specimen in accordance with method C (ion selective electrode) of ASTM D512. 4.3.1.7 Nickel. Determine the nickel content of the specimen in accordance with method

34、 A (direct atomic absorption) of ASTM D1886. 4.3.1.8 Ammonia (as NH4). Determine the ammonia content of the specimen in accordance with method B (ion selective electrode) of ASTM D1426. 4.3.1.9 Nitrites (as NO2). Determine the nitrites content of the specimen in accordance with EPA method B-1011 as

35、described in Waters Corporation document 980896. 4.3.1.10 Nitrates (as NO3). Determine the nitrates content of the specimen in accordance with EPA method B-1011 as described in Waters Corporation document 980896. NOTE: For a complete description of EPA method B-1011, refer to Waters Corporation Meth

36、od B-1011. 5. PACKAGING 5.1 Packaging. The requirements for packaging shall be as specified in the acquisition order (see 6.2). 5.2 Unit quantity. The battery water shall be provided in either 1-gallon or 5-gallon containers, or in bulk quantity as specified in the acquisition order (see 6.2). 6. NO

37、TES INFORMATION FOR GUIDANCE ONLY. (This section contains information of a general or explanatory nature that is helpful, but is not mandatory.) 6.1 Intended use. The battery water is intended for use in lead-acid storage batteries only. 6.2 Acquisition requirements. Acquisition documents should spe

38、cify the following: a. Title, number, revision, and date of this standard. b. Responsibility for inspection, if different (see 4.1). c. Inspection facility, if different (see 4.1). Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-O-B-41H 6 d. Alternat

39、ive inspection, if required (see 4.1.3). e. Acid and base reagents, if other than specified (see 4.3.1). f. Packaging requirements (see 5.1). g. Unit quantity required (see 5.2). 6.3 Definitions. 6.3.1 Batch. A batch is a specific quantity of material that has been manufactured by some unit chemical

40、 process or subjected to some physical mixing operation intended to make the final product substantially uniform. 6.3.2 Specific gravity. Specific gravity is the ratio of the density (mass of a unit volume) of a substance to the density of a given reference material. Specific gravity commonly refers

41、 to relative density with respect to water, which has a specific gravity of unity (1) at 20 C. 6.4 Subject term (key word) listing. Lead-acid Rechargeable Specific gravity Storage Wet cell 6.5 Changes from previous issue. Asterisks are not used in this revision to identify changes with respect to th

42、e previous issue due to the extent of the changes. MILITARY INTERESTS: CIVIL AGENCY COORDINATING ACTIVITY:Custodians: GSA - FAS Army - EA Navy - YD Air Force - 68 DLA - GS Review Activity: Army - AT Preparing Activity: DLA - GS3 (Project 6810-2010-014) NOTE: The activities listed above were interest

43、ed in this document as of the date of this document. Since organizations and responsibilities can change, you should verify the currency of the information above using the ASSIST database at https:/assist.daps.dla.mil/. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-