DLA A-A-59456-1999 FERRIC CHLORIDE ANHYDROUS CRYSTALLINE TECHNICAL《工业水晶无水氯化铁》.pdf

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1、A-A-5445b Sai 9018054 0011134 727 Requirement Water insolubles, as Fe,O, , Percent by weight Minimum Maximum - 4.0 METRIC A-A-59456 18 June 1999 SUPERSEDING 25 February 1975 MIL-F-1458OC COMMERCIAL ITEM DESCRIPTION FERRIC CHLORIDE, ANHYDROUS, CRYSTALLINE, TECHNICAL The General Services Administratio

2、n has authorized the use of this commercial item description for all federal agencies. 1. SCOPE. This commercial item description (CID) covers one technical grade of crystalline anhydrous ferric chloride. It is intended for use in water purification. 2. SALIENT CHARACTERISTICS 2.1 Chemical compositi

3、on. The anhydrous ferric chloride shall conform to table I when tested as follows: TABLE I. Chemical composition. Ferrous chloride (FeCl,) - Ferric chloride FeC1,) I 95.5 Beneficial comments, recommendations, additions, deletions, clarifications, etc., and any data which may improve this document sh

4、ould be sent by letter to: Defense Supply Center Richmond (DSCR), ATTN: DSCR-VBD, 8000 Jefferson Davis Highway, Richmond, VA 23297-56 1 O. AMSC N/A DISTRIBUTION STATEMENT A. Approved for public release; distribution is unlimited. FSC 68 1 O Provided by IHSNot for ResaleNo reproduction or networking

5、permitted without license from IHS-,-,-A-A-5945b 111 9018054 0011135 663 5 A-A-59456 2.1.1. Water insolubles. Without undue exposure to air, transfer 4 to 5 grams of ferric chloride to a tared weighing bottle, using a clean paper funnel to prevent ferric chloride from coming in contact with the grou

6、nd joint. Stopper the bottle immediately, and reweigh the bottle and contents. Wash the specimen into a 500 milliliter (mL) volumetric flask with water, cool to approximately 25 OC, and fill the bottle to the mark with water and shake by hand. Allow the contents to settle for about 10 minutes and th

7、en vacuum filter approximately 425 mL of the solution through a tared Gooch crucible, containing an acid-washed asbestos pad, into a dry vacuum flask. Remove the flask containing the filtrate and save the filtrate for succeeding analyses. Replace the vacuum flask with another vacuum flask and filter

8、 the remaining solution. Wash the flask with water and add washings to the Gooch crucible. Repeat the washing procedure six times, allowing the filter to pull dry between each washing. Wash the precipitate once with ethyl alcohol. Dry the crucible and precipitate for 30 minutes at 100 OC, heat for 1

9、5 minutes at 600 OC, cool in a desiccator to room temperature, and reweigh. All weighings shall be to the nearest milligram (mg). Calculate the percent water insolubles as follows: Percent water insolubles = 1 O0 A B Where A = Weight of precipitate (weight of crucible with asbestos pad and precipita

10、te minus weight crucible with asbestos pad), and B = Weight of sample (weight of weighing bottle and sample minus weight of weighing bottle). 2.1.2 Ferrous chloride (FeCl,). A sample of the filtrate from 2.1.1 shall have the percentage of ferrous chloride determined 6 accordance with the procedures

11、of the American Water Works Association (AWWA) Standard for Liquid Ferric Chloride, ANSUAWWA B407. 2.1.3 Ferric chloride (FeCl3. A sample of the filtrate from 2.1.1 shall have the percentage of total iron determined, and subsequently the percentage of ferric chloride calculated, when tested in accor

12、dance with the procedures of ANSUAWWA B407. 2.2 Impurities. The ferric chloride supplied shall be certified as suitable for contact with or treatment of drinking water in accordance with the requirements for impurities given in ANSI/AWWA B407. 3. REGULATORY REQUIREMENTS 3.1 Marking, packaging, and l

13、abeling. Material shall be labeled, packed, and marked in accordance with Title 49, Code of Federal Regulations (CFR) paragraphs 100 to 185. . 3.2 Recycled materials. The offeror/contractor is encouraged to use recovered materials to the maximum extent practical, in accordance with paragraph 23.403

14、of the Federal Acquisition Regulation (FAR). 2 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-A-A-59456 e OLU54 OOLLL3b 5TT 81 A-A-59456 3.3 Material safety data sheet MSDS). The manufacturer shall comply with requirements set forth by the Hazardous

15、 Communications Standard 29 CFR, paragraph 19 1 O. 1200 (d) through (g). 4. QUALITY ASSURANCE PROVISIONS 4.1 Product conformance. The product provided shall meet the salient characteristics of this commercial item description, conform to the producers own drawings, specifications, standards, and qua

16、lity assurance practices, and be the same product offered for sale in the commercial market. The government reserves the right to require proof of such conformance. 4.2 Market acceptability. The item offered must have been sold to the Government or commercial market. 5. PACKAGING. Preservation, pack

17、ing, and marking shall be as specified in the contract or order. 6. NOTES. This section contains information of a general or explanatory nature that is helpful, but is not mandatory. 6.1 Source of documents. 6.1.1 The CFR and FAR may be obtained from the Superintendent of Documents, U.S. Government

18、Printing Office, Washington, DC 20402-0001. 6.1.2 Copies of the AWWA standard may be obtained from the American Water Works Association, 6666 West Quincy Avenue, Denver, CO 80235. 6.1.3 Copies of American National Standards Institute standard may be obtained from the American National Standards Inst

19、itute Inc., 1430 Broadway, New York, NY 1001 8. 6.2 Ordering data. Acquisition documents must speci the following: a. Title, number, and date of this CID. b. Unit and quantity required. c. Packaging requirements (see 5). 6.3 National stock numbers CNSNs). The following NSNs correspond to this CID: 6

20、8 10-00-664-0283 and 68 10-00-682-6677. These may not be indicative of all possible NSNs associated with this document. 3 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-A-A-5945b 70L8054 OOLLL37 q3b A-A-59456 6.4 Source of supply. The following is a

21、 supplier whose products are known to meet the requirements of this CID. Competition is not to be limited to this source. PVS Technologies 10900 Harper Avenue Detroit, MI 4821 3 (313) 571-1 100 MILITARY INTERESTS: Custodians Army - AT Air Force - 68 Navy - YD2 CIVIL AGENCY COORDINATING ACTIVITY: GSA - IOFTE Preparing Activity: DLA - GS (Project 6810-1639) Reviewers Army - MD1, MI Navy - MC 4 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-