CEN TS 17083-2017 Foodstuffs - Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS).pdf
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1、Foodstuffs Determination of acrylamide in food and coffee by gas chromatographymass spectrometry (GCMS)PD CEN/TS 17083:2017BSI Standards PublicationWB11885_BSI_StandardCovs_2013_AW.indd 1 15/05/2013 15:06TECHNICAL SPECIFICATION SPCIFICATION TECHNIQUE TECHNISCHE SPEZIFIKATION CEN/TS 17083 June 2017 I
2、CS 67.050; 67.060; 67.140.20; 67.080.20 English Version Foodstuffs - Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS)Produits alimentaires - Dosage par CG-SM des produits alimentaires et caf avec GC-MS Lebensmittel - Bestimmung von Acrylamid in Lebensmit
3、teln und Kaffee mit Gaschromatographie-Massenspektrometrie (GC-MS) This Technical Specification (CEN/TS) was approved by CEN on 14 May 2017 for provisional application. The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to
4、submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard. CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS available promptly at national level in an appropriate form. It is p
5、ermissible to keep conflicting national standards in force (in parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Es
6、tonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTE
7、E FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2017 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. CEN/TS 17083:2017 ENational fore
8、wordThis Published Document is the UK implementation of CEN/TS 17083:2017.The UK participation in its preparation was entrusted to Technical Committee AW/275, Food analysis - Horizontal methods.A list of organizations represented on this committee can be obtained on request to its secretary.This pub
9、lication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. The British Standards Institution 2017 Published by BSI Standards Limited 2017ISBN 978 0 580 80854 8ICS 67.080.20; 67.060; 67.050; 67.140.20Compliance with a British St
10、andard cannot confer immunity from legal obligations. This Published Document was published under the authority of the Standards Policy and Strategy Committee on 31 August 2017.Amendments/corrigenda issued since publicationDate Text affectedPUBLISHED DOCUMENTPD CEN/TS 17083:2017TECHNICAL SPECIFICATI
11、ON SPCIFICATION TECHNIQUE TECHNISCHE SPEZIFIKATION CEN/TS 17083 June 2017 ICS 67.050; 67.060; 67.140.20; 67.080.20 English Version Foodstuffs - Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS)Produits alimentaires - Dosage par CG-SM des produits alimenta
12、ires et caf avec GC-MS Lebensmittel - Bestimmung von Acrylamid in Lebensmitteln und Kaffee mit Gaschromatographie-Massenspektrometrie (GC-MS) This Technical Specification (CEN/TS) was approved by CEN on 14 May 2017 for provisional application. The period of validity of this CEN/TS is limited initial
13、ly to three years. After two years the members of CEN will be requested to submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard. CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the
14、CEN/TS available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached. CEN members are the national standards bodies
15、of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Sloveni
16、a, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2017 CEN All rights of exploitation in any form and by any means reserved wo
17、rldwide for CEN national Members. Ref. No. CEN/TS 17083:2017 EPD CEN/TS 17083:2017CEN/TS 17083:2017 (E) 2 Contents Page European foreword . 3 1 Scope 4 2 Normative references 4 3 Principle . 4 4 Reagents . 4 5 Standard solution preparation 6 6 Apparatus . 7 7 Procedure. 8 8 GC-MS analysis . 10 9 Cal
18、culating and reporting . 12 10 Test report 12 11 Precision data 13 Annex A (informative) Typical chromatograms 14 Annex B (informative) GC-MS troubleshooting 16 Annex C (informative) Single laboratory validation 18 Annex D (informative) Interlaboratory trial precision data . 20 Bibliography . 22 PD
19、CEN/TS 17083:2017CEN/TS 17083:2017 (E) 3 European foreword This document (CEN/TS 17083:2017) has been prepared by Technical Committee CEN/TC 275 “Food analysis - Horizontal methods”, the secretariat of which is held by DIN. Attention is drawn to the possibility that some of the elements of this docu
20、ment may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent rights. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association. Annexes A, B, C and D are informative. WARNING 1
21、 The use of this Technical Specification can involve hazardous materials, operations and equipment. This document does not purport to address all the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices an
22、d determine the applicability of regulatory limitations prior to use. WARNING 2 Some precaution is required when using polyacrylamide-based plastics because acrylamide may leach from these materials. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the follo
23、wing countries are bound to announce this Technical Specification: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlan
24、ds, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. PD CEN/TS 17083:2017CEN/TS 17083:2017 (E) 4 1 Scope This Technical Specification specifies a method for the determination of acrylamide in cereal-based products, potato-based
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