ASTM D1200-2010(2014) Standard Test Method for Viscosity by Ford Viscosity Cup《采用福特粘度杯的粘度标准试验方法》.pdf

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1、Designation: D1200 10 (Reapproved 2014)Standard Test Method forViscosity by Ford Viscosity Cup1This standard is issued under the fixed designation D1200; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A

2、number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S. Department of Defense.1. Scope1.1 This test method covers the determination of the

3、viscos-ity of Newtonian or near-Newtonian paints, varnishes,lacquers, and related liquid materials with the Ford-type effluxviscosity cup. If the material is non-Newtonian, that is,shear-thinning or thixotropic, Test Method D2196 should beused.1.2 The values stated in SI units are to be regarded as

4、thestandard. The values given in parentheses are for informationonly.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the

5、applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D2196 Test Methods for Rheological Properties of Non-Newtonian Materials by Rotational (Brookfield type)ViscometerE1 Specification for ASTM Liquid-in-Glass Thermometers3. Terminology3.1 Definitions:3.1.1

6、 Newtonian liquid, na liquid in which the viscosity isindependent of the shear stress or shear rate. If the ratio ofshear stress to shear rate is not constant, the liquid is non-Newtonian.3.1.2 Near-Newtonian liquid, na liquid in which thevariation of viscosity with shear rate is small and the effec

7、t onviscosity of mechanical disturbances such as stirring is negli-gible.4. Summary of Test Method4.1 The Ford viscosity cup is filled level full with the liquidunder test, and the time for the material to flow through one ofthe standard orifices is measured.5. Significance and Use5.1 This test meth

8、od is useful for the determination ofpackage and application viscosities of a number of paints andother coatings and in the thinning of these materials, but islimited to Newtonian or near-Newtonian liquids.5.2 There are other types of apparatus for measuring vis-cosity in the laboratory that produce

9、 more accurate results.6. Apparatus6.1 Ford Viscosity CupsNos. 1, 2, 3, 4, and 5 Fordviscosity cups made of corrosion- and solvent-resistant mate-rials assembled as complete units (Note 1), and conforming tothe dimensional requirements shown in Fig. 1. The orificedimensions are considered as a guide

10、 only as the combinationof cup and orifice dimensions must permit conformance to theflow formula for each cup as listed in the Appendix.NOTE 1If the orifice is removed from the cup for any reason the cupshould be recalibrated before use as described in the Appendix.6.2 ThermometerSaybolt Viscosity T

11、hermometer con-forming to the requirements forThermometer 17C (19 to 27C)or 17F (66 to 80F) as prescribed in Specification E1.Inaddition, temperature measuring devices such as non-mercuryliquid-in-glass thermometers, thermocouples, or platinum re-sistance thermometers that provide equivalent or bett

12、er accu-racy and precision, that cover the temperature range forthermometer 17C and 17F, may be used.6.3 Timing DeviceAny timing device may be used pro-viding that the readings can be taken with a discrimination of0.2 s or better.7. Test Specimen7.1 The specimen of the material to be tested shall be

13、 visiblyhomogeneous and free of any foreign material or air bubbles.8. Temperature of Testing8.1 All measurements with the Ford viscosity cups shall bemade at 25C (77F) or a temperature agreed upon between1This test method is under the jurisdiction of ASTM Committee D01 on Paintand Related Coatings,

14、 Materials, andApplications and is the direct responsibility ofSubcommittee D01.24 on Physical Properties of Liquid Paints and Paint Materials.Current edition approved Dec. 1, 2014. Published December 2014. Originallyapproved in 1952. Last previous edition approved in 2010 as D1200 10. DOI:10.1520/D

15、1200-10R14.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Driv

16、e, PO Box C700, West Conshohocken, PA 19428-2959. United States1producer and user. Temperature drift during the test should bekept to a minimum and should not exceed 60.2C (60.4F).NOTE 2 It is impossible to predict the effect of temperature change oneach material with which the apparatus may be used

17、. This factor may beless than 1 % per degree Celsius for some liquids whereas others may beas high as 8 to 10 % per degree Celsius.9. Calibration9.1 Cups should be calibrated in accordance with theprocedure described in Appendix X1. The frequency of thiscalibration check depends upon the amount of u

18、se and the carethat the individual cup receives. If the cup varies more than10 % from standard, it should not be used.10. Conditioning10.1 Bring the material to a temperature a few degreesbelow that desired and then agitate vigorously for 10 min on areciprocating shaker in a pint can two-thirds full

19、. Allow tostand undisturbed for 10 min while adjusting further to thedesired temperature. Make the viscosity determination at theend of the 10-min period.11. Procedure11.1 Make viscosity determinations in a room free of draftsand rapid changes in temperature. For the highest degree ofprecision the r

20、oom temperature should be between 22 and28C (72 and 82F). Determinations should be made at atemperature above the dew point of the atmosphere surround-ing the apparatus.11.2 Choose the proper cup so that the time of efflux will bebetween 20 and 100 s (preferably between 30 and 100 s) forcup Nos. 3,

21、4, and 5; between 55 and 100 s for cup No. 1; andbetween 40 and 100 s for cup No. 2 (Fig. 2).11.3 Level the instrument so that a cup may be filled levelfull without a meniscus or overflow at one side.11.4 Determine the time in seconds of efflux as follows:Close the orifice, for example, by holding a

22、 rubber stopperagainst it. Fill the cup with the prepared specimen. Thepreferred method is to overfill the cup and scrape off the excesswith a straightedge. Pull the stopper away and simultaneouslystart the timing device. Measure the time until the first break inthe stream.11.5 Measure the temperatu

23、re of the fluid in the effluxstream.11.6 If the cup has been established to be nonstandard whencalibrated as described in the Appendix, apply the percentdifference to the measured seconds to get the correctedviscosity in Ford-cup seconds.12. Care of Cup12.1 Following each determination, clean the cu

24、p by the useof a suitable solvent and a soft brush. Under no conditionsshould metal cleaning tools be brought into contact with theinstrument. Particular care must be exercised in cleaning theorifice to avoid any film deposit or nicks on the inside walls.13. Report13.1 Report the following informati

25、on:Orifice A, mm Orifice A, mmNo. 1 1.90 No. 3 3.40No. 2 2.53 No. 4 4.12No. 5 5.20FIG. 1 Ford Viscosity Cup and OrificesFIG. 2 Approximate Viscosity Curves for Ford CupsD1200 10 (2014)213.1.1 The efflux time to the nearest 0.2 s for the cup orificecombination (for example, viscosity 33.2 s with No.

26、4 Fordcup), the temperature of the test specimen (as in the effluxstream), and the immediate history of agitation and rest prior tothe measurement.14. Precision and Bias14.1 PrecisionOn the basis of an interlaboratory test ofthis test method in which eight cooperators from four differentlaboratories

27、 made measurements on five different paints, thewithin-laboratory coefficient of variation was found to be2.8 % with 35 df and the between-laboratory coefficient ofvariation was found to be 6.9 % with 30 df. Based on thesecoefficients, the following criteria should be used for judgingthe acceptabili

28、ty of results at the 95 % confidence level:14.1.1 RepeatabilityTwo results obtained by the sameoperator on different days should be considered suspect if theydiffer by more than 8 %.14.1.2 ReproducibilityTwo results obtained by operatorsin different laboratories should be considered suspect if theyd

29、iffer by more than 20 %.14.2 BiasSince there is no accepted reference materialsuitable for determining bias for the procedure in this testmethod, bias cannot be determined.15. Keywords15.1 flow cup; Ford cup; viscometersFordAPPENDIX(Nonmandatory Information)X1. Calibration Procedure for Ford CupsX1.

30、1 The orifice of the Ford cup is commonly made of brassor some other corrosion-resistant material which is subject towear with use and cleaning. A small change in diameter of theorifice becomes significant in the results obtained with the useof this type of viscosity-measuring apparatus.X1.2 The vis

31、cosity standards3are available only as 1-ptsamples.X1.3 Select the appropriate liquid viscosity standard for thecup to be calibrated (see Table X1.1). Bring this cup and theliquid viscosity standard to a constant temperature as close aspossible to 25.0C (77.0F) or to the operating temperature ofthe

32、cup. Determine the time of efflux to the nearest 0.2 s usingthe procedure detailed in Section 11. Keep the temperature driftto within 60.2C (60.4F). If the temperature is not 77F, theactual temperature must be noted and the viscosity of thestandard oil corrected to this temperature.X1.4 The followin

33、g formulas are used to convert the time offlow in seconds, t, to kinematic viscosity V:V1= 0.49 (t 35.0)V2= 1.44 (t 18.0)V3= 2.31 (t 6.58)V4= 3.85 (t 4.49)V5= 12.1 (t 2.00)where V1, V2, V3, V4, and V5= kinematic viscosity usingorifice No. 1, 2, 3, 4, and 5, respectively, cSt.X1.5 The difference betw

34、een the certified viscosity and thedetermined viscosity, multiplied by 100 and divided by thecertified viscosity, will give the percent variation of the cupfrom standard. A percent correction can be applied to theseconds flow when the cup is in normal use. If the cup variesmore than 10 % from standa

35、rd, it is recommended that theorifice be replaced and that the cup be recalibrated.3Certified kinematic viscosity standards are available from the Cannon Instru-ment Co., P.O. Box 16, State College, Pa. 16801. For particular oils applicable foruse with the Ford Cups refer to Table X1.1. Oils availab

36、le from other sources,having known kinematic viscosities, may also be used.TABLE X1.1 Viscosity Standards Recommended for CalibratingFord Viscosity CupsCupNumberApproximate CupViscosity Range, cStStandard OilDesignationApproximateDesignatedViscosity at77F (25C),cStA1 10to35 S-10 202 25 to 120 S-20 3

37、53 49 to 220 S-60 1204 70 to 370 S-60 1205 200 to 1200 S-200 460AExact viscosities are supplied with the oil samples.D1200 10 (2014)3ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standar

38、d are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif

39、not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, whic

40、h you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,Un

41、ited States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 10 (2014)4