ARMY MIL-O-60371 A-1986 OXAMIDE EXPLOSIVE COMPOSITION《草酰氨混合炸药》.pdf

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1、+ -37-2 - UIL-0-60371A 13 9777706 0337973 5 E MIL-0-6037 1X (AR) 7 March 1986 SUPERSEDING MIL-0-60371 (MU) . 29 June 1966 MILITARY SPECIFICATION OXAMIDE EXPLOSIVE COMPOSITION This Specification is approved for use within the US Army Armament, Munition and Chemical Command and is available for use by

2、 all Departments and Agencies of the Department of Defense. 1. SCOPE 1.1 Scope. This specification covers a high explosive composition designated as Oxamide Explosive intended for use in a bursting charge. 2. APPLICABLE DOCUmNTS 2.1 Government documents. 2.1.1 Specifications-and standards. Unless ot

3、herwise specified, the following specifications and standards of the issue listed in that issue of the Department of Defense Index of Specifications and Standards (DoDISS) specified in the solicitation form a part of this specification to the extent specified herein. a SPECIFICATIONS MIL I TARY MIL-

4、T-248 - Trinitrotoluene (TNT) MIL-C-40 1 - Composition B MIL-W-20553 - Wax, Desensitizing MIL-0-60863 - Oxamide MIL-R-398 - RDX Beneficial comments (rtcommtndatfons, additim, deletions) and any pertinent dita which may be of use in improving this document should be addressed ta Commander, MI Amy Arm

5、ament Research and Development Center, Attn: AMSMC-QA, Dover, New Jnsy 01801-5001 ty usng the self-addressed Standardization Document Improvemsnt Propasal (DD Farn 1426) nppeulng at the end of this document or by letter. AMSC N/A FSC 1376 DISTRIBUTION STATEMENT A. Approved for public release; distri

6、bution is unlimited. a THIS DOCUMENT CONTAINS . / 4 PAGES. 1. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-STANDARDS MILITARY MIL-STD-105 MIL-STD-109 MIL - S T D -. 6 50 MIL-STD-lX68 MIL-STD-1171 MIL-STD-1218 - MIL-STD-1235 - Sampling Procedures a

7、nd Tables for I ns pec t ion by At t r i but es - Quality Assurance Terms and Definitions - Exposives: Sampling, Inspection and Tes ti ng. - Lot Numbering of Ammunition - Acceptable and Description Sheets (for propellants and exposives) - ACS Chemicals - Single and Multilevel Continuous Sampling Pro

8、cedures and Tables for I nspec t ion by Attribut es MIL-0-60371A 13 = 777770b 0337774 7 m MIL-0-60321A (AR) . 2.1.2 Other qovernment documents, drawings, and publications. The following other Government documents, drawings, and publications form a part of this specification to the extent specified h

9、erein. Unless otherwise specified, the issues shall be those in effect on the date of the solicitation. DBAWXNGS US ARMY ARMAMENT RESEARCH AND DEVELOPMENT CENTER (ARDC) 7548644 - Box, Packing for High Explosives, Assembly, Details, Packing and Marking 7548645 - Box, Fiberboard, Packing, Reusable, Co

10、llaps i ble for H igh Explos i ves 9257923 - Box, Fiberboard, Packing, Reusable, Collapsible, for High Explosives, Single P.fiece 49 CFR 100-199 - Department of Transportation Rules and Regulations forthe Transportation of Explosives and Other Danger ou$ Ar ties (The Interstate Commerce Commission R

11、egulations are now a part of Che Code of Federal Regulations, available from the Superintendent of documents, US Government Printing Off ice, Washington, DC 20402.1 (Copies of specifications, standards, drawings and publications, required by manufacturers in connection with specific acquisition func

12、tions should be obtained from the contracting activity or as directed by the contracting officer .) 2 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-c r - MIL-O-60372A 23 777770b 0337775 7 m! - MIL-O-60371A (AR) 2.2 Other publications. The following

13、 other publications form a part of this specification to the extent specified herein. The issue of the documents which are indicated as DoD adopted shall be the issue listed in the current DoDISS and the supplement thereto, if applicable. AMERICAN SOCIETY FOR TESTING AND MATERIALS (ASTM) ASTM Design

14、ation E300 - Recommended Practice for ASTM D2905 - Statement of Number of Sampl ing Indus tr i al Chemicals Specimens Required to Determine the Average Quality of a Textile Material (Application for copies should be addressed to the American Society for Testing and Materials, 1916 Race Street, Phila

15、delphia, PA. 19103.) 2.3 Order of precedence. In the event of a conflict between the text of this specification and the references cited herein, the text of this specification shall take precedence . 3. REQUIREMENTS 3.1 Material. 3.1.1 Made with composition B. The Oxamide Explosive composi- tion sha

16、ll be made with Composition B in accordance with Table I. TABLE I Oxamide explosive composition (with comp B) MATERIAL PERCENT SPECIFICATIONS Composition B . 83.3 2 2.0 MIL-C-401 Type II TNT 6.7 2 0.5 MIL-T-248 Type I Oxamide 10.0 2 0.5 MIL-0-60863 Type I 3.1.2 Made with RDX. The Oxamide explosive c

17、omposition shall be made with RDX in accordance with Table II. TABLE II Oxamide explosive composition (with RDX) MATERIAL PERCENT SPECIFICATIONS RDX 49.5 5 2.0 MIL-R-398 Type I or II TNT 39.6 5 2.0 MIL-T-248 Type I Oxamide 10.0 5 0.5 MIL-0-60863 Type I Class I Wax, Desensitizing 0.9 5 0.5 MIL-W- 2 0

18、 5 53 3.2 Physical and chemical properties. Oxamide Explosive shall conform to the requirements specified in Table III when tested by the applicable test methods. 3 /- Y Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-0-6037LA 13 9999906 0337996

19、O -. MIL-0-60371A (AR) TABLE III Applicable test method composition P ROPE RT Y REQUIREMENT Composition RDX, percent 49.5 -i- 2.0 Oxamide , percent 1a.o ZC 0.5 Wax, percent 0.9 ZC 0.5 Viscosity, effluxc - u TNT, percent 39.6 2 2.0 Moisture, percent, max. O. 25 secont% , max. TEST PARAGRAPH 4.6.3 4.6

20、.1 4.6.2 4,6.2 4.6.4 4.6.5 - i/ To be determined. Report for informational purposes only. 3.3 Data requirements. Description sheets for each lot of Oxamide explosive tested shall be provided to the technical agency in accordance with 4.5 . 3.2 . 3.4 First article inspection. This specification conta

21、ins technical provisions for first article inspection. Requirements for the submission of first article samples by the contractor shall be as specified In the contract (see 4.5). 3.5 Workmanship. The manufacturer shall use procedures and controls which assure that the Composition B produced does not

22、 contain foreign material such as dirt, rust, paint or metal chips, etc., and that the safety and reliability of the explosive are not compromised. Compliance with this requirement shall be as speci- fied in 4.6.6. 4. QUALITY ASSURANCE PROVISIONS 4.1 Responsibility for inspection an standard quality

23、 assurance provisions. Unless otherwise specified in the contract or purchase order, the supplier is responsible for the performance of all inspections specified herein, Except as otherwise specified in the contract or purchase order, the supplier may use his own or any other facilities suitable for

24、. the perfarmance of the inspec- tions specified herein, unless disapproved by the government. The government reserves the right to perform any of the inspections set forth in the specification where such inspections are deemed necessary to assure supplies and services conform to the prescribed requ

25、irements. Reference shall be made to MIL-STD-109 to define terms used herein, 4.2 Process control data. A Process Control Document shall be submitted to the Technical Agency AMCMC-QAR-R (D) in accordance with Data Item Description, DI-P-10392. The document shall contain a description of the process,

26、 all materials used, process condi- tions/procedures and production/inspection equipment used to Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-0-6037LA 13 7779706 0337797 2 W MIL-0-60371A (AR) produce Oxamide Explosive meeting the requirements

27、of this specif i- cation (see 6.2.2). In addition, whenever there is a change (change in source of materials, process conditions, procedures, etc.) from previously reported process control data, the Technical Agency shall be notified of the new process control data and the reason for the change . 4.

28、3 Classification of inspections. The following types of inspections shall be conducted on this item: a. First article inspection (see 4.4). b. Quality conformance inspection (see 4.5). 4.4 First article inspection. 4.4.1 Submission. The contractor shall submit a first article sample as designated by

29、 the contracting officer for evaluation in accordance with provisions of 4.4.2. The first article sample shall be ten (10) pounds of Oxamide explosive. The sample shall be obtained from the first production lot which has been produced by the contractor using the same production processes , procedure

30、s and equipment as will be used in fulfilling the contract. All materials shall be obtained from the same sources of supply as will be used in regular production. 4.4.2 Inspections to be performed. The sample may be subjec- ted by the government to any or all of the examinations and tests specified.

31、 in 4.5 and 4-6 of-this specification and any or all requirements of the applicable drawings. 4.4.3 Rejection., If any sample fails to comply with any of the applicable requirements, the first article quantity shall be rejected. The government reserves the right to terminate its inspection upon any

32、failure of a sample to comply with any of the stated r equ ir emen t c . 4.5 Quality conformance inspection. 4.5.1 Lot formation. A lot shall consist of one or more batches of Oxamide Explosive composition produced by one manufac- turer in accordance with the same specification, and same specifi- ca

33、tion revision under one continuous set of operating conditions. Each lot shall consist of that quantity of Oxamide explosive composition which has been subjected to the same unit chemical or physical process intended to make the final product homogeneous. In addition, each lot shall contain: a.- TNT

34、 fram one interfix lot only, from one manufacturer. b. KDX from one interfix lot only, from one manufacturer. 5 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,- MIL-O-60371A 13 %-7Ob 0337778 L1 a MIL-0-60371A (AR) c . Wax , one type only, from one ma

35、nufacturer 0 d. Oxamide from one lot only, from one manufacturer. The product shall be submitted for inspection in accordance with MIL-STD-105 unless otherwise specified. The criteria and proce- dures for the assignment of lot numbers shall be in accordance with MIL-STD-1168. 4.5.2 Examination. Samp

36、ling plans and procedures for the following classifications of defects shall be in accordance with MIL-STD-105. Contractors sampling plans, if used, shall be approved by the government and shall provide as a minimum, the protection afforded the government by the sampling plans in MIL-STD-105. Contin

37、uous sampling plans in accordance with MIL-STD-1235 may be used if approved by the contracting officer. Also at the option of the contracting officer, AQLs and sampling plans may be applied to the individual characteristics listed, using an AQL of 0.40 percent for each major defect and an AQL of 0.6

38、5 percent for each minor defect. 6 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-a x O a a O .a & a, .a .I4 u- & O c a, a B 2 8 4- - I* e m di a a, cm &O Orl +io &ih Od +i u a, & & O u c .rl Fi a, c .I4 rl u O a, pc 3r B 7 / 4- . Provided by IHSNot

39、 for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-0-60371A 13 W 777770b 0338000 7 m I4 x H rl 8 t I4 a rl m E L o LL O 2- =c O 2 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-O-bO373A 33 m 9777706 0338003 7 m a

40、 c P a - (3 I- r v C U I c: s F I- 8 li 5 oi x O a 5 & m O a LI a, a rci 5 a, d .d 1: :VI M ni m T? a e - O00 mm m lilili lili li * a. . 5 a, C -4 rci a, W a, c O 2 W a, rl a,“ ai 4.c II) a3 II) il u Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-I

41、MIL-0-6037LA 13 9779706 0338002 O W MIL-0-60371A (AR) 4.5.3 Testing. PRECAUTION WARNING This specification covers sampling and testing of toxic or hazardous materials. Accordingly, it is emphasized that all applicable safety rules, regulations and procedures must be followed in handling and processi

42、ng these materials. 4.5.3.1 Samplinq. A representative sample of approximately one kg taken in accordance with ASTM Procedure E300 for solids shall be taken from each batch of Oxamide Explosive. The selection of batches for testing shall be in accordance with MIL-STD-1235, CSP-1 Plan, AQL 6.5%. If a

43、ny sample fails to meet any test requirement, the batch represented by the sample shall be rejected. All batches produced between the time that the last batch was tested and accepted and the batch which failed shall be tested in accordance with the applicable methods given in paragraph 4.6. If any o

44、f these batches fail to meet any of the test requirements, that batch shall also, be rejected. In addition, after any failure of a batch the contractor will return to 100% inspection until iii“ successive batches are accepted in accordance with MIL-STD-1235. Classification of defects shall be as giv

45、en in Table IV. 4.5.3.2 Product testing. Unless otherwise specified, the samples obtained in 4.5.3.1 shall be subjected to the tests listed in Table III. Unless otherwise specified in the contract (see 6.1) the results of the tests shall be reported in accordance with MIL-STD-1171 . TABLE IV. Classi

46、fication of defects I ns pec tion Re qu i r ement Defect Classification Test Method Compos i tion RDX eontent TNT content Qxamide content Wax content Moisture Viscosity Major defect Major defect Major defect 4.6.3 4.6.1 4.6. 2 4.6.2 4.6.4 4.6.5 4.5.4 Inspection equipment. For the performance of all

47、tests and examinations specified in 4.5 and 4.6, commercial inspection equipment should be employed. The contractor shall have available, and utilize correctly, this equipment and is charged with the responsibility of assuring that proper calibration procedures are followed. Government approval of a

48、ll inspection equipment is required prior to its use for acceptance purposes (see 6.3). Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-0-60371A 13 7799906 033003-2 I MIL-0-603 71A (AR) - 4.6 Methods of inspection. The following tests chal1 be pe

49、rformed using prescribed analytical procedures for replicate determinations given in standard analytical textbooks or ASTM Method D2905. Also, unless otherwise specified herein, all chemicals and reagents shall be ACS grade in accordance with MIL-STD-1218 or reagent grade (see 6.2 for use of equivalent test methods) 4.6.1 TNT content. Prepare TNT cal