GBZ T 160.80-2004 工作场所空气有毒物质测定 炸药类化合物.pdf

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1、C 52 GBZ GBZ/T 160.80 2004 Methods for determination of explosives in the air of workplace 2004 5 21 2004 12 1 GBZ/T 160.80 2004 GBZ 1 GBZ 2 Cyclonite,RDX Nitroglycerine Nitroguanidine Cyclotetramethylenetetranitramine Octogen HMX 2004 12 1 GB 16236 1996 A 1996 GBZ/T 160.80 2004 1 2 GBZ 159 3 - 3.1

2、GDX103 3.2 3.2.1 GDX103 100mg/50mg GDX103 3.2.2 0 500ml/min 3.2.3 5ml 3.2.4 10 l 3.2.5 63 Ni 1.5m 3mm OV-17: Chromosorb WAW DMCS = 1.5:100 155 200 200 60ml/min 3.3 3.3.1 GDX103 40 60 GDX103 30min 105 25min 3.3.2 3.3.3 OV-17 3.3.4 Chromosorb WAW DMCS 60 80 3.3.5 25ml 2 2 3 100.0 g/ml 3.4 GBZ 159 GDX1

3、03 200ml/min 15min GDX103 7d 3.5 3.5.1 GDX103 3.5.2 GDX-103 1.0ml 1min 30min 3.5.3 0.0 1.0 2.50 5.0 10.020.0 g/ml 1.0 l 3 ( g/ml) 3.5.4 ( g/ml) 3.6 3.6.1 1 2 93 P V o = V 1 273 + t 101.3 Vo L V L t P kPa 3.6.2 2 c 1+ c 2 v C = 2 V o D C mg/ m 3 c 1 , c 2 g /ml v ml Vo L D 3.7 3.7.1 0.1 g/ml 0.033mg/

4、 m 3 3L 0.1 20g/ml 2.7 5.8 3.7.2 100mgGDX-103 0.6mg 96.6104.2 GDX-103 3.7.3 3.7.4 4 4.1 4.2 4.2.1 0.8 m 4.2.2 40mm 4.2.3 25mm 4.2.4 0 5L/min 4.2.5 5ml 4.2.6 300mm 4.6mm ODS C 18 264nm : 70:30 0.8ml/min 4.3 4.3.1 4.3.2 0.4000g 99.9 100 100ml 4.0mg/ml 100.0g/ml 4.4 GBZ 159 4.4.1 3L/min 15min 4.4.2 1L/

5、min 2 8h 4.4.3 1L/min 2 8h 7d 4.5 4.5.1 4.5.2 2.0ml 50 60min 4.5.3 0.0 10.0 20.0 30.0 40.0 g/ml 10.0 l 3 ( g/ml) 4.5.4 ( g/ml) 4.6 4.6.1 1 4.6.2 3 2 c C = 3 V o C mg/ m 3 c g/ml 2 ml Vo L 4.6.3 GBZ 159 4.7 4.7.1 0.15 g/ml 0.007mg/ m 3 ( 45L ) 0.15 40 g/ml 0.4 6.3 4.7.2 98 99.9 5 5.1 264nm 5.2 5.2.1

6、0.8 m 5.2.2 40mm 5.2.3 25mm 5.2.4 0 5L/min 5.2.5 10ml 5.2.6 5.3 5.3.1 9 V/V 5.3.2 0.4000g 99.9 100 100ml 4.0mg/ml 100.0g/ml 5.4 GBZ 159 5.4.1 3L/min 15min 5.4.2 1L/min 2 8h 5.4.3 1L/min 2 8h 7d 5.5 5.5.1 5.5.2 10.0ml 5060min 5.5.3 7 0.0 0.100.20 0.300.40 0.500.60ml 10.0ml 0.0 10.0 20.0 30.0 40.0 50.

7、0 60.0 g 264nm 3 ( g) 5.5.4 ( g) 5.6 5.6.1 1 5.6.2 4 m C = 4 V o C mg/ m 3 m g Vo L 5.6.3 GBZ 159 5.7 5.7.1 0.1 g/ml 0.013mg/m 3 ( 75L ) 0.1 6 g/ml 3.6 3.8 5.7.2 98 98.3 5.7.3 2 g/ml 6 6.1 RDX 580nm 6.2 6.2.1 6.2.2 40mm 6.2.3 25mm 6.2.4 0 5L/min 6.2.5 25ml 10ml 6.2.6 6.2.7 6.2.8 6.3 6.3.1 6.3.2 20 1

8、.84g/ml 6.3.3 1g 100ml 6.3.4 0.1000g 100ml 1.0mg/ml 10.0 g/ml 6.4 GBZ 159 6.4.1 3L/min 15min 6.4.2 1L/min 2 8h 6.4.3 1L/min 2 8h 7d 6.5 6.5.1 6.5.2 25ml 10.0ml 10min 1.0ml 10ml 6.5.3 6 10ml 0.00.10 0.501.03.0 5.0ml 0.01.05.0 10.030.0 50.0 g 80 1ml 20min5ml 1ml 3ml 25min 580nm 3 ( g) 6.5.4 ( g) 6.6 6

9、.6.1 1 6.6.2 5 1 0 m C = 5 V o C mg/m 3 m g Vo L 6.7 6.7.1 0.1 g/ml 0.022mg/m 3 ( 45L ) 0.1 5 g/ml 1.4 9.1 6.7.2 90.3 95.7 6.7.3 6.7.4 7 7.1 HMX 540nm 7.2 7.2.1 7.2.2 40mm 7.2.3 25mm 7.2.4 0 5L/min 7.2.5 25ml 7.2.6 7.2.7 7.3 7.3.1 7.3.2 20g/L 7.3.3 2.7 V/V 7.3.4 5g 50ml 600ml 0.05g 1000ml 1 7.3.5 0.1000g ( 2 ) 100ml 1.0mg/ml 10.0 g/ml 7.4 GBZ 159 7.4.1 3L/min 15min 7.4.2 1L/min 2 8h 7.4.3 1L/min 2 8h 2 7d 7.5 7.5.1 7.5.2 10.0ml 10min 5.0ml 7.5.3 7 0.0 0.10 0.20 0.50 1.0 2.0 3.0ml 5.0ml 0.0 1.0 2.0 5.0 10.020.0 30.0 g 4.0ml 80 15min 4.0ml