DB45 T 1724-2018 尿中锑的测定石墨炉原子吸收光谱法.pdf

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1、ICSg3g20g22g17g20g19g19g3 g38g3g24g21g3 g3 DB45 g5301g16309g3876g7173g14368g8945g2416g3430g7151g7741g2044g3 DB g23g24g18g55g3g20g26g21g23g258g21g19g20g27g3 g3 g4725g1123g19271g11450g9089g4560g3g11817g3806g9919g2517g4486g2670g7020g1919g16999g8971g3 g39g72g87g72g85g80g76g81g68g87g76g82g81g3g82g73g3g68

2、g81g87g76g80g82g81g92g3g76g81g3g88g85g76g81g72g3g69g92g3g74g85g68g83g75g76g87g72g3g73g88g85g81g68g70g72g3g68g87g82g80g76g70g3g68g69g86g82g85g83g87g76g82g81 g86g83g72g70g87g85g82g80g72g87g85g92g3 g3 g21g19g20g27 g16 g19g23 g16 g21g19g2567g5177 g21g19g20g27 g16 g19g24 g16 g21g19g4564g7155 g5301g16309g

3、3876g7173g14368g8945g2416g17246g18437g6326g7525g11527g11673g4726g3 g3 g3 g2567g5177 g3 g39g37g23g24g18g55g3g20g26g21g23g21g19g20g27g3 g44g3 g2179g3 g3 g16438g3 g7516g7735g2038g6457g10135g42g37g18g55g3g20g17g20g252g21g19g19g28g13577g2090g11444g16372g2121g17319g14713g452g3 g7516g7735g2038g11105g5295g1

4、6303g3870g7167g14362g8939g2410g2459g11087g2748g16849g2114g11087g14050g4100g2696g1354g6656g2090g452g3 g7516g7735g2038g11105g5295g16303g3870g7167g14362g8939g2410g2459g11087g7735g2038g2374g6320g7519g4100g2696g1354g5506g2579g452g3 g7516g7735g2038g1131g16305g17319g14713g2437g1405g726g5295g16303g3870g7167

5、g14362g8939g2410g13948g1098g11253g19554g8939g11844g12454g19602g452g3 g7516g7735g2038g1131g16305g17319g14713g1258g726g16307g2137g7861g451g7550g14739g4175g451g7521g4554g4124g451g21748g1094g7095g451g21748g1072g5174g451g19576g7794g21614g451g19574g7189g7794g451g19990g10245g10245g451g3g3g3g3g3g3g3g3g3g3g3

6、 g7550g4671g14909g451g14022g7861g451g19990g3373g19229g451g4529g6960g14495g451g7550g10245g452 g39g37g23g24g18g55g3g20g26g21g23g21g19g20g27g3 g20g3 g4725g1123g19271g11450g9089g4560g3g11817g3806g9919g2517g4486g2670g7020g1919g16999g8971g3 g20g3 g14649g3370g3 g7516g7735g2038g16372g4554g1206g4719g1117g192

7、65g11444g11811g3800g9913g2511g4480g2664g7014g1913g16993g9083g4554g7145g8965g452g3 g7516g7735g2038g17970g11096g1214g13948g1098g6613g16406g1258g2696g4719g1117g19265g9091g5334g11444g9083g4554g452g3 g21g3 g16378g14649g5725g5451g11102g7101g1324g3 g1083g2119g7095g1318g4649g1214g7516g7095g1318g11444g5316g1

8、1096g7263g5621g1085g2591g4673g11444g452g2065g7263g8984g7189g7503g11444g5445g11096g7095g1318g712g1269g8984g7189g7503g11444g10360g7516g17970g11096g1214g7516g7095g1318g452 g2065g7263g1085g8984g7189g7503g11444g5445g11096g7095g1318g712g1958g7472g7136g10360g7516g708g2357g6428g6256g7481g11444g1566g7017g243

9、7g709g17970g11096g1214g7516g7095g1318g452g3 g42g37g18g55g3g25g25g27g21g3g3g2102g7616g4558g20668g4564g11096g8804g16372g7788g2748g16901g20668g7145g8965g3 g42g37g61g18g55g3g21g28g24g3g3g13948g1098g1258g13780g11087g10393g11521g9083g7145g8965g3g3g5739g2121g3 g22g3 g2517g10812g3 g4719g7783g11096g7458g6393

10、g17994g708g55g85g76g87g82g81g3g59g16g20g19g19g709g9446g9186g12336g18426g2622g712g8984g1941g11811g3800g9913g2511g4480g2374g3224g1117g712g19265g1907g13136g3416g11811g3800g12753g1973g20744g9305g2511g4480 g2374g712g3626g5681g19265g2511g4480g4649g21g20g26g17g25 g3 g81g80g3g11444g10409g5553g16993g13551g17

11、977g6425g5719g2664g7014g712g1958g2664g1913g5334g1644g2748g19265g11444g9091g5334g6208g8595g8708g452g3 g23g3 g16907g2168g2754g7558g7119g3 g23g17g20g3 g19604g2582g7481g16932g7230g3910g712g3416g2102g7616g1117g6256g1455g11096g16901g2162g3447g1130g1352g13527g13535g712g4558g20668g11096g13535g8804g12630g261

12、6g42g37g18g55g3g25g25g27g21g1117g1212g13527g8804g16372g4554g452g3 g23g17g21g3 g9091g11917g18344g712g21g19g729g20g17g23g21g3g74g18g80g47g452g3 g23g17g22g3 g3626g1411g7017g17931g2162g726g11917g18344g19167g712g20g17g19 g3 g74g18g47g452g3 g23g17g23g3 g7735g2038g9446g9186g726g18423g11096g3373g4582g16852g

13、2591g11444g19265g1907g13136g7735g2038g9446g9186g20g19g19g19g17g19 g3 g80g74g18g47g1130g7735g2038g17246g3895g9186g712g1124g11096g2173g11096g11917g18344g9446g9186g11g20g711 g28g28g12g12336g18426g6208g20g19g19g17g19 g3 uni00B5g74g18g47g19265g1907g13136g7735g2038g5316g11096g9186g452g3 g23g17g24g3 g7458g

14、6393g17994g708g55g85g76g87g82g81g3g59g16g20g19g19g709g9446g9186g726g20g711g28g28g28g452g3 g23g17g25g3 g8793g8772g726g13535g5334g1085g1406g1214g28g28g17g28g28g705g452g3 g24g3 g1312g3230g16884g3901g3 g24g17g20g3 g2511g4480g2664g7014g1913g16993g1306g712g1959g7481g11811g3800g9913g451g19265g12458g5619g19

15、556g7601g9887g452g3g3 g24g17g21g3 g4719g8708g18429g6344g4660g16849g712g2102g17880g10679g19g17g19g19g20g452g3 g24g17g22g3 g1959g3726g13962g1161g10015g3713g7113g11046g712g20g19g19 g3 g80g47g727g1959g3726g13962g1161g10015g3713g7113g12753g712g20g17g24 g3 g80g47g452g3 g24g17g23g3 g5598g18431g12331g9186g3

16、224g712g21g19 g3 uni00B5g47g794g21g19g19 g3 uni00B5g47g451g20g19g19 g3 uni00B5g47g794g20 g3 g19g19g19 g3 uni00B5g47g452g3 g24g17g24g3 g4585g18431g11046g712g24g19 g3 g80g47g451g20g19g19 g3 g80g47g452g3 g24g17g25g3 g2155g5334g2664g12753g712g20 g3 g80g47g451g20g19 g3 g80g47g452g3 g3 g39g37g23g24g18g55g

17、3g20g26g21g23g21g19g20g27g3 g21g3 g25g3 g7789g2807g3 g7783g2801g18423g19702g451g17920g17859g2748g1549g4488g451g4719g8708g18429g7920g9083g6457g10135g3g42g37g61g18g55g3g21g28g24g6295g15996g452g3 g26g3 g16907g20674g8603g20698g3 g26g17g20g3 g7783g2801g3892g10806g726g18423g19702g11444g4719g7783g7022g1372

18、6g4564g9305g2622g712g6775g2352g712g2566g4719g7783g19g17g21g19 g3 g80g47g13726g1959g3726g13962g1161g10015g3713g7113g12753g712g2256g1941g19g17g27g19 g3 g80g47 g11444g7458g6393g17994g708g55g85g76g87g82g81g3g59g16g20g19g19g709g9446g9186g1909g2102g9255g2352g452g3 g26g17g21g3 g16901g2162g12458g11437g726g2

19、566g19g17g21 g3 g80g47g13535g8804g1299g7471g4719g7783g712g6457g7783g2801g2620g7783g3892g10806g452g3 g26g17g22g3 g5141g1420g7458g13551g18301g2150g1086g9083g4554g726g2566g24g7007g20g17g24 g3 g80g47g1959g3726g13962g1161g10015g3713g7113g12753g15g2102g2139g2256g1941g19g17g27g19 g3 g80g47g451g19g17g26g19

20、g3 g80g47g451g19g17g25g19 g3 g80g47g451 g19g17g24g19 g3 g80g47g451g19g17g23g19 g3 g80g47g11444g7458g6393g17994g708g55g85g76g87g82g81g3g59g16g20g19g19g709g9446g9186g15g1981g2102g2139g2256g1941g19g17g19 g3 g80g47g451g19g17g20g19 g3 g80g47g451g19g17g21g19 g3 g80g47g451g19g17g22g19 g3 g80g47g451 g19g17g

21、23g19 g3 g80g47g19265g1907g13136g7735g2038g5316g11096g9186g712g2612g2256g19g17g21 g3 g80g47g11444g12458g11437g4719g7783g712g18301g2150g6208g19g17g19g74g18g47g451g20g19g17g19g74g18g47g451g21g19g17g19g74g18g47g451g22g19g17g19g74g18g47g451 g23g19g17g19 g3 g74g18g47g19265g7735g2038g9446g9186g13099g2119g

22、452g2546g10135g1306g3224g9083g4554g7569g1318g712g4662g2511g4480g2664g7014g1913g16993g1306g16947g7076g2144g7472g1443g9083g4554g10470g5681g712g17931g7783g18431g3g3g3g3 g20g19g17g19 g3 g47g712g3626g1411g7017g17931g2162g21g17g19 g3 g47g712g9083g4554g2612g12753g11444g2664g1913g5334g712g2612g12753g2664g19

23、13g5334g11444g2664g1913g5334g1130g13541g3456g7735g712g19265g9091g5334g1130g8282g3456g7735g712 g13576g2150g7735g2038g7458g13551g452g3 g26g17g23g3 g7783g2801g9083g4554g726g6457g10135g1086g13576g2150g5141g1420g7458g13551g11560g2620g11444g7569g1318g9083g4554g16901g7783g11444g2664g1913g5334g452g3 g26g17g

24、24g3 g1306g3224g9083g4554g7569g1318g726g2612g4558g20668g4564g2591g7785g6558g1306g3224g16932g7230g1174g17977g6425g7472g1443g9083g4554g7569g1318g452g2546g13875g11444g1306g3224g9083g4554g7569g1318g16369g16024g20g452g3 g16030g20g3 g1312g3230g9089g4560g7575g1324g3 g1306g3224g7569g1318g3 g11811g3800g9913g

25、7569g1318g3 g8597g20692g3 g9305g5334g708g263g709g3 g2423g9305g3473g5334g708g263g18g86g709g3 g1676g11145g7206g19492g708g86g709g3 g1913g9408g3 g19265g12458g5619g19556g7601g9887g3 g20g451g5282g10261g3 g20g19g19g3 g20g19g3 g20g19g3 g8978g19375g3 g21g20g26g17g25 g3 g81g80g3 g3 g20g21g19g3 g21g19g3 g20g24

26、g3 g9887g11109g9073g3 g27g80g36g3 g3 g20g24g19g3 g24g3 g21g19g3 g10525g13645g3 g19g17g24 g3 g81g80g3 g21g451g9888g2374g3 g20 g3 g22g19g19g3 g22g19g19g3 g20g24g3 g17931g7783g18431g3 g20g19 g3 g996g47g3 g22g451g2511g4480g2374g3 g21 g3 g21g19g19g3 g19g3 g22g3 g14076g7327g7761g8595g3 g3726g7468g3 g23g45

27、1g9269g9031g3 g21 g3 g24g19g19g3 g19g3 g22g3 g27g3 g16907g20674g7078g6564g3898g10812g3 g27g17g20g3 g6457g708g20g709g5439g16849g12743g4719g7783g6546g12743g6208g7735g2038g8708g18429g708g20g17g19g21g19g709g1083g11444g9091g5334g7761g8595g13099g7072g708kg709g726g3 g3g3g3 000.1 000.1020.1 = g4558g9083g870

28、8g18429 k g3g3g3g3g3g3g3 (1) g27g17g21g3 g6457g708g21g709g5439g16849g12743g4719g1117g19265g9091g5334g726g3 = V VC X 1 kg3g3g3g3g3g3g3g3g3g3g3 (2) g5439g1117g726g3 Xg252g4719g7783g1117g19265g11444g9091g5334g712g173g74g18g47g727g3 Cg252g11105g7761g2038g7458g13551g1117g7701g5575g16901g7783g1117g19265g1

29、1444g9091g5334g712g173g74g18g47g727g3 Vg252g6256g2566g4719g7783g11444g1411g12319g712g80g47g727g3 g39g37g23g24g18g55g3g20g26g21g23g21g19g20g27g3 g22g3 1 V g252g2150g3895g2622g16901g7783g11444g1411g12319g712g80g47g727g3 k g252g9091g5334g7761g8595g13099g7072g708g27g17g20g709g452g3 g28g3 g7926g2096g1959

30、0g573g13044g4604g5340g2754g2044g11940g5340g3 g7516g8965g11444g7920g2090g19584g1130g19g17g21 g3 uni00B5g74g18g47g712g4554g18431g1083g19584g1130g19g17g26 g3 uni00B5g74g18g47g712g7472g1406g7920g2090g9091g5334g1130g20g17g19g3 g3 uni00B5g74g18g47g708g6457g12336g18426g24g1597g16849g709g727g11560g4649 g773

31、5g2038g1663g5150g1130g20g17g19g705g794g24g17g22g705g708g81g32g25g709g727g4719g7783g2256g7735g3342g7014g10679g1130g28g19g17g19g705g794g28g27g17g23g705g452g3 g3 g66g66g66g66g66g66g66g66g66g66g66g66g66g66g66g66g66g66g66g66g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g3 g726g1255g800g3486g1056g1430g1677

32、g2296g5940g1696g2996g3221g1101g1 g2123g726g6761g4361g3645g2047g1 g4482g1818g3886g1299g2004g1389g2949g1039g6119g3585g1 g37g35g21g22g16g53g1g18g24g19g21g803g19g17g18g25g1 g2296g5940g1828g3007g5292g3572g1244g6158g6617g2686g3126g4386g4437g2124g4945g694g1278g1156g1 g10366g7545g1097g7487g3g3g1515g7545g5627g12460g3