ISO 1833-11-2006 Textiles - Quantitative chemical analysis - Part 11 Mixtures of cellulose and polyester fibres (method using sulfuric acid)《纺织品 定量化学分析 第11部分 纤维.pdf

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1、 Reference numberISO 1833-11:2006(E)ISO 2006INTERNATIONAL STANDARD ISO1833-11First edition2006-06-01Textiles Quantitative chemical analysis Part 11: Mixtures of cellulose and polyester fibres (method using sulfuric acid) Textiles Analyse chimique quantitative Partie 11: Mlanges de fibres de cellulos

2、e et de polyester (mthode lacide sulfurique) ISO 1833-11:2006(E) PDF disclaimer This PDF file may contain embedded typefaces. In accordance with Adobes licensing policy, this file may be printed or viewed but shall not be edited unless the typefaces which are embedded are licensed to and installed o

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5、inform the Central Secretariat at the address given below. ISO 2006 All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing fr

6、om either ISO at the address below or ISOs member body in the country of the requester. ISO copyright office Case postale 56 CH-1211 Geneva 20 Tel. + 41 22 749 01 11 Fax + 41 22 749 09 47 E-mail copyrightiso.org Web www.iso.org Published in Switzerland ii ISO 2006 All rights reservedISO 1833-11:2006

7、(E) ISO 2006 All rights reserved iiiForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body i

8、nterested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechn

9、ical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by th

10、e technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights

11、. ISO shall not be held responsible for identifying any or all such patent rights. ISO 1833-11 was prepared by Technical Committee ISO/TC 38, Textiles. This first edition of ISO 1833-11 cancels and replaces Clause 10 of ISO 1833:1977. ISO 1833:1977 will be cancelled and replaced by ISO 1833-1, ISO 1

12、833-3, ISO 1833-4, ISO 1833-5, ISO 1833-6, ISO 1833-7, ISO 1833-8, ISO 1833-9, ISO 1833-10, ISO 1833-11, ISO 1833-12, ISO 1833-13, ISO 1833-14, ISO 1833-15, ISO 1833-16, ISO 1833-17, ISO 1833-18 and ISO 1833-19. ISO 1833 consists of the following parts, under the general title Textiles Quantitative

13、chemical analysis: Part 1: General principles of testing Part 2: Ternary fibre mixtures Part 3: Mixtures of acetate and certain other fibres (method using acetone) Part 4: Mixtures of certain protein and certain other fibres (method using hypochlorite) Part 5: Mixtures of viscose, cupro or modal and

14、 cotton fibres (method using sodium zincate) Part 7: Mixtures of polyamide and certain other fibres (method using formic acid) Part 8: Mixtures of acetate and triacetate fibres (method using acetone) Part 9: Mixtures of acetate and triacetate fibres (method using benzyl alcohol) Part 10: Mixtures of

15、 triacetate or polylactide and certain other fibres (method using dichloromethane) Part 11: Mixtures of cellulose and polyester fibres (method using sulfuric acid) Part 12: Mixtures of acrylic, certain modacrylics, certain chlorofibres, certain elastanes and certain other fibres (method using dimeth

16、ylformamide) Part 13: Mixtures of certain chlorofibres and certain other fibres (method using carbon disulfide/acetone) ISO 1833-11:2006(E) iv ISO 2006 All rights reserved Part 14: Mixtures of acetate and certain chlorofibres (method using acetic acid) Part 15: Mixtures of jute and certain animal fi

17、bres (method by determining nitrogen content) Part 16: Mixtures of polypropylene fibres and certain other fibres (method using xylene) Part 17: Mixtures of chlorofibres (homopolymers of vinyl chloride) and certain other fibres (method using sulfuric acid) Part 18: Mixtures of silk and wool or hair (

18、method using sulfuric acid) Part 19: Mixtures of cellulose fibres and asbestos (method by heating) Part 21: Mixtures of chlorofibres, certain modacrylics, certain elastanes, acetates, triacetates and certain other fibres (method using cyclohexanone) The following parts are under preparation: Part 6:

19、 Mixtures of viscose or certain types of cupro or modal or lyocell and cotton fibres (method using formic acid and zinc chloride) Part 20: Mixtures of elastane and certain other fibres (method using dimethylacetamide) Part 22: Mixtures of viscose or certain types of cupro or modal or lyocell and fla

20、x fibres (method using formic acid and zinc chlorate) Part 23: Mixtures of polyethylene and polypropylene (method using cyclohexanone) Part 24: Mixtures of polyester and some other fibres (method using phenol and tetrachloroethane) INTERNATIONAL STANDARD ISO 1833-11:2006(E) ISO 2006 All rights reser

21、ved 1Textiles Quantitative chemical analysis Part 11: Mixtures of cellulose and polyester fibres (method using sulfuric acid) 1 Scope This part of ISO 1833 specifies a method, using sulfuric acid, to determine the proportion of cellulose fibre, after removal of non-fibrous matter, in textiles made o

22、f mixtures of natural and regenerated cellulose fibres and polyester fibre. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the refere

23、nced document (including any amendments) applies. ISO 1833-1, Textiles Quantitative chemical analysis Part 1: General principles of testing 3 Principle The cellulose fibre is dissolved out from a known dry mass of the mixture, with 75 % (mass fraction) sulfuric acid. The residue is collected, washed

24、, dried and weighed; its mass is expressed as a percentage of the dry mass of the mixture. The proportion of cellulose fibre is found by the difference. 4 Reagents Use the reagents described in ISO 1833-1 together with those given in 4.1 and 4.2. 4.1 Sulfuric acid, 75% (mass fraction). A suitable re

25、agent can be prepared by adding carefully, while cooling, 700 ml of concentrated sulfuric acid ( 1,84 g/ml) to 350 ml of distilled water. After the solution has cooled to room temperature, dilute it to 1 I with water. The concentration is not critical within the range 73 % to 77 % (mass fraction) su

26、lfuric acid. 4.2 Ammonia, dilute solution. Dilute 80 ml of concentrated ammonia solution ( 0,880 g/ml) to 1 I with water. ISO 1833-11:2006(E) 2 ISO 2006 All rights reserved5 Apparatus Use the apparatus described in ISO 1833-1 together with those given in 5.1 and 5.2. 5.1 Conical flask, minimum capac

27、ity 500 ml, glass-stoppered. 5.2 Heating apparatus suitable for maintaining the temperature of the flask at (50 5) C. 6 Test procedure Follow the general procedure given in ISO 1833-1, and then proceed as follows. To the specimen contained in the conical flask, add 200 ml of sulfuric acid per gram o

28、f specimen. Insert the stopper and shake the flask carefully to wet out the specimen. Maintain the flask at (50 5) C for 1 h, shaking the flask and contents gently at intervals of about 10 min. Filter the contents of the flask through the weighed filter crucible using suction. Transfer any residual

29、fibres to the crucible by washing out the flask with a little more sulfuric acid. Drain the crucible using suction, and wash the residue on the filter once by filling the crucible with a fresh portion of sulfuric acid. Do not apply suction until the crucible has drained under gravity or stood for 1

30、min. Wash the residue successively several times with cold water, twice with dilute ammonia solution, and then thoroughly with cold water, draining the crucible using suction after each addition. Do not apply suction until each washing liquor has drained under gravity. Finally, drain the crucible us

31、ing suction, dry the crucible and residue, then cool and weigh them. 7 Calculation and expression of results Calculate the results as described in the general instructions of ISO 1833-1. The value of d is 1,00. 8 Precision On a homogeneous mixture of textile materials, the confidence limits of the results obtained by this method are not greater than 1 for the confidence level of 95 %. ISO 1833-11:2006(E) ICS 59.060.01 Price based on 2 pages ISO 2006 All rights reserved