SAE J 2884-2014 Thermoset Elastomer Specification System《热固弹性体的规格体系》.pdf

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1、_SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising theref

2、rom, is the sole responsibility of the user.”SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions.Copyright 2014 SAE InternationalAll rights reserved. No part of this publi

3、cation may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE.TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada)Tel: +1 724-776-4970 (out

4、side USA)Fax: 724-776-0790Email: CustomerServicesae.orgSAE WEB ADDRESS: http:/www.sae.orgSAE values your input. To provide feedbackon this Technical Report, please visithttp:/www.sae.org/technical/standards/J2884_201406SURFACE VEHICLESTANDARDJ2884 JUN2014Issued 2009-09Revised 2014-06Superseding J288

5、4 SEP2009Thermoset Elastomer Specification SystemRATIONALEIncorporate SAE J2979 into SAE J2884.FOREWORDAn alternate to SAE J200. No global equivalent standard exists.1. SCOPEThis document provides a method/procedure for specifying the properties of vulcanized elastomeric materials (natural rubber or

6、 synthetic rubbers, alone or in combination) that are intended for, but not limited to, use in rubber products for automotive applications. This document covers materials that do not contain any re-use; recycled; or regrind materials unless otherwise agreed to by manufacturer and end user. The use o

7、f such materials, including maximum % must be specified using a “Z” suffix.This classification system covers thermoset High Consistency Elastomers (HCEs) only. Thermoplastic Elastomer (TPE) materials are classified using SAE J2558. Silicone Formed In Place Gasket (FIPG) systems such as Room Temperat

8、ure Vulcanized (RTV) Silicones, and Liquid Silicone Rubber (LSR) systems are classified using ASTM F 2468.1.1 PurposeThis classification system is an alternative document to SAE J200.This document utilizes certain elements of SAE J200, SAE J2236 and SAE J2558 along with new elements to build a line

9、call out without the need for laboratory round robins to generate data for table creation/ modification.1.2 Document BasisThe basis for a line call out for any material using this document includes:Elastomer ChemistryMaterial HardnessTensile StrengthElongationContinuous Upper Temperature Resistance

10、(CUTR)IRM 903 Oil Volume Change1.3 Requirements and RecommendationsSAE INTERNATIONAL J2884 Revised JUN2014 Page 2 of 24The creator of a line call out, prior to material testing must have a good grasp of the application requirements and elastomeric material principles. Certain polymer description and

11、 physical property characteristics are required in a line call out and are covered in 1.2 and Section 3. Additional physical property characteristics are discretionary based on the needs of the application, and are covered in Section 4.It is recommended to utilize this document to classify elastomer

12、ic materials for specific applications in order to maintain a minimum length line call out.It is recommended the material manufacturer and the user develop a final line call out for a functioning material based on 30 data points (minimum for statistical analysis) per requirement from 6 different pro

13、duction batch runs minimum for large scale production. Development of a line call out for low volume/ small scale production in which 6 different production batch runs may not be feasible In these cases development may be based on 20 data points per requirement from at least 1 production batch and 3

14、 laboratory lots (or any combination totaling 4 lots, as long as 1 production lot is included). If using this alternative, it is recommended that each production lot be validated to the full line call out prior to use.Production batch runs must be prepared using the production intent equipment param

15、eters (type, size, and other compounding parameters).Test plaques used for physical property evaluations should, as close as possible, mimic the production process, including state of cure.1.4 Example FormatThe format of examples used in each section/subsection lists the basic requirements along wit

16、h the applicable suffix requirement. The examples shall resemble as close as possible, real life materials. The portion of the example to be defined for each subsection are shown in bold print.2. REFERENCES2.1 Applicable DocumentsThe following publications form a part of this specification to the ex

17、tent specified herein. Unless otherwise indicated, the latest issue of SAE publications shall apply.2.1.1 SAE PublicationsAvailable from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.org.SAE J200

18、 Classification System for Rubber MaterialsSAE J369 Flammability of Polymeric Interior Materials - Horizontal Test MethodSAE J1681 Gasoline, Alcohol, and Diesel Fuel Surrogates for Materials TestingSAE J2236 Standard Method for Determining Continuous Upper Temperature Resistance of ElastomersSAE J25

19、58 Classification System for Thermoplastic ElastomersSAE J2665 Test Procedure to Measure the Fuel Permeability of Materials by the Cup Weight Loss MethodSAE J2979 Test Method for Vulcanized Rubber and Thermoplastic Elastomer Determination of Compressive Stress Relaxation (CSR) Response2.1.2 ASTM Pub

20、licationsSAE INTERNATIONAL J2884 Revised JUN2014 Page 3 of 24Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.orgASTM D 297 Test Methods for Rubber Products - Chemical AnalysisASTM D 395 Test Methods for Rubber Pro

21、perty - Compression SetASTM D 412 Test Methods for Vulcanized Rubber and Thermoplastic Elastomers - TensionASTM D 430 Test Methods for Rubber Deterioration - Dynamic FatigueASTM D 471 Test Method for Rubber Property - Effects of LiquidsASTM D 573 Test Method for Rubber Property - Deterioration in Ai

22、r OvenASTM D 624 Test Method for Tear Strength of Conventional Vulcanized Rubber and Thermoplastic ElastomersASTM D 865 Test Method for Rubber - Deterioration by Heating in Air (Test Tube Enclosure)ASTM D 925 Test Methods for Rubber Property - Staining of Surfaces (Contact, Migration, and Diffusion)

23、ASTM D 1053 Test Methods for Rubber Property - Stiffening at Low Temperatures: Flexible Polymers and Coated FabricsASTM D 1149 Test Method for Rubber Deterioration - Surface Ozone Cracking in a ChamberASTM D 1329 Test Method for Evaluating Rubber Property - Retraction at Lower Temperatures (TR Test)

24、ASTM D 1349 Practice for Rubber - Standard Temperatures for TestingASTM D 1418 Practice for Rubber and Rubber Latices - NomenclatureASTM D 2240 Test Method for Rubber Property - Durometer HardnessASTM D 2632 Test Method for Rubber Property - Resilience by Vertical ReboundASTM D 6147 Test Method for

25、Vulcanized Rubber and Thermoplastic Elastomer - Determination of Force Decay (Stress Relaxation) in CompressionASTM D 7426 Standard Test Method for Assignment of the DSC Procedure for Determining Tgof a Polymer or an Elastomeric CompoundASTM F 2468 Specifying Silicone Adhesives and Sealants Transpor

26、tation Applications2.1.3 ISO PublicationAvailable from American National Standards Institute, 25 West 43rd Street, New York, NY 10036-8002, Tel: 212-642-4900, www.ansi.org.ISO 3795 Road vehicles, and tractors and machinery for agriculture and forestryDetermination of burning behaviour of interior ma

27、terials2.1.4 FMVSS PublicationAvailable from the Superintendent of Documents, U.S. Government Printing Office, Mail Stop: SSOP, Washington, DC 20402-9320.FMVSS 302 Flammability of Interior MaterialsSAE INTERNATIONAL J2884 Revised JUN2014 Page 4 of 243. BASIC REQUIREMENTSBasic requirements must be sp

28、ecified in all line call outs. The basic requirements of a line call out contain a series of letters to describe the Elastomer Chemistry followed by 10 numbers to describe the various basic physical properties of the elastomer system. A space must be left between the acronym(s) and 1stnumber set, an

29、d each subsequent number set that is used in describing a property.3.1 Specifying Basic Physical PropertiesBasic requirements must be specified as Non-Zero letters/ values.IRM 903 is the only exception, since non-polar materials are not expected to have resistance to volume swell in non-polar oils s

30、uch as the IRM 903 (also the Fluid Aging Property Change Table in 4.4.3 does allow a “0” indicating “No Requirement”). Polar materials will have a measure of IRM903 oil resistance and must contain a non-zero value.No zeros (0s) may be used as place holders for any other basic requirement.In a line c

31、all out, the aged portion (168 hour volume change in IRM 903 Oil) cannot be modified by suffix requirements (EOC). If used, an EOC suffix requirement is in addition to the basic requirements.3.1.1 Elastomer ChemistryThis is specified using the appropriate acronym(s) as listed in the table in 3.2.3.1

32、.2 Hardness, Type A DurometerExpressed as Points 5 per ASTM D 2240 1stand 2ndnumbers.NOTE: Delay used in readings is a common source of correlation between laboratories. Materials tested and specified using this document must follow ASTM D 2240, which specifies a delay of 1 0.1 seconds as the defaul

33、t delay, unless an alternate delay is agreed on between supplier and user, and specified using a “Z” (i.e. Zn=ASTM D 2240 determined using a 5 second delay).3.1.3 Tensile StrengthExpressed as MPa minimum per ASTM D 412 Die C 3rdand 4thnumbers. For this basic requirement only, tensile requirements le

34、ss than 10 MPa may be expressed using a decimal. As such as a tensile requirement of 8.5 MPa would be allowable, but 11.7 MPa would not, unless done so using a “Z” Special Requirements modifier.3.1.4 Ultimate ElongationExpressed as % minimum per ASTM D 412 Die C 5th, 6th, and 7thnumbers.3.1.5 Contin

35、uous Upper Temperature Resistance (CUTR) as determined per SAE J22368thand 9thnumber representing temperature from the “Aging Duration and Temperature” table in Section 4.3.1.6 IRM 903 Oil Aged Volume ChangeExpressed as % maximum taken from the “Fluid Aging Property Change Table -Volume Change” colu

36、mn in 4.4.3. Material aged for 168 hours at 150 C. If the material CUTR is less than 150 C, the aging shall be done at the CUTR. -10thnumber.SAE INTERNATIONAL J2884 Revised JUN2014 Page 5 of 243.2 Specifying Elastomer ChemistryTable 1 lists the elastomer acronyms per ASTM D 1418 with the correspondi

37、ng reference to their generic material names.TABLE 1 - ASTM D 1418 ACRONYMS AND GENERIC MATERIAL DESCRIPTIONAcronym Elastomer Generic Name Acronym Elastomer Generic NameACM Polyacrylate FKM (3) Vinylidene Fluoride Tetrafluoroethylene Fluorinated Vinyl Ether TerpolymerAEM Ethylene Acrylate FKM (4) Vi

38、nylidene Fluoride Tetrafluoroethylene Propylene TerpolymerAFMU Tetrafluoroethylene Trifluoronitrosomethane Nitrosoperfluorobutyric Acid TerpolymerFKM (5) Hexafluoropropylene Vinylidene Fluoride Tetrafluoroethylene Fluorinated Vinyl Ether Ethylene PentapolymerANR Acrylonitrile Acrylate (Ethyl or othe

39、r) Co-polymerFVMQ Fluoro Vinyl Methyl Silicone (Fluorosilicone Rubber)AU Polyester Urethane FZ FluoroalkoxyphosphazeneBIIR Bromo-Isobutene- Isoprene Rubber GECO Epichlorohydrin Ethylene Oxide Allyl Glycidyl Ether TerpolymerBIMSM Brominated Isobutylene p-Methylstyrene CopolymerGPO Propylene Oxide All

40、yl Glycidyl Ether CopolymerBR Butadiene Rubber HNBR Hydrogenated Acrylonitrile Butadiene RubberCFM Polychloro-Trifluoro-Ethylene IIR Isobutene Isoprene RubberCIIR Chloro-Isobutene-Isoprene Rubber IR Isoprene RubberCM Chloro-Polyethylene MQ Methyl Silicone RubberCO Polychloromethyl Oxirane (Epichloro

41、hydrin)NBR Acrylonitrile Butadiene RubberCR Chloroprene Rubber NIR Acrylonitrile Isoprene CopolymerCSM Chloro-Sulfonyl-Polyethylene NR Natural rubberECO Ethylene Oxide- Chloromethyl Oxirane (Epichlorohydrin Copolymer)NRG Guayule Natural RubberENR Epoxidized Natural Rubber PBR Vinylpyridine Butadiene

42、 CopolymerENRG Epoxidized Guayule Natural Rubber PMQ Phenyl Methyl Silicone RubberEOM Ethylene Octene Copolymer PSBR Vinylpyridine Styrene - Butadiene TerpolymerEOT Ethylene Polysulfide Ether PVMQ Phenyl Vinyl Methyl Silicone RubberEPDM Ethylene Propylene Diene Terpolymer PZ Phenoxyphosphazene Rubbe

43、rEPM Ethylene Propylene Copolymer RBR ReclaimEU Polyether Urethane SBR Styrene Butadiene RubberEVM Ethylene Vinyl Acetate Copolymer SIR Styrene Isoprene RubberFEPM Tetrafluoroethylene Propylene Copolymer; or Tetrafluoroethylene Perfluorinated Vinyl Ether Ethylene TerpolymerT Polysulfide RubberFMQ Fl

44、uoromethyl Silicone VMQ Methyl Silicone RubberFFKM Perfluoroelastomer XBR Carboxylic Butadiene RubberFKM (1) Hexafluoropropylene Vinylidene Fluoride CopolymerXNBR Carboxylic Acrylonitrile - Butadiene RubberFKM (2) Hexafluoropropylene Vinylidene Fluoride Tetrafluoroethylene TerpolymerXSBR Carboxylic

45、Styrene - Butadiene RubberSAE INTERNATIONAL J2884 Revised JUN2014 Page 6 of 243.2.1 Single Elastomer SystemsSingle Elastomer Chemistry Systems are designated by use of one acronym at the beginning of a line call out.Example:EPDM 58 10 275 10 0EPDM = Ethylene Propylene Diene Terpolymer (per Table 1).

46、58 = 58 5 points Type A Hardness ASTM D 2240 Type A.10 = 10 MPa Tensile Strength minimum ASTM D 412 Die C.275 = 275% Ultimate Elongation minimum ASTM D 412 Die C.10 = 150 C CUTR (per the “Aging Duration and Temperature” table in Section 4.) SAE J2236.0 = No Requirement (per the “Fluid Aging Property

47、 Change Table -Volume Change” column in 4.4.3).Example (Showing Tensile less than 10 MPa):EPDM 58 8.5 275 10 0EPDM = Ethylene Propylene Diene Terpolymer (per Table 1).58 = 58 5 points Type A Hardness ASTM D 2240 Type A.8.5 = 8.5 MPa Tensile Strength minimum ASTM D 412 Die C.275 = 275% Ultimate Elong

48、ation minimum ASTM D 412 Die C.10 = 150 C CUTR (per the “Aging Duration and Temperature” table in Section 4.) SAE J2236.0 = No Requirement (per the “Fluid Aging Property Change Table -Volume Change” column in 4.4.3).Example:ACM 55 07 175 10 5ACM = Polyacrylate (per Table 1).55 = 55 5 points Type A H

49、ardness ASTM D 2240 Type A.07 = 7 MPa Tensile Strength minimum ASTM D 412 Die C.175 = 175% Ultimate elongation minimum ASTM D 412 Die C.10 = 150 C CUTR (per the “Aging Duration and Temperature” table in Section 4.) SAE J2236.5 = 25% Volume Change maximum in IRM 903 oil after 168 hours at 150 C (per the “Fluid Aging Property Change Table -Volume Change” column in 4.4.3.) ASTM