SAE AMS 6935B-2015 Titanium Alloy Bars Forgings and Forging Stock 6 0Al C 6 0V C 2 0Sn Solution Heat Treated and Aged (UNS R56620).pdf

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1、_ SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising there

2、from, is the sole responsibility of the user.” SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions. Copyright 2015 SAE International All rights reserved. No part of this p

3、ublication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-497

4、0 (outside USA) Fax: 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your input. To provide feedback on this Technical Report, please visit http:/www.sae.org/technical/standards/AMS6935B AEROSPACE MATERIAL SPECIFICATION AMS6935 REV. B Issued 2004-01 Revised 2

5、015-07 Superseding AMS6935A Titanium Alloy Bars, Forgings and Forging Stock 6.0Al 6.0V 2.0Sn Solution Heat Treated and Aged (Composition similar to UNS R56620) RATIONALE AMS6935B results from a Five Year Review and update of this specification that includes the removal of sample size allowance for h

6、ydrogen of Table 1 (covered by ASTM E1447), requires agreement on mechanical property values for material outside specification ranges (3.5.1.1.6 and 8.7), the addition of AS6279 (3.8) and revises the report paragraph (4.4). 1. SCOPE 1.1 Form This specification covers a titanium alloy in the form of

7、 bars up through 4.000 inches (101.60 mm) in nominal diameter or least distance between parallel sides, inclusive, forgings of thickness up through 4.000 inches (101.60 mm), inclusive, with bars and forgings having a maximum cross-sectional area of 32 square inches (204.46 cm2), and stock for forgin

8、g of any size (See 8.7). 1.2 Application These products have been used typically for parts requiring high strength-to-weight ratio up to 750 F (399 C), but usage is not limited to such applications. 1.2.1 Certain processing procedures and service conditions may cause these products to become subject

9、 to stress-corrosion cracking; ARP982 recommends practices to minimize such conditions. 2. APPLICABLE DOCUMENTS The issue of the following documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to a subsequent re

10、vision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the last published issue of that document shall apply. SAE INTERNATIONAL AMS6935B Page 2 of 8 2.1 SAE Publications Available from SAE In

11、ternational, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or +1 724-776-4970 (outside USA), www.sae.org. AMS2241 Tolerances, Corrosion and Heat-Resistant Steel, Iron Alloy, Titanium, and Titanium Alloy Bars and Wire AMS2249 Chemical Check Analysis Limi

12、ts, Titanium and Titanium Alloys AMS2368 Sampling and Testing of Wrought Titanium Raw Materials, Except Forging and Forging Stock AMS2631 Ultrasonic Inspection, Titanium and Titanium Alloy Bar and Billet AMS2643 Structural Examination of Titanium Alloys, Chemical Etch Inspection AMS2750 Pyrometry AM

13、S2808 Identification Forgings AMS2809 Identification, Titanium and Titanium Alloy Wrought Products ARP982 Minimizing Stress-Corrosion Cracking in Wrought Titanium Alloy Products AS6279 Practices for Production, Distribution, and Procurement of Metal Stock 2.2 ASTM Publications Available from ASTM In

14、ternational, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org. ASTM E8/E8M Tension Testing of Metallic Materials ASTM E1409 Determination of Oxygen and Nitrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Technique ASTM E1447 Determi

15、nation of Hydrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Thermal Conductivity/Infrared Detection Method ASTM E1941 Determination of Carbon in Refractory and Reactive Metals and Their Alloys by Combustion Analysis ASTM E2371 Analysis of Titanium and Titanium Alloys by Direct Current

16、 Plasma and Inductively Coupled Plasma Atomic Emission Spectrometry 3. TECHNICAL REQUIREMENTS 3.1 Composition Shall conform to the percentages by weight shown in Table 1; carbon shall be determined in accordance with ASTM E1941, hydrogen in accordance with ASTM E1447, oxygen and nitrogen in accordan

17、ce with ASTM E1409, and other elements in accordance with ASTM E2371. Other analytical methods may be used if acceptable to the purchaser. SAE INTERNATIONAL AMS6935B Page 3 of 8 Table 1 - Composition Element min max Aluminum 5.00 6.00 Vanadium 5.00 6.00 Tin 1.50 2.50 Iron 0.35 1.00 Copper 0.35 1.00

18、Oxygen - 0.20 Carbon - 0.05 Nitrogen - 0.04 (400 ppm) Hydrogen - 0.015 (150 ppm) Yttrium (3.1.1) - 0.005 ( 50 ppm) Other Elements each (3.1.1) - 0.10 Other Elements, total (3.1.1) - 0.30 Titanium remainder 3.1.1 Determination not required for routine acceptance. 3.1.2 Check Analysis Composition vari

19、ations shall meet the applicable requirements of AMS2249. 3.2 Melting Practice Alloy shall be multiple melted. The first melt shall be made by vacuum consumable electrode, nonconsumable electrode, electron beam cold hearth, or plasma arc cold hearth melting practice. The subsequent melt or melts sha

20、ll be made under vacuum using vacuum arc remelting (VAR) practice. Alloy additions are not permitted in the final melt cycle. 3.2.1 The atmosphere for nonconsumable electrode melting shall be vacuum or shall be argon or helium at an absolute pressure not higher than 1000 mm of mercury. 3.2.2 The ele

21、ctrode tip for nonconsumable electrode melting shall be water-cooled copper. 3.3 Condition The product shall be supplied in the following condition: 3.3.1 Bars Hot finished with or without subsequent cold reduction, solution heat treated, aged, and descaled. A machined or ground surface is permitted

22、 unless prohibited by the purchaser. The product shall be processed to the final thickness/diameter by metallurgical working operations prior to any straightening, dimensional sizing or surface finishing operations. Bar shall not be cut from plate. 3.3.2 Forgings Solution heat treated, aged, and des

23、caled. 3.3.3 Stock for Forging As ordered by the forging manufacturer. SAE INTERNATIONAL AMS6935B Page 4 of 8 3.4 Heat Treatment Bars and forgings shall be solution heat treated and aged at 1550 to 1700 F (843 to 927 C) holding at the selected temperature within 25 F (14 C) for a time commensurate w

24、ith section thickness and the heating equipment and procedure used, and water quenched (except that thin sections may be air cooled) and aged at 875 to 1150 F (468 to 621 C), hold at the selected temperature within 15 F (8 C) for 2 to 10 hours. Pyrometry shall be in accordance with AMS2750. 3.5 Prop

25、erties The product shall conform to the following requirements: 3.5.1 Bars and Forgings 3.5.1.1 Tensile Properties Shall be as specified in Table 2, determined in accordance with ASTM E8/8M with the rate of strain set at 0.005 inch/inch/minute (0.005 mm/mm/minute) and maintained within a tolerance o

26、f 0.002 inch/inch/minute (0.002 mm/mm/minute) through the 0.2% offset yield strain. 3.5.1.1.1 Tensile property requirements apply in both the longitudinal and transverse directions. Transverse tensile properties of Table 2 apply only to product that a test specimen not less than 2.50 inches (63.5 mm

27、) in length can be obtained. 3.5.1.1.2 Specimens for the longitudinal requirements in Table 2 shall be taken with the axis of the specimen within 15 degrees of parallel to the grain flow. 3.5.1.1.3 Yield strength and reduction of area requirements do not apply to product under 0.125 inch (3.18 mm) i

28、n nominal diameter or least distance between parallel sides. 3.5.1.1.4 Table 2 properties are limited to product with a maximum cross-sectional area of 32 square inches (204.5 cm2). 3.5.1.1.5 Values in brackets apply to the short transverse direction for short transverse dimensions of 3.00 inches (7

29、6.2 mm) or greater. Table 2 - Minimum tensile properties (see 8.2) Nominal Diameter or Least Distance Between Parallel Sides Inch (mm) Tensile Strength ksi (MPa) Yield Strength At 0.2% Offset ksi (MPa) Elongation in 2 Inches (50.8 mm) or 4D, % (3.5.1.1.5) Reduction of Area % (3.5.1.1.5) Up to 1.000

30、(25.40), incl 175 (1206) 160 (1103) 8 20 Over 1.000 (25.40) to 2.000 ( 50.80) incl 170 (1172) 155 (1068) 8 20 Over 2.000 (50.80) to 3.000 ( 76.20) incl 155 (1068) 145 ( 999) 8 20 Over 3.000 (76.20) to 4.000 (101.60) incl 150 (1034) 140 ( 965) 8 6 20 15 3.5.1.1.6 Mechanical property requirements for

31、product outside the size range covered by 3.5.1.1.4 and Table 2 shall be agreed upon between purchaser and producer. 3.5.1.2 Microstructure Shall be that structure resulting from processing within the alpha-beta phase field. Microstructure shall conform to 3.5.1.2.1 or 3.5.1.2.2 (See 8.3). 3.5.1.2.1

32、 Equiaxed and/or elongated primary alpha in a transformed beta matrix with no continuous network of alpha at prior beta grain boundaries. 3.5.1.2.2 Primary alpha in an aged transformed beta matrix. SAE INTERNATIONAL AMS6935B Page 5 of 8 3.5.1.2.3 A microstructure showing a continuous network of alph

33、a in prior beta grain boundaries is not acceptable. 3.5.1.3 Surface Contamination Except as specified in 3.5.1.3.1, the product shall be free of any oxygen-rich layer (See 8.4), such as alpha case, or other surface contamination, determined by microscopic examination at not lower than 400X magnifica

34、tion or by other method agreed upon by purchaser and producer. 3.5.1.3.1 When permitted by purchaser, product to be machined all over may have an oxygen-rich layer, provided such layer is removable within the machining allowance on the product. 3.5.1.4 Macrostructure Product shall be uniform in qual

35、ity and condition, homogenous, sound, and free from foreign materials and from internal imperfections detrimental to fabrication or performance of parts. 3.5.2 Forging Stock When a sample of stock is forged to a test coupon and heat treated as in 3.4, specimens taken from the heat treated coupon sha

36、ll conform to the requirements of 3.5.1.1. If specimens taken from the stock after heat treatment as in 3.4 conform to the requirements of 3.5.1.1, the tests shall be accepted as equivalent to tests of a forged coupon. 3.6 Quality The product, as received by purchaser, shall be uniform in quality an

37、d condition, sound, and free from foreign materials and from imperfections detrimental to usage of the product. 3.6.1 Ultrasonic Inspection Product 0.500 inch (12.70 mm) to 1.500 inches (38.10 mm) inclusive in nominal thickness, diameter or least distance between parallel sides shall meet Class A1 o

38、r stricter requirements of AMS2631. Product over 1.500 inches (38.10 mm) in nominal thickness, diameter or least distance between parallel sides shall meet Class A or stricter requirements of AMS2631. 3.7 Tolerances Bars shall conform to all applicable requirements of AMS2241. 3.8 Production, distri

39、bution, and procurement of metal stock shall comply with AS6279. This requirement becomes effective September 1, 2016. 4. QUALITY ASSURANCE PROVISIONS 4.1 Responsibility for Inspection The producer of the product shall supply all samples for producers tests and shall be responsible for the performan

40、ce of all required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the product conforms to the specified requirements. 4.2 Classification of Tests 4.2.1 Acceptance Tests The following requirements are acceptance tests and shall be

41、 performed on each heat or lot as applicable. 4.2.1.1 Composition (3.1) of each heat. 4.2.1.2 Hydrogen content (3.1), tensile properties (3.5.1.1), microstructure (3.5.1.2), surface contamination (3.5.1.3), and macrostructure (3.5.1.4) of each lot of bars and forgings. SAE INTERNATIONAL AMS6935B Pag

42、e 6 of 8 4.2.1.3 Ultrasonic quality (3.6.1) of each bar, forging, or forging stock. 4.2.1.4 Tolerances (3.7) of bars. 4.2.2 Periodic Tests Ability of forging stock (3.5.3) to develop specified properties is a periodic test and shall be performed at a frequency selected by the producer unless frequen

43、cy of testing is specified by purchaser. 4.3 Sampling and Testing Shall be in accordance with AMS2368 and as follows: A lot shall be all product of the same nominal size from the same heat processed at the same time. 4.3.1 For Acceptance Tests 4.3.1.1 Composition At least one sample from each heat,

44、except that for hydrogen determinations one sample from each lot obtained after all thermal and chemical processing is completed. 4.3.1.2 Tensile Properties At least one sample from bars from each lot. The number, location, and orientation of samples from each lot of forgings shall be as agreed upon

45、 by purchaser and producer. 4.3.1.3 A specimen at least 0.5 inch (12.7 mm) long by full cross-section from each end of the bars selected for sampling shall be macrostructurally examined for conformance to the quality requirements. Unless otherwise specified, macrostructural examination shall be perf

46、ormed in accordance with AMS2643. The number of bars selected for examination shall not be less than the amounts shown in Table 3. Table 3 - Number of bars selected for macrostructural examination Number of Bars in Lot Number of Bars Selected 1 to 15 1 16 to 50 2 51 to 150 3 151 to 500 5 over 500 4

47、+ amount shown above over 500 4.4 Reports 4.4.1 The producer shall furnish with each shipment a report showing producer identity, country where the metal was melted (e.g., final melt in the case of metal processed by multiple melting operations) and the results of tests for composition of each heat

48、and for the hydrogen content, tensile properties, and surface contamination of each lot, ultrasonic quality, and state that the product conforms to the other technical requirements. The report shall include the purchase order number, heat and lot numbers, AMS6935B, product form and mill produced siz

49、e (and/or part number, if applicable), specific solution heat treatment and aging treatment used to develop precipitation hardened properties, and quantity. If forgings are supplied, the size and melt source of stock used to make the forgings shall also be included. 4.4.2 Report the nominal metallurgically worked cross sectional size and the cut size, if different (See 3.3.1). SAE INTERNATIONAL AMS6935