1、Designation: D2519 07 (Reapproved 2012)Standard Test Method forBond Strength of Electrical Insulating Varnishes by theHelical Coil Test1This standard is issued under the fixed designation D2519; the number immediately following the designation indicates the year oforiginal adoption or, in the case o
2、f revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S. Department of Defense.1. Scope*1.1 This te
3、st method covers determination of the bondstrength of an electrical insulating varnish when applied to ahelical coil. The helical coil can be made from bare aluminumor copper wire or from film or fiber-insulated magnet wire.Helical coils made from bare aluminum or bare copper wirewill yield values o
4、f bond strength for the varnish when appliedto bare metal conductors. The use of film or fiber-insulatedmagnet wire will show values for that particular combinationof insulation and varnish.1.2 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for i
5、nformationonly.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.
6、 See Section 7.2. Referenced Documents2.1 ASTM Standards:2D115 Test Methods for Testing Solvent Containing Var-nishes Used for Electrical InsulationD1711 Terminology Relating to Electrical InsulationD6054 Practice for Conditioning Electrical Insulating Mate-rials for Testing (Withdrawn 2012)3E691 Pr
7、actice for Conducting an Interlaboratory Study toDetermine the Precision of a Test Method3. Terminology3.1 Definitions:3.1.1 For definitions of other terms relating to electricalinsulation, see Terminology D1711.3.1.2 bond strengtha measure of the force required toseparate surfaces which have been b
8、onded together.3.2 Definitions of Terms Specific to This Standard:3.2.1 event timethe time between initial application of aphysical or electrical stress and failure of the specimen undertest.3.2.2 response timethe time required for an indicating orrecording device to react to change in stress on a s
9、pecimenunder test.4. Summary of Test Method4.1 Flexural strength tests are made on varnish-treatedhelical coils to determine the force required to break the coilunder specified conditions.5. Significance and Use5.1 Values obtained by flexural tests can provide informa-tion with regard to the bond st
10、rength of the particular varnish,in combination with a particular wire, when measured underconditions described in this test method.6. Apparatus6.1 Tensile Testing MachineUse an adjustable-speed driveand a suitable instrument for measuring force to break thespecimen. Available tensile testing machin
11、es or an accuratespring gauge and a separate adjustable-speed drive are suitable.To cover the range of load strength values which are commonlyencountered it is recommended that a multirange tester beused.6.1.1 It has been found that gages rated 5, 25, 150, and500 N (1, 5, 30, and 100 lbf) are adequa
12、te to cover the range ofvarnishes.6.2 Test FixtureThe test fixture consists of two rollers,attached to a common frame, and a 90 V-block. One part,either the rollers or the V-block, is held stationary while theother part is moved. No friction contact which will affect this1This test method is under t
13、he jurisdiction of ASTM Committee D09 onElectrical and Electronic Insulating Materials and is the direct responsibility ofSubcommittee D09.01 on Electrical Insulating Varnishes, Powders and Encapsulat-ing Compounds.Current edition approved April 1, 2012. Published April 2012. Originallyapproved in 1
14、966. Last previous edition approved in 2007 as D2519 07. DOI:10.1520/D2519-07R12.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page
15、 onthe ASTM website.3The last approved version of this historical standard is referenced onwww.astm.org.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1movement is allow
16、ed. The general shape and the relativeposition of these parts are shown in Fig. 1. The rollers have adiameter of 9.5 mm (0.375 in.) at the center and are parallelhaving a center-to-center distance of 44.5 mm (1.75 in.). The90 V-block has a radius at the apex of 0.8 mm (0.03 in.).6.3 Test Fixture Enc
17、losureFor tests at other than roomtemperature, use an insulated heat-resistant enclosure, designedto fit around the test fixture and connected to the tension testingmachine. This enclosure permits a frictionless connectionbetween the test fixture and the instrument that measures thebreaking force. T
18、he enclosure is designed with a suitablelocation for holding six or more specimens. It is heated orcooled by a separate source of uniformly circulating hot or coldair. The temperature control system is capable of returning thetest specimens and the chamber to the test temperature in lessthan 10 min.
19、 A thermostatic control, with the measuringthermocouple located within 25 mm (1.0 in.) of the center ofthe coil being tested, is set to maintain the temperature of thechamber to within 6 2C of the desired temperature after thetemperature has stabilized.7. Safety Precautions7.1 It is unsafe to use va
20、rnish at temperatures above theflash point without adequate ventilation, especially if thepossibility exists that flames or sparks are present. Storevarnish in sealed containers.8. Test Specimens8.1 The test specimens are 75 mm (3 in.) long coils of No.18 AWG wire, cut from a helix of convenient len
21、gth which hasbeen wound without space between turns ona6mm(0.25 in.)diameter mandrel. Bend the last loop on each end of the coil toapproximately 90 to the coil to provide a means of support.Treat the coil with the varnish to be tested. Make the helicalcoils as agreed to by interested parties from on
22、e of thefollowing:8.1.1 Bare aluminum wire,8.1.2 Bare copper wire,8.1.3 Film-coated magnet wire, or8.1.4 Fiber-insulated magnet wire.NOTE 1A practical method of winding a tight helical coil is to guidethe wire from the rotating reel between folds of a clean cloth onto therotating mandrel using moder
23、ate hand tension. Maintain a trailing angle of1 to 5 from a perpendicular to the mandrel. When the wire is cut, the coilmust be restrained to avoid rapid spring back.8.2 Prepare six or more specimens for each condition to beinvestigated.8.3 Adjust the viscosity of the varnish to be tested, by trial,
24、to produce a dry film build of 0.043 to 0.053 mm (0.0017 to0.0021 in.) on a metal panel double coated in accordance withTest Methods D115.8.4 Use solventless varnish in the “as received” condition.8.5 Immerse coils made from bare wire in a solvent of 50 %toluene and 50 % denatured alcohol by weight
25、for 30 min.Remove and dry for 15 min at 100 C before treating withvarnish. Do not clean coils made from insulated wire beforetreating with varnish.8.6 Attach several coils to a rack and immerse vertically inthe varnish until bubbling stops. Withdraw them at 100 65mm/min (4 60.2 in./min) and allow th
26、em to drain 10 to 30 minat the Standard Laboratory Atmosphere in accordance withPractice D6054. Place the coils in an oven in the same positionas dipped at the temperature and for the time specified by themanufacturer. For solvent containing varnishes, reverse dip andbake the coils, following the ab
27、ove procedure.9. Procedure9.1 Rate of LoadingAdjust the testing machine to acrosshead speed of 50 mm/min (2 in./min).9.1.1 Position the coils in the test fixture with the center ofthe coils below the V-block. Each coil is broken only once.9.2 Number of SpecimensTest a minimum of five speci-mens for
28、each condition. It is allowable to use one of theoriginal six specimens for adjusting the testing machine.9.3 Selection of Test RangeSelect the proper test rangewhich corresponds to the specified rate of loading. The propertest range is the one where the anticipated bond strength will bereached in t
29、he middle or upper portion of the test range,whenever possible. For testers with chart recorders it isessential that the test range be selected in such a manner thatthe event time is greater than the response time of the recorder.9.4 Tests at Other than Room Temperature:9.4.1 Adjust the temperature
30、control until the temperature ofthe chamber becomes constant within 6 2C of the specifiedtest temperature.9.4.2 Place one specimen in the test fixture. Place theremaining specimens in the enclosure. Allow the enclosure tostabilize for 5 6 1 min at the test temperature. Break thespecimen in the test
31、fixture as described in 9.1 9.3.9.4.3 Replace broken specimen with an untested specimenfrom within the enclosure. Allow the enclosure to stabilize forFIG. 1 Test Fixture for Bond Strength TestD2519 07 (2012)2approximately 1 min at the test temperature. Break the speci-men in the test fixture as desc
32、ribed in 9.1 9.3.9.4.4 Repeat 9.4.3 for the remaining specimens.10. Report10.1 Report the following information:10.1.1 Description of varnish,10.1.2 Identification of wire used,10.1.3 Cure time and temperature for each coat and numberof dips used to prepare the coils, and10.1.4 The individual values
33、 in newtons (pounds-force) ofbond strength and their averages at each test condition.11. Precision and Bias11.1 PrecisionTable 1 lists the results based on a roundrobin test conducted in accordance with Practice E691 involv-ing six laboratories and three materials. Each test result was theaverage of
34、 five specimens. Each laboratory obtained two testresults for each material.11.2 BiasThis test method has no bias because the valuefor bond strength of electrical insulating varnishes by thehelical coil test is determined solely in terms of this testmethod.Combined data from six laboratories:Mean =
35、220.6 N (49.6 lbf)Standard deviation = 41.99 N (6.96 lbf)95 % Confidence level = 82.25 N (13.64 lbf)12. Keywords12.1 bond strength; helical coil; varnishSUMMARY OF CHANGESCommittee D09 has identified the location of selected changes to this test method since the last issue,D2519 02, that may impact
36、the use of this test method. (Approved May 1, 2007)(1) Revised Sections 6, 8, and 9.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the
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41、ter, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 1 Results in NewtonsMaterial AverageStandardDeviationRepeatabilityStandardDeviationReproducibilityStandard DeviationRepeatabilityLimitReproducibilityLimitSolvent Varnish 97.21 13.92 1.75 12.81 4.90 35.87Unsaturated Polyester 166.76 34.03 6.26 31.59 17.53 88.45Epoxy 208.43 37.45 10.41 35.48 29.15 99.34D2519 07 (2012)3
