1、 ENGINEERING MATERIAL SPECIFICATIONDate Action Revisions 2009 10 27 N-STATUS No known use. No Replacement Named D. DiGregorio, NA 2004 05 24 Revised Para 3.0 inserted; para 3.1, 3.7 & 4 deleted 1988 12 01 Released SM/ER0831TC D. Allcock Printed copies are uncontrolled Copyright 2009, Ford Global Tec
2、hnologies, LLC Page 1 of 8 OIL - ENGINE, SAE 10W-30 API SG/CD, WSD-M2C904-A INITIAL FILL NOT TO BE USED FOR NEW DESIGN 1. SCOPE This material specification defines the minimum acceptable performance requirements and physical/chemical properties of engine oil to be used by Ford Motor Company in its w
3、orldwide engine/vehicle manufacturing operations. 2. APPLICATION This specification was released originally for initial fill engine oils used for lubrication of spark ignition engines using gasolines and for naturally aspirated and turbo-charged compression ignition engines using diesel fuels. 3. RE
4、QUIREMENTS 3.0 STANDARD REQUIREMENTS FOR PRODUCTION MATERIALS Material suppliers and part producers must conform to the Companys Standard Requirements For Production Materials (WSS-M99P1111-A). 3.2 PERFORMANCE Shall meet all the requirements of API service category “SG/CD“ as defined in SAE Standard
5、 J 183 (latest revision), “Engine Oil Performance and Engine Service Classification“, or in ASTM D 4485, “Standard Performance Specification for Automotive Engine Oils“. All required engine tests shall be conducted in accordance with the most recently approved procedures as described in ASTM Special
6、 Technical Publications 315, 509 and applicable ASTM Research Reports and Information Letters. All tests under surveillance by ASTM must be conducted using test equipment monitored by and calibrated to the requirements of the ASTM Test Monitoring Center. 3.3 VISCOSITY GRADE Shall meet all the requir
7、ements of the applicable SAE viscosity grade as defined in SAE Standard J300 (latest revision), “Engine Oil Viscosity Classification“. 3.4 ENERGY CONSERVING PERFORMANCE (ASTM Sequence VI) Average Improvement (EFEI), min 2.7% vs HR-2 or equiv. Shall meet all the requirements of the API “Energy Conser
8、ving II“ category as defined in SAE Recommended Practice J1423 (latest revision), “Passenger Car and Light Duty Truck Energy Conserving Oil Classification.“ All tests must be conducted using test equipment monitored by and calibrated to the requirements of the ASTM Test Monitoring Center. ENGINEERIN
9、G MATERIAL SPECIFICATIONWSD-M2C904-APrinted copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 2 of 8 3.5 PHYSICAL/CHEMICAL PROPERTIES 3.5.1 Viscosity at Temperature, max (FLTM BJ 127-01, Scanning Brookfield) SAE 10W-30 30 Pa.s at -25 C Copy of curve plotted per FLTM BJ 127-0
10、1 (Figure 2) is required. 3.5.2 Viscosity (After Shear Evaluation) Report (mm2/s) (ASTM D 445 or ISO 3104 at 100 C) Sheared viscosity after each of the following tests: a. ASTM D 3945, or after 30 cycles of CEC L-14A-78. b. ASTM STP 509 A, Part IV and ASTM D 3607, after 10 h in L-38 test and removal
11、 of volatile contaminants. 3.5.3 Viscosity at 150 C and 1E6/s, min (ASTM D 4683 or CEC L-36T-84) New Oil Sheared Oil* SAE 10W-30 2.9 mPa.s 2.6 mPa.s *Perform after item a. of para 3.5.2 3.5.4 Volatility Shall meet either “Evaporative Loss“ or “Distillation by Gas Chromatography“ requirements as foll
12、ows: Evaporative Loss (Noack), max (DIN 51581, 1 h at 250 C) SAE 10W-30 20% or Distillation by Gas Chromatography, max 20% (ASTM D 2887, Distilled at 371 C) 3.5.5 Flash Point, min 180 C (ASTM D 93 or ISO 2719) 3.5.6 Copper Corrosion, max 1b (ASTM D 130 or ISO 2160, 3 h at 100 C) (Dark Orange) ENGINE
13、ERING MATERIAL SPECIFICATIONWSD-M2C904-APrinted copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 3 of 8 3.5.7 Filterability (FLTM BJ 124-01) Flow rate decrease, max 50% 3.5.8 Foaming, max Foam Stability (ASTM D 892, Opt. A) Foaming Tendency 5 min Settling Sequence I 10 mL 0
14、 mL Sequence II 50 mL 0 mL Sequence III 10 mL 0 mL Sequence IV* Rate and Rate and Report Report* * Same as Sequence I except at 150 +/- 3 C and 200 +/- 5 mL/min air flow rate. *5 s settling. 3.5.9 Seal Compatibility Shall be compatible with all current production component materials. 3.5.10 Physical
15、 Appearance and Odor Shall be clear and bright with no objectionable odor. 3.5.11 Homogeneity and Miscibility (FTM 791 C, Method 3470.1) Shall remain homogeneous and when mixed with SAE reference oils shall remain miscible. 3.6 QUALIFICATION PROCEDURE 3.6.1 Documentation Supplier must furnish to the
16、 affected Materials Engineering activity a completed and certified copy of the attached Supplement A and test reports demonstrating full compliance with all the requirements of this specification. The test reports must include results on both the candidate oil and the appropriate ASTM reference oils
17、. The standard photographs of the test components are considered an essential part of the required test documentation. The oil sample code used for identification in each test document must be consistent. Any deviation in sample code uniformity must be explained and shown on the cover of each test r
18、eport. All tests must be certified by a qualified and authorized representative of the test facility. 3.6.2 “Read Across“ Guidelines It is recommended that all performance tests be conducted on the final formulation, however, some exceptions may be permitted on an individual basis. Supplementary sup
19、portive data on similar formulations may be necessary in determining final approval. Minimum Energy Conserving performance of the SAE 10W-30 oil may be established on the corresponding SAE 10W-40 formulation. ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-APrinted copies are uncontrolled Copyright 200
20、9, Ford Global Technologies, LLC Page 4 of 8 3.6.3 Fleet Testing Materials which, in the opinion of the affected Materials Engineering activity, constitute a significant departure from conventional formulations, whether in base stocks, refining processes or additive packages, must be fleet tested, i
21、n addition to the requirements outlined herein. These tests must include the type(s) of service judged to be affected by the difference in formulation technology. The affected Materials Engineering activity should be consulted prior to testing. 3.6.4 Verification The affected Materials Engineering a
22、ctivity reserves the right to conduct verification testing. If the test results do not support the originally submitted data, the supplier must re-test the product in coordination with the affected Materials Engineering activity. This re-test must be conducted and certified by a mutually agreed upon
23、 test facility. 3.6.5 Chemical and Physical Properties Supplier shall furnish appropriate chemical and physical properties as required on Supplement A along with the manufacturing limits that apply to the material upon which approval is requested. 3.6.6 Quality Control Upon engineering approval, sup
24、plier and affected Materials Engineering activity shall establish mutually agreed upon quality control limits, to be listed on Supplement B, and will be used for ongoing product verifications at mutually agreed upon frequencies. The infrared absorption spectra of the approved material shall constitu
25、te the reference standard and shall be kept on file. All samples shall produce infrared curves that correspond to the reference standard when tested under the same conditions as those specified on the master curve. ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-APrinted copies are uncontrolled Copyrig
26、ht 2009, Ford Global Technologies, LLC Page 5 of 8 API SG/CD SAE 10W30 Supplement A Page 1 of 3 Oil Company_ Date_ Product Name_ Viscosity Grade_ Product Code_ Blend Plant Location(s)_ Base Stocks Manufacturing Limits Nominal Base Oil Viscosity, mm2/s Cloud Point, C/ Type Vol. % 100 C 40 C Sulphur,
27、% Pour Point, C A _ _ _ _ _ _ B _ _ _ _ _ _ C _ _ _ _ _ _ D _ _ _ _ _ _ Refinery Name & Location Process Type Crude source A _ _ _ B _ _ _ C _ _ _ D _ _ _ Note: Viscosity Sulphur Cloud Point Pour Point (ASTM D 445) (ASTM D 129) (ASTM D 2500) (ASTM D 97) (ASTM D 1552) (ASTM D 2622) Additives Carrier
28、Oil Additive In Type/ Manufacturer In Additive Finished Oil Function Name Code Description Vol. % Vol. % E _ _ _ _ _ _ F _ _ _ _ _ _ G _ _ _ _ _ _ H _ _ _ _ _ _ I _ _ _ _ _ _ Signature_ Title_ ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-APrinted copies are uncontrolled Copyright 2009, Ford Global T
29、echnologies, LLC Page 6 of 8 API SG/CD SAE 10W-30 Supplement A Page 2 of 3 Oil Company_ Date_ Product Name_ Product Code_ Performance Requirements Lab./Date/ Test Number Specification Test Results Sequence IID _ _ Average Engine Rust _ 8.5 min _ Stuck Valve Lifters 0 _ Sequence IIIE _ Viscosity Incr
30、ease 64 h, % _ 375 max _ Average Engine Sludge 9.2 min _ Average Piston Skirt Varnish 8.9 min _ Average Oil Ring Land Deposit 3.5 min _ Stuck Piston Rings Report _ Stuck Valve Lifters 0 _ Scuffed and/or Worn Cam Lobes 0 _ Valve Lifters 0 _ Cam Plus Lifter Wear Average, micrometre 30 max _ Maximum, m
31、icrometre 64 max _ Oil Consumption, L 4.62 max _ Sequence VE _ Average Engine Sludge _ 9.0 min _ Rocker Arm Cover Sludge 7.0 min _ Average Piston Skirt Varnish 6.5 min _ Average Engine Varnish 5.0 min _ Oil Ring Clogging, % 15 max _ Oil Screen Clogging, % 20 max _ Stuck Compression Rings (Hot) 0 _ C
32、am Wear Average, micrometre 130 max _ Maximum, micrometre 380 max _ Test Method L-38 _ Bearing Weight Loss, mg _ 40 max _ Piston Skirt Varnish 9.0 min _ Test Method 1H2 (if available) _ Groove #1 Carbon Fill Vol., % _ 45 max _ Weighted Total Demerits 140 max _ Ring Side Clearance Loss, micrometre 13
33、 max _ Test Method 1G2 _ Groove #1 Carbon Fill Vol., % _ 80 max _ Weighted Total Demerits 300 max _ Ring Side Clearance Loss, micrometre 13 max _ Sequence VI _ Average Improvement (EFEI) _ 2.7% vs HR-2 _ Signature_ Title_ ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-APrinted copies are uncontrolled
34、Copyright 2009, Ford Global Technologies, LLC Page 7 of 8 API SG/CD SAE 10W-30 Supplement A Page 3 of 3 Oil Company_ Date_ Product Name_ Product Code_ Specification Test Mfg. Physical/Chemical Properties Requirements Results Limits Viscosity at 150 C (ASTM D 445), mm2/s _ _ Viscosity at 100 C (ASTM
35、D 445), mm2/s 9.3-.001%) _ _ _ Signature_ Title_ ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-APrinted copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 8 of 8 API SG/CD SAE 10W-30 Supplement B Oil Company_Date_ Product Name_ Product Code_ Blend Plant Location_ Quality Contr
36、ol Certification Approved Physical/Chemical Properties Limits Frequency Viscosity at 100 C (ASTM D 445), mm2/s _ _ Viscosity at 40 C (ASTM D 445), mm2/s _ _ Density (ASTM D 1298), kg/L _ _ Viscosity at -20 C (SAE J300 App. A), mPa.s _ _ Viscosity at -25 C (SAE J300 App. A), mPa.s _ _ Borderline Pump
37、ing Temp. (ASTM D 4684), C _ _ Pour Point (ASTM D 97), C _ _ Stable Pour Point (SAE J300 App. B), C _ _ Viscosity at -25 C (FLTM BJ 127-01), Pa.s _ _ Flash Point (ASTM D 93), C _ _ Volatility Evap. Loss, 1 h at 250 C (DIN 51581), % _ _ Dist. by GC at 371 C (ASTM D 2887), % _ _ Shear Stability (ASTM
38、D 445), mm2/s After ASTM D 3945 or CEC L-14A-78 _ _ After 10 h in “L-38“ test _ _ Viscosity at 150 C and 1E6/s (ASTM D 4683 or CEC L-36T-84), mPa.s New Oil _ _ After ASTM D 3945 or CEC L-14A-78 _ _ Copper Corrosion (ASTM D 130, 3 h at 100 C) _ _ Filterability (FLTM BJ 124-01), % _ _ Foaming Sequence I, mL _
