1、May 2010 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 83.
2、180!$bXz“1635387www.din.deDDIN EN 13415Test of adhesives for floor covering Determination of the electrical resistance of adhesive films andcompositesEnglish translation of DIN EN 13415:2010-05Prfung von Klebstoffen fr Bodenbelge Bestimmung des elektrischen Widerstandes von Klebstoff-Filmen und Verb
3、undenEnglische bersetzung von DIN EN 13415:2010-05Essai des adhsifs pour revtements de sol Dtermination de la rsistance lectrique des composites et films dadhsifTraduction anglaise de DIN EN 13415:2010-05SupersedesDIN EN 13415:2002-08www.beuth.deIn case of doubt, the German-language original shall b
4、e considered authoritative.Document comprises 12 pages05.10 DIN EN 13415:2010-05 2 A comma is used as the decimal marker. National foreword This standard has been prepared by Technical Committee CEN/TC 193 “Adhesives” (Secretariat: AENOR, Spain). The responsible German body involved in its preparati
5、on was the Normenausschuss Materialprfung (Materials Testing Standards Committee), Technical Committee NA 062-04-54 AA Prfung von Klebstoffen fr Bodenbelge, Wand- und Deckenbekleidung. Amendments This standard differs from DIN EN 13415:2002-08 as follows: a) Composites have been included in the titl
6、e and in the scope of the standard. b) Definitions of the vertical resistance of floor covering, resistance to ground, point to point resistance, adhesive resistance and vertical resistance of composite have been included. c) The preparation of the test specimens has been modified. d) The storing of
7、 the specimens has been specified. e) The test procedure has been modified. Previous editions DIN 53276: 1977-05 DIN EN 13415: 2002-08 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 13415 January 2010 ICS 83.180 Supersedes EN 13415:2002English Version Test of adhesives for floor covering - Det
8、ermination of the electrical resistance of adhesive films and composites Essai des adhsifs pour revtements de sol - Dtermination de la rsistance lectrique des composites et films dadhsif Prfung von Klebstoffen fr Bodenbelge - Bestimmung des elektrischen Widerstandes von Klebstoff-Filmen und Verbunde
9、n This European Standard was approved by CEN on 28 November 2009. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical
10、references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN me
11、mber into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Irela
12、nd, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17
13、, B-1000 Brussels 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 13415:2010: EEN 13415:2010 (E) 2 Contents Page Foreword 31 Scope 42 Normative references 43 Terms and definitions .44 Apparatus and materials .55 Preparation of
14、 test specimens .65.1 Preparation of test specimens for determination of adhesive resistance R465.2 Preparation of test specimens for determination of vertical resistance of composite R5.76 Storing the specimens 86.1 Storing the specimens for determination of adhesive resistance R4.86.2 Storing the
15、specimens for determination of vertical resistance of composite R587 Test procedure .97.1 General 97.2 Adhesive resistances, R497.3 Vertical resistance of composite, R598 Test report 9Bibliography . 10DIN EN 13415:2010-05 EN 13415:2010 (E) 3 Foreword This document (EN 13415:2010) has been prepared b
16、y Technical Committee CEN/TC 193 “Adhesives”, the secretariat of which is held by AENOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by July 2010, and conflicting national standards shall be with
17、drawn at the latest by July 2010. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 13415:2002. SAFETY STATE
18、MENT Persons using this document should be familiar with the normal laboratory practice, if applicable. This document does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and
19、 to ensure compliance with any regulatory conditions. ENVIRONMENTAL STATEMENT It is understood that some of the material permitted in this standard may have negative environmental impact. As technological advantages lead to acceptable alternatives for these materials, they will be eliminated from th
20、is standard to the extent possible. At the end of the test, the user of the standard should take care to carry out an appropriate disposal of the wastes, according to local regulation. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries
21、are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Croatia, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia,
22、Spain, Sweden, Switzerland and the United Kingdom. DIN EN 13415:2010-05 EN 13415:2010 (E) 4 1 Scope This European Standard specifies a test method to measure the electrical resistance as a material physical parameter of an adhesive film and composites of floor covering material and adhesive film. Th
23、e electrical resistance is reciprocal to the electrical conductivity. This laboratory method does not take account of all influences which may occur in practice. In contrast to EN 1081, which applies to the determination of the electrical resistance of resilient floor coverings R1, R2and R3(see Clau
24、se 3), this method applies to the determination of the electrical resistance of adhesive films on glass and of composites of floor coverings, adhesively bonded to a fibre cement substrate R4and R5(see Clause 3). 2 Normative references The following referenced documents are indispensable for the appl
25、ication of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 923:2005+A1:2008, Adhesives Terms and definitions EN 1067, Adhesives Examination and preparation of samples for
26、 testing EN 1081:1998, Resilient floor coverings Determination of the electrical resistance EN ISO 9142, Adhesives Guide to the selection of standard laboratory ageing conditions for testing bonded joints (ISO 9142:2003) EN ISO 15605, Adhesives Sampling (ISO 15605:2000) ISO 554, Standard atmospheres
27、 for conditioning and/or testing Specifications 3 Terms and definitions For the purposes of this document, the terms and definitions given in EN 923:2005+A1:2008 and the following apply. 3.1 vertical resistance of floor covering R1electrical resistance, measured at an unbounded floor covering sample
28、 between the tripod electrode on the surface of the floor covering and a second electrode on the opposite underside 3.2 resistance to ground R2electrical resistance, measured at a bonded floor covering between a tripod electrodes on the surface of the floor covering and ground 3.3 point to point res
29、istance R3electrical resistance measured on the surface of a bonded floor covering between two tripod electrodes in a distance of 100 mm DIN EN 13415:2010-05 EN 13415:2010 (E) 5 3.4 adhesive resistance R4electrical resistance of a cured adhesive film, measured between two copper strips in a distance
30、 of 500 mm to each other 3.5 vertical resistance of composite R5electrical resistance of a bonded floor covering, measured between a tripod electrode on the surface of the floor covering and a copper strip on the underside in a distance of 500 mm to each other 4 Apparatus and materials 4.1 Glass pla
31、te, dimensions: approximately 600 mm 120 mm 4 mm. 4.2 Uncoated fibre cement panels, fully compressed and autoclaved, asbestos free, with dimensions of approximately 750 mm 300 mm 6 mm. 4.3 Adhesive applicator with an opening of (1,0 0,1) mm height and a width of (100 1) mm (see Figure 1). Dimensions
32、 in millimetres Figure 1 Opening dimensions of the adhesive applicator 4.4 Adhesive trowel, serrated blade with a notch size specified by the adhesive manufacturer. 4.5 Three copper strips, preferably self-adhesive, dimensions: approximately 120 mm x 10 mm x 0,08 mm. 4.6 Conductive floor covering, d
33、imensions: approx. 700 mm x 250 mm. 4.7 Roller, of width (60 1) mm, diameter (95 1) mm and total mass (3,5 0,1) kg with handle at 90 to the axis (see Figure 2). DIN EN 13415:2010-05 EN 13415:2010 (E) 6 Dimensions in millimetres Figure 2 Roller 4.8 Tripod electrode in accordance with EN 1081:1998 (se
34、e EN 1081:1998, 5.1 and Figure 1). 4.9 Load able to apply at least 300 N to the tripod electrode. 4.10 Resistance meter, calibrated, with an accuracy of 5 % for R values in the range of 103 to 1010, and of 10 % for more than 1010. For resistances less than or equal to 106 the open circuit voltage sh
35、all be 10 V d.c., for resistances greater than 106 but not exceeding 1010 it shall be 100 V and for resistances greater than 1010 it shall be 500 V. NOTE Recommended is a resistance meter with an inside resistance of 100 k and an inside circuit according to IEC 60093:1980, A.2.2. 4.11 Dry heat chamb
36、er, ventilated and adjustable to a temperature between 20 C and 200 C according to EN ISO 9142. 5 Preparation of test specimens 5.1 Preparation of test specimens for determination of adhesive resistance R4The side of the glass plate (4.1) intended for applying the adhesive shall be free of grease, d
37、ust and other contamination. DIN EN 13415:2010-05 EN 13415:2010 (E) 7 Take a sample of the adhesive to be tested in accordance with EN ISO 15605, examine and prepare it for testing in accordance with EN 1067. Two copper strips (4.5) shall be affixed (500 10) mm away from each other in parallel to th
38、e shorter edges on the glass plate, making sure they protrude about 30 mm beyond the edge of the plate. Apply adhesive to produce a uniform thickness of 1 mm. A sufficient quantity of adhesive shall be applied to the prepared surface on one shorter edge of the plate. The adhesive shall be spread eve
39、nly using the applicator in accordance with 4.3, in parallel to the longer edge glass plate (see Figure 3). Dimensions in millimetres Key 1 Glass plate 2 Copper strip 3 Adhesive film area Figure 3 Arrangements of the copper strips 5.2 Preparation of test specimens for determination of vertical resis
40、tance of composite R5The fibre cement panel (4.2) shall be likewise free of dust and other contamination, and before the adhesive is applied be conditioned for 120 h at (50 3) C in a dry-heat chamber (see 4.11) and reconditioned for at least 8 h at standard atmosphere 23/50 according to ISO 554. Tak
41、e a sample of the adhesive to be tested in accordance with EN ISO 15605, examine and prepare it for testing in accordance with EN 1067. A copper strip (4.5) shall be affixed parallel to the shorter edge of the fibre cement panel at the end of the panel making sure it protrudes about 30 mm beyond the
42、 edge of the panel. A sufficient quantity of adhesive shall be applied to the prepared surface on one shorter edge of the plate. The adhesive shall be spread evenly using the applicator in accordance with 4.4, in a width of 200 mm in the middle and parallel to the longer edge of cement panel. After
43、the open time specified by the adhesives producer, the conductive floor coverings (see 4.6) being tested shall be laid into the adhesive bed flush against one short side, just in the middle of the two long sides of the carrier slab, and rolled on using the roller (4.7) by rolling it evenly back and
44、forth three times without additional pressure (see Figure 4). DIN EN 13415:2010-05 EN 13415:2010 (E) 8 Dimensions in millimetres Key 1 Support (fibre cement panel) 2 Copper strip 3 Adhesive film covered with floor covering 4 Tripod electrode Figure 4 Fibre cement panel with bonded floor covering 6 S
45、toring the specimens 6.1 Storing the specimens for determination of adhesive resistance R4The samples are stored as follows: a) 24 h at standard atmosphere 23/50 according to ISO 554; plus b) 24 h at (40 3) C in a dry-heat chamber (see 4.11); plus c) 48 h at standard atmosphere 23/50 according to IS
46、O 554. 6.2 Storing the specimens for determination of vertical resistance of composite R5The samples are stored as follows: a) 24 h at standard atmosphere 23/50 according to ISO 554; plus b) 96 h at (40 3) C in a dry-heat chamber (see 4.11); plus c) 48 h at standard atmosphere 23/50 according to ISO
47、 554. DIN EN 13415:2010-05 EN 13415:2010 (E) 9 7 Test procedure 7.1 General The electrical resistances shall be measured following the storage period (6.1 and 6.2). 7.2 Adhesive resistances, R4The two copper strips are connected to the resistance meter (4.10). Testing begins with 100 V test voltage,
48、 (15 2) s after applying the test voltage the electrical resistance in ohms () shall be read. If the value exceeds 1010, the measuring shall be repeated with 500 V test voltage. 7.3 Vertical resistance of composite, R5The tripod electrode (see 4.8) is placed on the narrow side of the floor covering
49、(see Figure 4) and loaded with at least 300 N. The electrode and the copper strip on the opposite underside are connected with the resistance meter. Testing begins with 10 V test voltage, (15 2) s after applying the test voltage the electrical resistance in ohms () shall be read. If the value exceeds 106 the measuring shall be repeated with 100 V test voltage. If the value exceeds 1010 the final measuring shal
