1、Designation: D 4360 03Standard Specification forMethyl n-Amyl Ketone1This standard is issued under the fixed designation D 4360; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses ind
2、icates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope*1.1 This specification covers methyl n-amyl ketone (98 %grade) for use in paint, varnish, lacquer, and related products.1.2 For specific hazard information and gu
3、idance, see thesuppliers Material Safety Data Sheet for materials listed in thisspecification.1.3 The following applies to all specified limits in thisstandard; for purposes of determining conformance with thisstandard, an observed value or a calculated value shall berounded off “to the nearest unit
4、” in the last right-hand digitused in expressing the specification limit, in accordance withthe rounding-off method of Practice E 29.2. Referenced Documents2.1 ASTM Standards:D 268 Guide for Sampling and Testing Volatile Solventsand Chemical Intermediates for Use in Paint and RelatedCoatings and Mat
5、erial2D 1078 Test Method for Distillation Range of VolatileOrganic Liquids2D 1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)2D 1364 Test Method for Water in Volatile Solvents (KarlFischer Reagent Titration Method)2D 1613 Test Method for Acidity in Volatile Solvents andChemical In
6、termediates Used in Paint, Varnish, Lacquer,and Related Products2D 3893 Test Method for Purity of Methyl Amyl Ketone andMethyl Isoamyl Ketone by Gas Chromatography2D 4052 Test Method for Density and Relative Density ofLiquids by Digital Density Meter3E 1 Specification for ASTM Thermometers4E 29 Prac
7、tice for Using Significant Digits in Test Data toDetermine Conformance with Specifications5E 300 Practice for Sampling Industrial Chemicals62.2 Federal Specification:PPP-C-2020 Chemicals, Liquid, Dry, and Paste: Packagingof73. Properties3.1 Methyl n-amyl ketone shall conform to the followingrequirem
8、ents:Apparent specific gravity20/20Cor25/25C0.8150.818or0.8120.815Color, Pt-Co scale, max 10Distillation, 760 mm Hg, CInitial boiling point, minDry point, max147153.5Water, max, weight % 0.1Acidity, as acetic acid, max, weight % 0.02Purity, min, weight % 984. Sampling4.1 The material shall be sample
9、d in accordance withPractice E 300.5. Test Methods5.1 The properties enumerated in this specification shall bedetermined in accordance with the following ASTM methods.5.1.1 Apparent Specific GravityDetermine the specificgravity by any convenient method that is accurate to the thirddecimal place, the
10、 temperature of both specimen and waterbeing 20 or 25C. (See Test Method D 4052 and the SpecificGravity section of Guide D 268.)5.1.2 ColorTest Method D 1209.5.1.3 Distillation RangeTest Method D 1078, using anASTM Solvents Distillation Thermometer 42C having a rangefrom 95 to 255C and conforming to
11、 the requirements ofSpecification E 1.5.1.4 WaterTest Method D 1364.5.1.5 AcidityTest Method D 1613.1This specification is under the jurisdiction of ASTM Committee D01 on Paintand Related Coatings, Materials, and Applications and is the direct responsibility ofSubcommittee D01.35 on Solvents, Plasti
12、cizers, and Chemical Intermediates.Current edition approved July 10, 2003. Published August 2003. Originallyapproved in 1984. Last previous edition approved in 1990 as D 4360 - 90 (1999).2Annual Book of ASTM Standards, Vol 06.04.3Annual Book of ASTM Standards, Vol 05.02.4Annual Book of ASTM Standard
13、s, Vol 14.03.5Annual Book of ASTM Standards, Vol 14.02.6Annual Book of ASTM Standards, Vol 15.05.7Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,Section D, 700 Robbins Ave., Philadelphia, PA 19111-50981*A Summary of Changes section appears at the end of this standard.Copyright
14、ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.5.1.6 PurityTest Method D 3893.6. Packaging and Package Marking6.1 Package size to be agreed upon between the purchaserand the supplier.6.2 Packaging shall conform to applicable carrier rules andr
15、egulations or when specified shall conform to SpecificationPPP-C-2020.7. Keywords7.1 2-heptanone; MAK; methyl n-amyl ketone; solventsSUMMARY OF CHANGESCommittee D01 has identified the location of selected changes to this standard since the last issue(D 4360 - 90 (1999) that may impact the use of thi
16、s standard.(1) Added Practice E 29 on significant digits to the scope.(2) Added Practice E 29 to the Referenced Documents section.(3) Inserted the word “or” between the apparent specificgravity specifications to allow the manufacturer to select justone of the two specified temperatures, 20 or 25C fo
17、r testing,rather than requiring testing at both temperatures.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such p
18、atent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited e
19、ither for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fai
20、r hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).D4360032
