1、 ISO 2012 Thermal insulating products for building applications Determination of long- term water absorption by immersion Produits isolants thermiques destins aux applications du btiment Dtermination de labsorption deau long terme par immersion INTERNATIONAL STANDARD ISO 16535 First edition 2012-05-
2、15 Reference number ISO 16535:2012(E) ISO 16535:2012(E) ii ISO 2012 All rights reserved COPYRIGHT PROTECTED DOCUMENT ISO 2012 All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including ph
3、otocopying and microfilm, without permission in writing from either ISO at the address below or ISOs member body in the country of the requester. ISO copyright office Case postale 56 CH-1211 Geneva 20 Tel. + 41 22 749 01 11 Fax + 41 22 749 09 47 E-mail copyrightiso.org Web www.iso.org Published in S
4、witzerland ISO 16535:2012(E) ISO 2012 All rights reserved iii Contents Page Foreword iv Introduction v 1 Scope 1 2 Normative references . 1 3 Principle . 1 4 Apparatus 1 5 Test specimens 4 5.1 Dimensions of test specimens 4 5.2 Number of test specimens 4 5.3 Preparation of test specimens . 4 5.4 Con
5、ditioning of test specimens 4 6 Procedure 5 6.1 Test conditions . 5 6.2 Test procedure . 5 7 Calculation and expression of results . 7 7.1 General . 7 7.2 Long-term water absorption by partial immersion . 7 7.3 Long-term water absorption by total immersion 7 8 Accuracy of measurement 8 9 Test report
6、 . 8 ISO 16535:2012(E) Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in
7、a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commissi
8、on (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical c
9、ommittees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall n
10、ot be held responsible for identifying any or all such patent rights. ISO 16535 was prepared by Technical Committee ISO/TC 163, Thermal performance and energy use in the built environment, Subcommittee SC 1, Test and measurement methods. ISO 16535 includes the original EN 12087 prepared by Technical
11、 Committee CEN/TC 88 “Thermal insulating materials and products”, with the following clauses modified to reflect the conditions for tropical countries: Clause 5.4: Conditioning of test specimens; Clause 6.1: Test conditions; Clause 9: Test report. iv ISO 2012 All rights reserved ISO 16535:2012(E) In
12、troduction ISO 16535 is one of a series of existing European Standards on test methods which were adopted by ISO. This group of International Standards comprises the following group of interrelated standards: ISO Title Respective EN standard 12344 Thermal insulating products for building application
13、s Determination of bending behaviour EN 12089 12968 Thermal insulation products for building applications Determination of the pull-off resistance of external thermal insulation composite systems (ETICS) (foam block test) EN 13495 29465 Thermal insulating products for building applications Determina
14、tion of length and width EN 822 29466 Thermal insulating products for building applications Determination of thickness EN 823 29467 Thermal insulating products for building applications Determination of squareness EN 824 29468 Thermal insulating products for building applications Determination of fl
15、atness EN 825 29469 Thermal insulating products for building applications Determination of compression behaviour EN 826 29470 Thermal insulating products for building applications Determination of the apparent density EN 1602 29471 Thermal insulating products for building applications Determination
16、of dimensional stability under constant normal laboratory conditions (23 degrees C/50 % relative humidity) EN 1603 29472 Thermal insulating products for building applications Determination of dimensional stability under specified temperature and humidity conditions EN 1604 29764 Thermal insulating p
17、roducts for building applications Determination of deformation under specified compressive load and temperature conditions EN 1605 29765 Thermal insulating products for building applications Determination of tensile strength perpendicular to faces EN 1607 29766 Thermal insulating products for buildi
18、ng applications Determination of tensile strength parallel to faces EN 1608 29767 Thermal insulating products for building applications Determination of short- term water absorption by partial immersion EN 1609 29768 Thermal insulating products for building applications Determination of linear dimen
19、sions of test specimens EN 12085 29769 Thermal insulating products for building applications Determination of behaviour under point load EN 12430 29770 Thermal insulating products for building applications Determination of thickness for floating-floor insulating products EN 12431 29771 Thermal insul
20、ating materials for building applications Determination of organic content EN 13820 ISO 2012 All rights reserved v ISO 16535:2012(E) 29803 Thermal insulation products for building applications Determination of the resistance to impact of external thermal insulation composite systems (ETICS) EN 13497
21、 29804 Thermal insulation products for building applications Determination of the tensile bond strength of the adhesive and of the base coat to the thermal insulation material EN 13494 29805 Thermal insulation products for building applications Determination of the mechanical properties of glass fib
22、re meshes EN 13496 16534 Thermal insulating products for building applications Determination of compressive creep EN 1606 16535 Thermal insulating products for building applications Determination of long- term water absorption by immersion EN 12087 16536 Thermal insulating products for building appl
23、ications Determination of long- term water absorption by diffusion EN 12088 16537 Thermal insulating products for building applications Determination of shear behaviour EN 12090 16546 Thermal insulating products for building applications Determination of freeze- thaw resistance EN 12091 16544 Therma
24、l insulating products for building applications Conditioning to moisture equilibrium under specified temperature and humidity conditions EN 12429 16545 Thermal insulating products for building applications Determination of behaviour under cyclic loading EN 13793 A further group of existing European
25、Standards on test methods for products used to insulate building equipment and industrial installations comprises the following group of interrelated International Standards: ISO 12623 Thermal insulating products for building equipment and industrial installations Determination of short-term water a
26、bsorption by partial immersion of preformed pipe insulation EN 13472 ISO 12624 Thermal insulating products for building equipment and industrial installations Determination of trace quantities of water soluble chloride, fluoride, silicate, sodium ions and pH EN 13468 ISO 12628 Thermal insulating pro
27、ducts for building equipment and industrial installations Determination of dimensions, squareness and linearity of preformed pipe insulation EN 13467 ISO 12629 Thermal insulating products for building equipment and industrial installations Determination of water vapour transmission properties of pre
28、formed pipe insulation EN 13469 vi ISO 2012 All rights reserved INTERNATIONAL STANDARD ISO 16535:2012(E) Thermal insulating products for building applications Determination of long-term water absorption by immersion 1 Scope This International Standard specifies the equipment and procedures for deter
29、mining the long-term water absorption of test specimens. It is applicable to thermal insulating products. This International Standard specifies two options: Method 1: partial immersion; and Method 2: total immersion. The long-term water absorption by partial immersion is intended to simulate the wat
30、er absorption caused by long-term water exposure. The long-term water absorption by total immersion is not directly related to the conditions on site, but has been recognized as a relevant condition of test for some products in some applications. 2 Normative references The following referenced docum
31、ent is indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 29768, Thermal insulating products for building applications Determination of
32、 linear dimensions of test specimens 3 Principle 3.1 Partial immersion (Method 1). The long-term water absorption by partial immersion is determined by measuring the change in mass of a test specimen, the lower part of which is in contact with water for a period of 28 days. The excess water adhering
33、 to the surface, not absorbed by the test specimen, is removed by drainage in Method 1A or taken into account by deduction of the initial water uptake in Method 1B. 3.2 Total immersion (Method 2). The long-term water absorption by total immersion is determined by measuring the change in mass of the
34、test specimen, totally immersed in water, over a period of 28 days. The excess water adhering to the surface, not absorbed by the test specimen, is removed by drainage in Method 2A or taken into account by deduction of the initial water uptake in Method 2B. 4 Apparatus 4.1 Balance, allows the determ
35、ination of the mass of a test specimen to 0,1 g. 4.2 Water tank, with a device for keeping the water level constant to within 2 mm, and a device to keep the test specimen in the required position. Examples of test devices are given in Figures 1, 2 and 3. The device to keep the test specimen in posit
36、ion shall not cover more than 15 % of the cross-sectional area of the test specimen, which is exposed to water. The device shall be such that the original form of the test specimen is maintained. ISO 2012 All rights reserved 1 ISO 16535:2012(E) 4.3 Tap water, adjusted to a temperature of (23 5) C. 4
37、.4 Equipment for drainage. The principle for Methods 1A and 2A is illustrated in Figures 4a) and 4b). Dimensions in millimetres. Key 1 water tank 2 load to keep the test specimen in position 3 test specimen Figure 1 Example of equipment for the determination of water absorption by partial immersion
38、(Methods 1A and 1B) Dimensions in millimetres. Key 1 water tank 2 load to keep the test specimen in position 3 test specimen Figure 2 Example of equipment for the determination of water absorption by total immersion (Methods 2A and 2B) 2 ISO 2012 All rights reserved ISO 16535:2012(E) Dimensions in m
39、illimetres. Key 1 balance 2 weighing table 3 linkage 4 water container 5 water 6 mesh cage made of stainless material with fixing rods or a sinker large enough in mass to compensate for the upthrust of the test specimen 7 test specimen Figure 3 Example of equipment for the determination of water abs
40、orption by total immersion (Method 2C) a) ISO 2012 All rights reserved 3 ISO 16535:2012(E) b) Key 1 stainless steel mesh 2 test specimen 3 perforated stainless steel Figure 4 Examples of equipment for drainage 5 Test specimens 5.1 Dimensions of test specimens The thickness of the test specimens shal
41、l be the original product thickness. The test specimens shall be squares with squarely cut edges having sides of (200 1) mm. 5.2 Number of test specimens The number of test specimens shall be as specified in the relevant product standard or any other European technical specification. In the absence
42、of such a specification, at least four test specimens shall be used. NOTE In the absence of a product standard or any other technical specification, the number of test specimens can be agreed between parties. 5.3 Preparation of test specimens The test specimens shall be cut so that they do not inclu
43、de original product edges. Test specimens shall be prepared by methods that do not substantially change the original structure of the product. Any skins, facings and/or coatings shall be retained. NOTE Special methods of preparation, when needed, are given in the relevant product standard or any oth
44、er European technical specification. 5.4 Conditioning of test specimens The test specimens shall be stored for at least 6 h at (23 5) C. In case of dispute, they shall be stored at (23 2) C and (50 5) % relative humidity (RH) for the time stated in the relevant product standard with a minimum of 6 h
45、. In tropical countries, different conditioning and testing conditions are relevant. In this case, the conditions shall be (27 5) C and (65 5) % RH, and be stated clearly in the test report. 4 ISO 2012 All rights reserved ISO 16535:2012(E) 6 Procedure 6.1 Test conditions The test shall be carried ou
46、t at (23 5) C. In case of dispute it shall be carried out at (23 2) C. In tropical countries, different conditioning and testing conditions can be relevant. In this case, the conditions shall be (27 2) C and (65 5) % RH. 6.2 Test procedure The method shall be as specified in the relevant product sta
47、ndard or any other European technical specification. NOTE 1 In the absence of such a specification the method can be agreed between parties. The long-term water absorption is determined after 28 days immersion. NOTE 2 If requested, readings can be made at shorter time periods, e.g. after 7 day and 1
48、4 day immersion periods. The dimensions of the test specimens shall be measured in accordance with ISO 29768 to the nearest 0,5 mm before the test. If any dimensional changes are noticed after the immersion period, the dimensions of the test specimens should be measured again. 6.2.1 Long-term water
49、absorption by partial immersion (Method 1) 6.2.1.1 Method 1A (drainage) Weigh the test specimen to the nearest 0,1 g to determine its initial mass, m 0 . The test is made with half of the test specimens with one major face upwards. The other half are tested with the same major face downwards. Place the test specimen in the empty water tank and apply a sufficient load to keep it partially immersed when water is added. Carefull
